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Phosphorus sulfur heterocycles incorporating an O P(S) O or O P(S) S S P(S) O scaffold : one pot synthesis and crystal structure study

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Figure

Figure 1.Figure 1.  3131P-NMR spectra of disulfideP-NMR spectra of disulfide  66 at the reactions temperatures of 20 at the reactions temperatures of 20 °C and  ◦C and −−78 °C.78 ◦C
Table 1. Details of the x-ray data collections and refinements for compounds 2, 3, 5 and 6.
Figure 2. and , 312, 5. , 6 and 12Table 3. Single crystal X-ray structures ofFigure 2
Figure 3. Single crystal X-ray structures ofFigure 3. Single crystal X-ray structures of  99 and  and11 11 (hydrogen atoms omitted for clarity)
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