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Synthesis and structural dynamics of five coordinate Rh(III) and Ir(III) PNP and PONOP pincer complexes

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Figure

Table 1. The solid-state structures are notable for pseudos-quare pyramidal metal geometries about the metal, with near-ideal N20−M−C15 but distinctly obtuse P2−M1−P3 angles
Figure 1. Solid-state structures ofcomponent in 1b (left) and 2b (right) determined at 150 K
Figure 3. Variable-temperature 1H NMR spectra of 1a (CD2Cl2, 500MHz).
Table 3. Carbonyl Stretching Frequencies of PNP andPONOP Complexes (CH2Cl2)
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