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Novel fluorinated phosphorus–sulfur heteroatom compounds : synthesis and characterization of ferrocenyl and aryl phosphonofluorodithioic salts, adducts, and esters

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Figure

Table 1. Details of the X-ray data collections and refinements for 3, 13, 14, and 18.
Figure 2. (S(2)–P(1)–C(1) 108.6(3), O(1)–P(1)–C(1) 99.8(3), S(3)–P(2)–F(1) 100.7(4), S(3)–P(2)–O(1) a) Single crystal structure of 13 (hydrogen atoms omitted for clarity)
Figure 3. ([110.9(4)], S(2)–P(1)–O(1) 108.7(3) [110.3(3)], S(2)–P(1)–C(1) 111.7(4) [111.6(3)],  a) Single crystal structure of 14
Figure 4. (a) Singlecrystal structure of 18. Selected bond lengths (Å) and angles (°)  (esds in parentheses): P(1)–S(1) 1.9020(13), P(3)–S(3) 1.9097(13), P(1)–S(6) 2.0762(14), P(3)–S(4) 2.0730(14), P(1)–O(2) 1.629(2), P(3)–O(2) 1.628(2), S(4)–C(11) 1.830(4

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