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Local surface structure and composition control the hydrogen evolution reaction on iron nickel sulfides

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Figure

Figure 2A for the schematic experimental set-up). By means of SECCM, amperometric or voltammetric measurements were performed in the confined area defined by the meniscus (droplet)
Figure 3. A) Averaged LSVs (scan rate, ν = 250 mV s‒1, [HClO4] = 0.1 M) obtained from a hexagonal Fe4.5Ni4.5S8 (111) crystal basal surface (blue trace) and macroscopic defect site (‘crack’, pink trace) and; Fe-rich areas of platelet-shaped crystals (red an

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