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4, a gallium ferrocenophane

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Figure

Fig. 2:  View of 4, showing the hydrogen bonds between cations and anion. Selected bond lengths [pm] and angles [°]: Ga(1)-C(1) 194.4(3)  , Ga(1)-O(1) 189.5(2) , Ga(1)-O(3) 189.2(2) , Ga(1)-O(5) 189.4(2) , C(6)-O(1) 131.4(3), C(6)-O(2) 124.0(3), C(8)-O(5) 130.9(4), C(8)-O(6) 123.5(4), C(10)-O(3) 131.0(3), C(10)-O(4) 123.3(3); O(1)-Ga(1)-O(3) 101.95(9), O(1)-Ga(1)-O(5) 103.38(9), O(3)-Ga(1)-O(5) 99.3(1),  O(1)-Ga(1)-C(1) 119.55(9), O(3)-Ga(1)-C(1) 107.6(1), O(5)-Ga(1)-C(1) 121.6(1), O(1)-C6)-O(2) 120.0(3)
Table I. Crystal and Intensity Collection Data for Complexes 4, 5 and 6.

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