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Iridium complexes of the conformationally rigid IBioxMe4Ligand : hydride complexes and dehydrogenation of cyclooctene

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Figure 1 : Solid-state structures of iridium IBioxMe4 hydride complexes. Thermal ellipsoids for selected atoms are drawn at the 50% probability level; most hydrogen atoms (hydrides located in 4), anions and solvent (5) are omitted for clarity;
Figure 2 : Solid-state structures of 6 (left), 7 (centre) and 8 (right). Thermal ellipsoids for selected atoms are drawn at the 50% probability level; most hydrogen atoms and anions are omitted for clarity
Figure 3: Optimised geometries of model isomers of 6, annotated with selected bond lengths (Å) and angles (º) – metrics associated with the alkene centroids in purple.21

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