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Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 1

Kingdom of Saudi Arabia

The National Commission for Academic Accreditation & Assessment

Course Specifications

(CS)

Spectroscopy of Inorganic Compounds

(CHEM 422)

(2)

Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 2

Institution: Tabuk University Date of Report: 2/1/1436H College/Department : Faculty of Science /Chemistry Department

A. Course Identification and General Information

1. Course title and code: Spectroscopy of Inorganic compounds (CHEM 422)

2. Credit hours : 3 Hours (2 + 0)

3. Program(s) in which the course is offered. (Chemistry)

4. Name of faculty member responsible for the course: Dr Hatem Ahmed Naji Al-Aoh 5. Level/year at which this course is offered: 8th level / 4th Year

6. Pre-requisites for this course (if any) : CHEM 421

7. Co-requisites for this course (if any):

N/A

8. Location if not on main campus:Chemistry Department Main Campus (Male students)

9. Mode of Instruction (mark all that apply)

a. Traditional classroom What percentage? b. Blended (traditional and online) What percentage? c. e-learning What percentage? d. Correspondence What percentage? f. Other What percentage?

Comments:

10%

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Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 3

B Objectives

1. What is the main purpose for this course?

• Understand the interpretation of different spectral data that correlated to the structure

and the geometry of the complexes.

• .Apply spectroscopic techniques for coordinate compounds.

• Assign the geometry of coordination compounds by spectroscopic methods.

• Understand the different methods used for determination of the magnetic properties.

• Differentiate between the organometallic and coordination compounds.

2. Briefly describe any plans for developing and improving the course that are being implemented. (e.g. increased use of IT or web based reference material, changes in content as a result of new research in the field)

• Help students to analyze the chemical problems correlated to the course and how to

select appropriate methods to solve such problems.

• New and updated text books.

• Related Web Sites.

• Provide time for tutorial

• Reduce number of students in class.

C. Course Description (Note: General description in the form to be used for the Bulletin or handbook should be attached)

1. Topics to be covered

No of weeks

1B Contact hours 2B

Topics

2

4

The vectors model and Russel -Saunders splitting energy level.

3

6

Term symbols of d

P

n

P

ion in Oh and Td complexes.

3

6

Orgel diagram of d

P n P

in Oh and Td complexes).

(4)

Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 4

applications for coordinate compounds.

• Electron spin resonance ESR.

2

4

Calculation and measurements of magnetic properties and

using Faraday and Gouy methods.

3

6

Chemistry of organometallic compounds of transition

metals.

Practical Work

1

3

Review and introduction to use of spectroscopic techniques in

coordination chemistry.

4

12

Synthesis and interpretation it’s UV-Vis. Spectra of some

transition metal complexes. (4 experiments).

3

9

Calculation of

RoR

for some transition metal complexes (2

experiments)

4

12

Synthesis and measuring of paramagnetic susceptibility some

transition metal complexes (2 experiments) (3 experiments).

1

3

Use of

P

1

P

H NMR to differentiate between

tris-acetylacatonatovandium(III) and aluminium(III) complexes.

2

6

Use of ESR to differentiate between

tris-acetylacatonatovandium(III) and aluminium(III) complexes.

2. Course components (total contact hours and credits per semester):

Lecture Tutorial Laboratory Practical Other: Total Contact

Hours

30 NA NA 45 NA 75

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Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 5

3. Additional private study/learning hours expected for students per week.

4. Course Learning Outcomes in NQF Domains of Learning and Alignment with Assessment Methods and Teaching Strategy

NQF Learning Domains And Course Learning Outcomes

Course Teaching Strategies

Course Assessment Methods 1.0 Knowledge

1.1

• Describe the basic principles and the

instrumental design of a variety of

spectroscopic techniques and methods

used for determination the magnetic

susceptibility.

• Lectures.

• Discussion in class.

• In class – quizzes

and homework.

1.2

• Demonstrate the knowledge of data

acquisition and analysis for various

techniques.

• The participation of the

discussion in class.

Mid-term and final

exams

1.3

• Interpret the UV-Vis,

1

HNMR and

ESR spectra for structure identification.

• Examples and solving problems of some inorganic compounds

• Presentation of the

homework

assignments.

The participation of

the discussion.

1.4

• Implement suitable methods of

investigation coordination compounds.

• Lectures.

Problems solving.

• Mid-term and final

exams

• In class – quizzes

and homework.

1.5

• Interpret the relevant chemical literature. • Lectures.

• Problems solving.

• Mid-term and final

exams

• In class – quizzes

and homework.

2.0 Cognitive Skills

2.1

• Compare various spectroscopic

methods and assess the advantages and

• Lectures

• Problems solving.

• In-class quizzes

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Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 6

2.2

• Demonstrate capability of choosing the

appropriate spectroscopic method for a

particular investigation.

• Lectures

• Discussion in class.

• Mid-term and final

exams.

2.3

• Demonstrate the differences between

various types of instruments in terms of

parts and functions.

• Encouraging students

to work during lectures

as groups.

• Performance in

discussions during

lectures.

2.4

• Identify the unknown inorganic

compounds by interpretation of

combined spectra.

Working individually or

as groups inside the

class.

Self performance in

class.

3.0 Interpersonal Skills & Responsibility 3.1

• Work effectively both individually and

in teams in both classroom and

laboratory.

Working individually or

as groups inside the

class.

• Self performance

in class.

3.2

• Demonstrate the ethical and

professional standards articulated by

professional organizations (e.g. the

American Chemical Society).

• Lectures

• Discussion in class

• Written

presentation of

assignments.

3.3

• Understand the interrelationships

among chemistry, technology, and

global society, and of the societal

implications of new developments in

science.

• Lectures

• Discussion in class

• Direct contact

during office

hours.

3.4

4.0 Communication, Information Technology, Numerical

4.1

• Evaluate the published works.

• Independent study.

• Performance in

problem solving

and assignments.

4.2

• Acquire a working knowledge of basic

research methodologies, data analysis

• Communicate

effectively in writing,

• Group and

personal tutorial

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Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 7

and interpretation.

orally and through

scientific diagrams.

classes.

4.3

• Formulate significant research

questions.

• Independent study.

• Discussion in class.

• Homework

assignments.

4.4

• Read, evaluate, and interpret

numerical, chemical and general

scientific information.

Problem solving in

class.

• Homework

assignments.

4.5

• Demonstrate effective written and oral

communication skills, especially the

ability to transmit complex technical

information in a clear and concise

manner.

Problem solving in

class.

Homework

assignments.

5.0 Psychomotor

5.1

Handle chemicals, glassware and

instruments.

Carry experiments in

lab.

• Laboratory

performance

(following the

procedure,

handling

chemicals and

glassware).

5. Schedule of Assessment Tasks for Students During the Semester Assessment task (e.g. essay, test, group project, examination,

speech, oral presentation, etc.)

Week Due Proportion of Total Assessment

1

Quiz 1

Week 3

5%

2

First Mid-term exam.

Week 7

25%

3

Quiz 2

Week 9

5%

4

Second Mid-term exam

Week 13

25%

(8)

Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 8

D. Student Academic Counseling and Support

1. Arrangements for availability of faculty and teaching staff for individual student consultations and academic advice. (include amount of time teaching staff are expected to be available each week)

Academic advice as needed by the students.

Office hours (10 per week for all students)

E. Learning Resources 1. List Required Textbooks

• Inorganic Chemistry, C. Housecraft, Alan G. Sharpe, 3rd

edition, Prentice Hall, 2007. • Inorganic Chemistry, D. Shriver and P. Atkins, , 4th

edition, Oxford University press (2006).

• Inorganic Chemistry, James E. House, Elsevier Inc., 2008 2. List Essential References Materials (Journals, Reports, etc.)

• Structural Methods in Molecular Inorganic Chemistry, C. Morrison, D., Rankin, N.W. Mitzel,

Wiely, 2013.

• Inorganic electronic structure and spectroscopy, Edward I. Solomon, A. Barry P. Lever, John

Wiley&Sons, 2006.

3. List Recommended Textbooks and Reference Material (Journals, Reports, etc)

• NMR spectroscopy in inorganic chemistry, , J. A. Iggo, Oxford Uiversity.Press,1999. • B.J. Hathaway, A.A.G. Tomlinson, Coord. Chem. Rev. 5 (1970) 1-43.

• Journal of American Chemical Society. • Inorganic Chemistry

• Transition Metal Chemistry • Polyhedron

4. List Electronic Materials (eg. Web Sites, Social Media, Blackboard, etc.) •

http://ocw.mit.edu/courses/chemistry/

http://www.iupac.org/

http://www.sciencedirect.com/

http://sdl.edu.sa/SDLPortal/AR/Publishers.aspx

.

5. Other learning material such as computer-based programs/CD, professional standards or regulations and software.

(9)

Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 9

Handouts.

Data show presentations.

Multimedia associated with textbooks.

F. Facilities Required

Indicate requirements for the course including size of classrooms and laboratories (i.e. number of seats in classrooms and laboratories, extent of computer access etc.)

1. Accommodation (Classrooms, laboratories, demonstration rooms/labs, etc.)

Classroom with 25 seats.

• Spectroscopy lab contains UV-Vis spectrophotometer, NMR spectrophotometer and magnetic susceptibility balance

2. Computing resources (AV, data show, Smart Board, software, etc.)

• Data Show • AV presentations

Simulated education programs if available.

Molecular models.

3. Other resources (specify, e.g. if specific laboratory equipment is required, list requirements or attach list)

• UV-Vis Spectrophotometer. • Magnetic Susceptibility Balance. • ESR Spectrometer.

• NMR spectrophotometer. • Electric Balance

• Glassware (beakers, measuring flasks, cylinders, pipettes and watch glass ) • Required Chemicals  Copper sulphate  Nickel Chloride  Potassium Permanganate  Potassium Dichromate  Chromium Chloride  Ferric Chloride Ferrous Sulphate  Manganese sulphate

G Course Evaluation and Improvement Processes

1 Strategies for Obtaining Student Feedback on Effectiveness of Teaching

• Course evaluation by students.

2 Other Strategies for Evaluation of Teaching by the Program/Department Instructor

Peer consultation on teaching.

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Form 5a_Course Specifications _SSRP_1 JULY 2013 Page 10

Discussion with Inorganic group.

3 Processes for Improvement of Teaching

Conducting workshops presented by experts on the teaching methodologies.

Departmental versions on its methods at teaching.

4. Processes for Verifying Standards of Student Achievement (e.g. check marking by an independent member teaching staff of a sample of student work, periodic exchange and remarking of tests or a sample of assignments with staff at another institution)

Assigning group of members teaching the same course to grade same questions for various students.

Conducting standard exams.

Faculty member from other universities to review and evaluate the accuracy of grading policy.

5 Describe the planning arrangements for periodically reviewing course effectiveness and planning for improvement.

The chairman of the department and faculty council take the responsibility.

The course material should be reviewed by departmental, faculty and higher council.

Faculty or Teaching Staff:Dr Hatem Ahmed Naji Al-Aoh

Signature: _______________________________ Date Report Completed: 26/10/2014 +9Received by: Prof. Dr. Mohsen M. Zareh Dean/Department Head

References

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