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(see attached scope of accreditation for fields of testing and accredited test methods)

This is to signify that

PROFESYONEL ÇEVRE ANALIZ LAB. GIDA TARIMSAL VE KAL. HIZ. SAN. VE TIC. A.Ş

TEOMANPAŞA MAH.GAZI BULVARI NO: 345

KEPEZ, ANTALYA

TURKEY

Testing Laboratory TL-577

has met the requirements of the IAS Accreditation Criteria for Testing Laboratories (AC89), has demonstrated compliance with

ISO/IEC Standard 17025:2005,

General requirements for the competence of testing and calibration laboratories

, and has been

accredited, commencing January 30, 2015, for the test methods listed in the approved scope of accreditation.

Patrick V. McCullen

C. P. Ramani, P.E.

(2)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş

Ulas Goktas

Teomanpaşa Mah. Gazi Bulvarı No: 345

Laboratory Manager

Kepez, Antalya

+0 242 339 12 22

Turkey

FIELDS OF TESTING ACCREDITED TEST METHODS

Category

Product Group

Microbiology Food and Animal Feed ISO 16649-1: Analysis of E.coli (membrane method) in food and animal feed,

TS EN ISO 6579 (ISO 6579): Detection of Salmonella spp. in Food and

animal feed,

TS 3522: Analysis of rope spore in food and animal feed,

BS ISO:21528-2: Analysis of Enterobacteriaceae in food and animal feed,

TS EN ISO 7937 (ISO 7937): Analysis of Sulfite reducing anaerobes

(Clostridium perfringens) in Food and animal feed,

TS EN ISO 4833-1 (ISO 4833-1): Analysis of Mesophilicaerobicbacteria in

foodandanimalfeed,

ISO 16649-2: Analysis of E.coli in food and animal feed,

ISO 11290-1 / AMD 1: Detection of Listeria monocytogenes in food and

animal feed,

ISO 16654: Detection of E.coli O157 in food and animal feed,

TS ISO 4832: Analysis of Coliform bacteria in food and animal feed,

ISO 16649-3: Analysis of E.coli (most probable number method-EMS) in food

and animal feed,

ISO TS 22964: Detection of Enterobacter (Cronobacter) sakazakii in food and

animal feed,

TS 6582-1 - EN ISO 6888-1 (ISO 6888-1): Analysis of Coagulase-positive

staphylococci in food and animal feed,

TS EN ISO 7932 (ISO 7932): Analysis of Bacillus cereus in food and animal

feed,

AOAC Official Method 993.06: Detection of Staphylococcal enterotoxinin

food and animal feed,

ISO 21872-1: Detection of V. parahaemolyticus, V. cholerae in food and

animal feed,

TS ISO 21527-1 (ISO 21527-1): Yeast, mold analysis (water activity greater than 0.95) in food and animal feed

TS ISO 21527-2: Yeast, mold analysis (water activity of less than 0.95) in food and animal feed.

Water XP T 90-412 Membran Filter: Analysis of Pathogen Staphylococcus in water,

TS EN ISO ISO 6222 (ISO 6222): Analysis of culturable water (22°C and

36°C),

TS EN ISO 9308-1 Membrane Filter (ISO 9308-1): Analysis of E.

(3)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

FIELDS OF TESTING ACCREDITED TEST METHODS

Category

Product Group

Microbiology (continued)

Water ISO 16266/Membrane Filter: Analysis of Pseudomonas aeruginosa in water,

TS EN ISO 7899-2 Membrane Filter (ISO 7899-2): Analysis of Enterococcus

in water,

ISO 11731-2 Membrane Filter: Detection of Legionella in water,

BS ISO 19250 MEMBRANE FILTER: Detection of Salmonella spp.in water.

Surfaces BS ISO 18593 - ISO 16649-2: Analysis of E. coli on all surfaces that come

into contact with food,

BS ISO 18593 - TS EN ISO 7932: Analysis of B. cereus on all surfaces that

come into contact with food,

BS ISO 18593 - TS 6582-1 - EN ISO 6888-1: Analysis of S. aureus on all surfaces that come into contact with food,

BS ISO 18593 - TS ISO 4832: Analysis of coliform bacteria on all surfaces that come into contact with food,

BS ISO 18593 – TS EN ISO 4833-1 (ISO 4833-1) Analysis of Total

mesophilic aerobic bacteria on all surfaces that come into contact with food,

BS ISO 18593 - TS EN ISO 6579: Detection of Salmonella spp. on all

surfaces that come into contact with food.

Cosmetics ISO 21150: Analysis of E.coli in cosmetics,

ISO 22717: Analysis of Pseudomonas aeruginosa in cosmetics,

ISO 22718: Analysis of Staphylococcus aureus in cosmetics,

ISO 16212: Analysis of yeast and mouldin cosmetics,

ISO 21149: Analysis of Mesophilic aerobic bacteria in cosmetics,

Biotechnology Meat and Meat Products DIAGEN study protocol/ELISA-TEK Cooked meat speciation

kits:Determination of types of meat and meat products

Pesticide Fresh Vegetables and

Fruits

EN 15662 (Quechers) *

Dried Vegetables and Fruits

AOAC Method 2007.01 (Quechers): Pesticide Analysis *

Whole Grains All of Feed and Feed

Additives, Oil seeds All Spices All Dried Fatty Fruits

(Dried Fruits) All of Feed and Feed

Additives

Mycotoxins All Dried Vegetables and

Fruits

Rapid Communications In Mass Spectrometry Rapid Commun. Mass

Spectrom.2006; 20:2649-2659: Analysis of Aflatoxin B1 and Total Aflatoxin

(B1 + B2 + G1 + G2) All Spices

(4)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

FIELDS OF TESTING ACCREDITED TEST METHODS

Category

Product Group

Mycotoxins (continued)

All Dried Fatty Fruits (Dried Fruits)

Rapid Communications In Mass Spectrometry Rapid Commun. Mass

Spectrom.2006; 20:2649-2659: Analysis of Aflatoxin B1 and Total Aflatoxin

(B1 + B2 + G1 + G2) All of Feed and Feed

Additives

Chemistry Vegetables and Fruits TSE 6183: Determination of nitrite-nitrate in foods

All fishery Products In house method

Journal of Chromatography B, 693 (1997) 23-30 HPLC Determination of

Biogenic Amines in fish implicated in food poisoning: Analyses of

histamine. All Water and Pool

Water

TS 7159: Determination of Ammonium by spectrophotometric method,

TS 7526 - EN 26777: Determination of Nitrite,

TS ISO 10566: Determination of aluminum by spectrophotometric method,

TS 6231: Determination of Nitrate by spectrophotometric method,

TS EN ISO 10523: Determination of pH,

TS 9748 - EN 27888: Determination of Electrical Conductivity,

T.96 (SOP) In house method (using TS EN 902): Determination of hydrogen

peroxide by the titrimetric method,

TS 3790 - EN ISO 9963-1: Determination of total and composite alkalinity by

the titrimetric method,

Apha SM 3500-Cu C.BathoCuproine Method: Determination of copper (Cu)

by spectrophotometric method,

TS 6229 - EN ISO 7393-2: Determination of the free and bound chlorine by

the colorimetric method,

T.64 (SOP) In house method: "Photometric determination of the free and

bound chlorine in water and pool water".

T.79 (SOP) In house method (Analytical Chemistry, Vol.73, No.14:2001):

Determination of cyanuric acid by HPLC,

T-179 (SOP) In house method: Determination of cyanuric acid by

spectrophotometric method

Apha SM 2130-B Nephelometric Method: Determination of turbidity by the

nephelometric method,

Apha SM 2120-C: Determination of the color by spectrophotometric method -

wavelength-to-multipoint,

Apha SM 2550-B: Determination of temperature,

T-47 (SOP) In house method: Biguanid.

Chemistry Soil TS 8336: Determination of organic matter (Walkley-Black Method),

TS 8333: Determination of water saturation (soil texture),

TS 8337 - ISO 11261: Determination of total nitrogen (Improved Kjeldahl

Method),

TS 8334: Determination of Salt,

TS ISO 10390: Determination of pH,

(5)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

FIELDS OF TESTING ACCREDITED TEST METHODS

Category

Product Group

Chemistry (continued)

Fertilizer TS 5869 - ISO 5073: Determination of Humic-Fulvic,

TS EN 15475 - TS EN 15476 – Turkish Gazette No. 28956Regulation of Market Surveillance and Control of fertilizer charter an additional 3 or

annex 3,AOAC 892.01: Determination of ammonium nitrogen, nitrate nitrogen

in chemical fertilizers,

TS ISO 10390: Determination of pH in chemical and organic fertilizers,

TS ISO 11265: Determination of Electrical Conductivity,

AOAC 967.05 - AOAC 967.04 - TS 2832: Determination of organic matter in

organic fertilizers,

TS 2832, Kacar- Kütük 2009:Determination of moisture content of fertilizers,

TS 6798-DUMAS 1962 BREMNER 1965: Determination of total nitrogen

(Dumas Method),

Turkish Official Gazette No. 28956 Regulation of Market Surveillance and Control of fertilizer charter an additional 3 or annex 3, TS 2832, TS EN

15958: Determination of water soluble phosphorus in chemical fertilizer,

TS 2832, Turkish Official Gazette No. 28956 - Regulation of Market

Surveillance and Control of fertilizer (annex 3), TS EN 15604: Determination

of urea nitrogen,

Turkish Official Gazette No. 28956 - Regulation of Market Surveillance and

Control of fertilizer (annex 3), TS EN 15961: Determination of water soluble

sulfur dioxide in chemical fertilizers,

Turkish Official Gazette No. 28956 - Regulation of Market Surveillance and

Control of fertilizer (annex 3), TS EN 15925: Determination of total sulfur,

Turkish Official Gazette No. 28956 - Regulation of Market Surveillance and

Control of fertilizer (annex 3), TS 2832/ TS EN 15477: Determination of

water-soluble potassium in chemical fertilizer

Chemicals Cosmetics T.188 (SOP) In house method: About required Composition Analysis

Methods for the Control of Cosmetic Products Notification No:İEG/2005/2:

Analysis of Alcohol (methanol) in cosmetics (non-aerosol samples only)

T.189 (SOP) In house method (J.Chem.Pharm.Res.,2010,2(6):92-97):

Analysis of Heavy Metal ; Lead(Pb) , Cadmium(Cd) , Arsenic(As) , Tin(Sn), Nickel(Ni) , Mercury(Hg) ‘in cosmetics

Sampling Water TS EN ISO 5667-1 - TS EN ISO 5667-3 - TS EN ISO 5667-14: Taking Water

samples Microbiological

Sampling

Water TS EN ISO 19458: Taking Water Sampling for microbiological analysis

(6)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

Table 1. List of pesticides that can be traced.

No.

Pesticide

Equipment Used

1 2,4,D LC-MS/MS 2 2,4-5T GC-MSD 3 4.4 Dichlorobenzophenone GC-MSD 4 Acephate LC-MS/MS 5 Acetamiprid LC-MS/MS 6 Acetochlor LC-MS/MS 7 Acibenzolar-S-methyl LC-MS/MS 8 Aclonifen LC-MS/MS 9 Acrinathrin LC-MS/MS 10 Alachlor LC-MS/MS 11 Aldicarb LC-MS/MS 12 Aldicarb-sulfone LC-MS/MS 13 Aldicarb-sulfoxide LC-MS/MS 14 Aldrin (HHDN) GC-MSD 15 Alpha-Cypermethrin GC-MSD 16 Alpha-Endosulfan GC-MSD 17 Amitraz LC-MS/MS 18 Anilazine LC-MS/MS 19 Atrazine LC-MS/MS 20 Azinphos-ethyl LC-MS/MS 21 Azinphos-methyl LC-MS/MS 22 Azimsulfuron LC-MS/MS 23 Azoxystrobin LC-MS/MS 24 Bendiocarb LC-MS/MS 25 Benfuracarb LC-MS/MS 26 Beta-Cyfluthrin GC-MSD 27 Beta-Endosulfan GC-MSD 28 Bifenthrin LC-MS/MS 29 Bitertanol LC-MS/MS 30 Bromacil LC-MS/MS 31 Bromophos-ethyl LC-MS/MS 32 Bromopropylate GC-MSD 33 Bromoxynl LC-MS/MS 34 Bromuconazole LC-MS/MS 35 Bupirimate LC-MS/MS 36 Buprofezin LC-MS/MS 37 Butralin LC-MS/MS 38 Cadusafos LC-MS/MS 39 Captafol GC-MSD 40 Captan GC-MSD

(7)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

No.

Pesticide

Equipment Used

41 Carbaryl LC-MS/MS 42 Carbendazim ,Benomyl LC-MS/MS 43 Carbofuran LC-MS/MS 44 Carbosulfan LC-MS/MS 45 Carboxin LC-MS/MS 46 Carfentrazone-ethyl LC-MS/MS 47 Chlorfenson GC-MSD 48 Chlorfenvinphos LC-MS/MS 49 Chlorfluazuron LC-MS/MS 50 Chloridazon LC-MS/MS 51 Chlorobenzilate GC-MSD 52 Chlorothalonil GC-MSD 53 Chloroxuron LC-MS/MS 54 Chlorpropham LC-MS/MS 55 Chlorpyrifos LC-MS/MS 56 Chlorpyrifos-methyl LC-MS/MS 57 Chlorsulfuron LC-MS/MS 58 Cinidon-ethyl LC-MS/MS 59 Clofentezine LC-MS/MS 60 Cyanazine LC-MS/MS 61 Cycloate GC-MSD 62 Cyfluthrin GC-MSD 63 Cymoxanil LC-MS/MS 64 Cypermethrin GC-MSD 65 Cyproconazole LC-MS/MS 66 Cyprodinil LC-MS/MS 67 Cyromazine LC-MS/MS 68 Daminozide LC-MS/MS 69 Dazomet GC-MSD 70 Deltamethrin GC-MSD 71 DDD-2.4'- GC-MSD 72 DDD-4.4'- GC-MSD 73 DDE-2.4'- GC-MSD 74 DDE-4.4'- GC-MSD 75 DDT-2.4'- GC-MSD 76 DDT-4.4'- GC-MSD 77 Dialifos LC-MS/MS 78 Diazinon LC-MS/MS 79 Dicamba GC-MSD 80 Dichlofluanıde LC-MS/MS 81 Dichlorvos (DDVP) LC-MS/MS 82 Diclofop-methyl LC-MS/MS

(8)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

No.

Pesticide

Equipment Used

83 Dicofol GC-MSD 84 Dicrotophos LC-MS/MS 85 Diethofencarb LC-MS/MS 86 Difenconazole LC-MS/MS 87 Diflubenzuron LC-MS/MS 88 Dimethoate LC-MS/MS 89 Dimethomorph LC-MS/MS 90 Diniconazole LC-MS/MS 91 Dinobuton GC-MSD 92 Dinocap LC-MS/MS 93 Diphenamid LC-MS/MS 94 Diphenylamine GC-MSD 95 Disulfoton LC-MS/MS 96 Ditalimfos LC-MS/MS 97 Dithianon LC-MS/MS 98 Diuron LC-MS/MS 99 Dodine LC-MS/MS 100 Endrin GC-MSD 101 Endosulfan GC-MSD 102 Epoxiconazole LC-MS/MS 103 Esfenvalerate GC-MSD 104 Ethalfluralin GC-MSD 105 Ethiofencarb LC-MS/MS 106 Ethion LC-MS/MS 107 Ethofumesate LC-MS/MS 108 Ethoprophos LC-MS/MS 109 Etofenprox LC-MS/MS 110 Etrimfos LC-MS/MS 111 Famoxadone LC-MS/MS 112 Fenamıdone LC-MS/MS 113 Fenamiphos LC-MS/MS 114 Fenarimol LC-MS/MS 115 Fenbuconazole LC-MS/MS 116 Fenazaquın LC-MS/MS 117 Fenhexamid LC-MS/MS 118 Fenitrothion LC-MS/MS 119 Fenoxycarb LC-MS/MS 120 Fenpropathrin LC-MS/MS 121 Fenpropimorph LC-MS/MS 122 Fenthion LC-MS/MS 123 Fenvelarate GC-MSD 121 Fenpropimorph LC-MS/MS

(9)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

No.

Pesticide

Equipment Used

122 Fenthion LC-MS/MS 123 Fenvelarate GC-MSD 124 Fipronil LC-MS/MS 125 Flubenzimine LC-MS/MS 126 Flucythrinate LC-MS/MS 127 Fludioxonil LC-MS/MS 128 Flufenoxuron LC-MS/MS 129 Fluorochloridone LC-MS/MS 130 Fluroxypyr LC-MS/MS 131 Flusilazole LC-MS/MS 132 Folpet GC-MSD 133 Formetanate-hydroclor LC-MS/MS 134 Formothion GC-MSD 135 Furathiocarb LC-MS/MS 136 gamma-HCH (Lindane) GC-MSD 137 Haloxyfop-2-ethoxy-ethyl LC-MS/MS 138 Hexachlorobenzene GC-MSD 139 Hexaconazole LC-MS/MS 140 Hexaflumuron LC-MS/MS 141 Hexythiazox LC-MS/MS 142 Imazalil LC-MS/MS 143 Imiadcloprid LC-MS/MS 144 Ioxynil LC-MS/MS 145 Iprodione LC-MS/MS 146 Iprovalicarb LC-MS/MS 147 Isoproturon LC-MS/MS 148 Isoxafluate LC-MS/MS 149 Kresoxim-methyl LC-MS/MS 150 Lambda-Cyhalothrin GC-MSD 151 Lenacil LC-MS/MS 152 Linuron LC-MS/MS 153 Lufenuron LC-MS/MS 154 Malaoxon LC-MS/MS 155 Malathion LC-MS/MS 156 Mecarbam LC-MS/MS 157 Mesotrione LC-MS/MS 158 Metobromuron LC-MS/MS 159 Metalaxyl-Metalaxyl M LC-MS/MS 160 Metamitron LC-MS/MS 161 Methacrifos LC-MS/MS 162 Methamidophos LC-MS/MS 163 Methidathion LC-MS/MS

(10)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

No.

Pesticide

Equipment Used

164 Methoxychlor GC-MSD 165 Metolachlor LC-MS/MS 166 Metribuzin LC-MS/MS 167 Metsulfuron-methyl LC-MS/MS 168 Mevinphos LC-MS/MS 169 Molinate LC-MS/MS 170 Monocrotophos LC-MS/MS 171 Monolinuron LC-MS/MS 172 Myclobutanil LC-MS/MS 173 Nicosulfuron LC-MS/MS 174 Nitrofen GC-MSD 175 Nitrothal-isopropyl GC-MSD 176 Nuarimol LC-MS/MS 177 Omethoate LC-MS/MS 178 Oxadiazon LC-MS/MS 179 Oxadixyl LC-MS/MS 180 Oxamyl LC-MS/MS 181 Oxyfluorfen LC-MS/MS 182 Parathion-ethyl LC-MS/MS 183 Parathion-methyl LC-MS/MS 184 Penconazole LC-MS/MS 185 Pencycuron LC-MS/MS 186 Pendimethalin LC-MS/MS 187 Permethrin GC-MSD 188 Phenmedipham GC-MSD 189 Phenthoate LC-MS/MS 190 Phorate LC-MS/MS 191 Phosalone LC-MS/MS 192 Phosmet LC-MS/MS 193 Phoxim LC-MS/MS 194 Picolinafen LC-MS/MS 195 Pirimicarb LC-MS/MS 196 Pirimiphos methyl LC-MS/MS 197 Pirimiphos-ethyl LC-MS/MS 198 Prochloroz LC-MS/MS 199 Procymidone GC-MSD 200 Profenofos LC-MS/MS 201 Profoxydim-lithium LC-MS/MS 202 Propargite LC-MS/MS 203 Propazine LC-MS/MS 204 Propham LC-MS/MS 205 Propiconazole LC-MS/MS

(11)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

No.

Pesticide

Equipment Used

206 Propoxur LC-MS/MS 207 Propyzamide LC-MS/MS 208 Prosulfuron LC-MS/MS 209 Prothiopfos LC-MS/MS 210 Pyrazophos LC-MS/MS 211 Pyridaben LC-MS/MS 212 Pyridaphenthion LC-MS/MS 213 Pyrıdate LC-MS/MS 214 Pyriproxyfen LC-MS/MS 215 Quaizalofop_p_ethyl LC-MS/MS 216 Quinalphos LC-MS/MS 217 Qunomethionate GC-MSD 218 Quintozene GC-MSD 219 Resmethrin LC-MS/MS 220 Rimsulfuron LC-MS/MS 221 Simazine LC-MS/MS 222 Spiroxamine LC-MS/MS 223 Tau-fluvalinate GC-MSD 224 Tebuconazole LC-MS/MS 225 Tebufenozide LC-MS/MS 226 Tecnazene GC-MSD 227 Teflubenzuron LC-MS/MS 228 Terbuthylazine LC-MS/MS 229 Terbutryn LC-MS/MS 230 Tetradiphon GC-MSD 231 Tetrasul GC-MSD 232 Thiabendazole LC-MS/MS 233 Thiamethoxam LC-MS/MS 234 Thiodicarb LC-MS/MS 235 Thiophanate-methyl LC-MS/MS 236 Tolyfluanid GC-MSD 237 Tralkoxydim LC-MS/MS 238 Triadimefon LC-MS/MS 239 Triadimenol LC-MS/MS 240 Triallate (Tri-allate) LC-MS/MS 241 Triazophos LC-MS/MS 242 Tribenuron-methyl LC-MS/MS 243 Trichlorfon LC-MS/MS 244 Tridemorph LC-MS/MS 245 Trifloxystrobin LC-MS/MS 246 Triflumizole LC-MS/MS 247 Trifluralin GC-MSD

(12)

Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş TL-577

No.

Pesticide

Equipment Used

248 Triphenylphosphate LC-MS/MS

249 Vamidothion LC-MS/MS

250 Vinclozolin GC-MSD

251 α (alpha)- HCH GC-MSD

252 β (beta) - HCH GC-MSD

References

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