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Curie temperature determination via thermogravimetric and continuous wavelet transformation analysis

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Academic year: 2020

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Figure

Fig. 1 Modified schematic of Setsys DSC-TGA: 1 Electromagnetic Coil, 2 Platinum Pan, 3 Control Thermocouple, 4 Microbalance, 5 Heater, 6 Water Cooling, and 7 Heat Shield [15] (used with permission)
Fig. 2 The modified Setaram DSC/TGA with exposed column showing magnet and wires to Agilent power supply on the far right
Fig. 3 Left: Initial test on Fe sample proves concept but is full of systematic errors and has small effect size
Fig. 4 End to end process of wavelet transform method for Curie point detection. a: Tg (mg) signal vs time (seconds) and sample temperature profile (°C) from Setsys 15/18
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