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Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 1 of 12

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ZINUS INC.

461-469#, HUANZHU ROAD, JIMEI DISTRICT, XIAMEN, FUJIAN, CHINA

The following sample(s) was / were submitted and identified on behalf of the client as: Sample Description : 100% COTTON FIBER BARRIER

SGS Ref No. : CAN12-178308 & GZSL1212132419TX & GZSL1212130190TX

Buyer : KEETSA INC.

Manufacturer : ZINUS

Supplier : ZINUS

Country of Destination : USA

Testing Request : As requested by applicant, selected test(s) with reference to OEKO-TEX Standard 100 edition 04/2012

Sample Receiving Date : Dec.20, 2012

Test Performing Date : Dec.20, 2012 to Jan.05, 2013

Test Result(s) : For further details, please refer to the following page(s)

Signed for and on behalf of SGS-CSTC Co., Ltd.

Jack Yao

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Test Summary Result

Part A

To determine the pH Value in the submitted sample(s) with reference to Client’s

requirement. PASS

Determination of Free Formaldehyde content in the submitted sample(s) with

reference to Client’s requirement. PASS

To determine the Extractable Heavy Metals contents in the submitted sample(s)

with reference to Client’s requirement. PASS

Determination of Organostannic compounds contents in the submitted sample(s)

with reference to Client’s requirement. PASS

Determination of O-phenylphenol (OPP) content(s) in the submitted sample(s)

with reference to Client’s requirement. PASS

To determine Content(s) of PBBs&PBDEs in the selected parts on the submitted

sample(s) with reference to Client’s requirement. PASS To determine the Tris(2,3-Dibromopropyl) phosphate(TRIS) content in the

submitted sample(s) with reference to Client’s requirement. PASS To determine the Tris (aziridinyl) phosphineoxide (TEPA) content in the submitted

sample(s) with reference to Client’s requirement. PASS To determine the Chlorinated Organic Carriers content in the submitted sample(s)

with reference to Client’s requirement. PASS

Determination of Chlorinated Phenols ( TeCP, PCP) content(s) in the submitted

sample(s) with reference to Client’s requirement. PASS To determine the Tris(2 chloroethyl)phosphate (TCEP) content in the submitted

sample(s) with reference to Client’s requirement. PASS To determine Polynuclear Aromatic Hydrocarbons (PAHs) in the submitted

sample(s) with reference to Client’s requirement. PASS To determine the Short Chained Chlorinated Paraffins (SCCP) contents in the

submitted sample(s) with reference to Client’s requirement. PASS To determine the Nonylphenol (NP), Octylphenol (OP), Nonylphenol Ethoxylates

(NPEOs) and Octylphenol Ethoxylates (OPEOs) content(s) in the submitted sample(s) with reference to Client’s requirement.

PASS

To determine the Hexabromocyclododecane (HBCDD) content in the submitted

sample(s) with reference to Client’s requirement. PASS

Part B Determination of Smell Development (SNV 195651: 1968) PASS Part C Colour Fastness To Water (ISO 105 E01:2010) Colour Fastness To Perspiration (ISO 105 E04:2008) PASS PASS

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Part A (SGS Ref No.: CAN12-178308)

Test Results :

Test Part Description :

Specimen No. SGS Sample ID Description

1 CAN12-178308.001 Beige fabric sheet

Remarks :

(1) 1 mg/kg = 0.0001%

(2) MDL = Method Detection Limit (3) ND = Not Detected ( < MDL ) (4) "-" = Not Regulated

pH Value

Test Method : With reference to ISO 3071, test performed by pH meter

Test Item(s) Limit 001

pH value 4.0-9.0 5.3

Notes:

(1) The limit is quoted from client’s requirement

Formaldehyde

Test Method : With reference to JIS L 1041:2000 Section 6.3.1 (b) Method B, analysis was preformed by UV-Vis.

Test Item(s) Limit Unit MDL 001

Free Formaldehyde Content 300 mg/kg 20 ND

Notes:

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Extractable Heavy metal

Test Method : With reference to ISO 105-E04:2008, analysis was performed by ICP-MS and UV-VIS.

Test Item(s) Limit Unit MDL 001

Arsenic (As) 1 mg/kg 0.1 ND Antimony (Sb) 30 mg/kg 1.0 ND Cadmium (Cd) 0.1 mg/kg 0.05 ND Chromium (Cr) 2 mg/kg 0.5 ND Lead (Pb) 1.0 mg/kg 0.1 ND Mercury (Hg) 0.02 mg/kg 0.01 ND Copper (Cu) 50.0 mg/kg 5.0 ND Nickel (Ni) 4 mg/kg 0.5 ND Cobalt (Co) 4 mg/kg 0.5 ND Chromium VI (Cr VI) ND mg/kg 0.5 ND Notes:

(1) The limit is quoted from client’s requirement

Organic-tin compounds

Test Method : With reference to ISO 17353: 2004 with carbamate, analysis was performed by GC-MS.

Test Item(s) Limit Unit MDL 001

Dibutyl tin (DBT) 2 mg/kg 0.02 ND

Tributyl tin (TBT) 1 mg/kg 0.02 ND

Dioctyl tin (DOT) 2 mg/kg 0.02 ND

Triphenyl tin (TPhT) 1 mg/kg 0.02 ND

Notes:

(1) The limit is quoted from client’s requirement

OPP

Test Method : SGS in house method (GZTC CHEM-TOP-055-01), analysis was performed by GC-MS.

Test Item(s) CAS_NO Limit Unit MDL 001

O-phenylphenol (OPP) 90-43-7 100 mg/kg 0.5 ND

Notes:

(1) The limit is quoted from client’s requirement

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PBBs/PBDEs

Test Method : With reference to US EPA 3550C:2007 for PBBs / PBDEs content, analysis was performed by GC-MS.

Test Item(s) Limit Unit MDL 001

Monobromobiphenyl ND mg/kg 5 ND Dibromobiphenyl ND mg/kg 5 ND Tribromobiphenyl ND mg/kg 5 ND Tetrabromobiphenyl ND mg/kg 5 ND Pentabromobiphenyl ND mg/kg 5 ND Hexabromobiphenyl ND mg/kg 5 ND Heptabromobiphenyl ND mg/kg 5 ND Octabromobiphenyl ND mg/kg 5 ND Nonabromobiphenyl ND mg/kg 5 ND Decabromobiphenyl ND mg/kg 5 ND Pentabromodiphenyl ether ND mg/kg 5 ND Octabromodiphenyl ether ND mg/kg 5 ND Decabromodiphenyl ether ND mg/kg 5 ND Notes:

(1) The limit is quoted from client’s requirement

TRIS(Tris(2,3-Dibromopropyl)-phosphate)

Test Method : With reference to EPA 3550C:2007 . Analysis was performed by LC-MS.

Test Item(s) CAS_NO Limit Unit MDL 001

Tris(2,3-Dibromopropyl) 126-72-7 ND mg/kg 5 ND -phosphate

Notes:

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Tris-(aziridinyl) phosphineoxide (TEPA)

Test Method : With reference to US EPA 3550C:2007, Analysis was performed by GC-NPD or GC-MS.

Test Item(s) Limit Unit MDL 001

Tris-(aziridinyl) phosphineoxide (TEPA) ND mg/kg 5 ND

Notes:

(1) The limit is quoted from client’s requirement

Chlorinated Organic Carriers

Test Method : With reference to DIN 54232:2007, analysis was conducted with GC-MS.

Test Item(s) Limit Unit MDL 001

Sum of chlorinated organic carriers 1 mg/kg 0.1 ND

2-Chlorotoluene - mg/kg 0.1 ND 3-Chlorotoluene - mg/kg 0.1 ND 4-Chlorotoluene - mg/kg 0.1 ND 1,3-Dichlorobenzene - mg/kg 0.1 ND 1,4-Dichlorobenzene - mg/kg 0.1 ND 1,2-Dichlorobenzene - mg/kg 0.1 ND 2,4-Dichlorotoluene - mg/kg 0.1 ND 2,5-Dichlorotoluene - mg/kg 0.1 ND 2,6-Dichlorotoluene - mg/kg 0.1 ND 1,3,5-Trichlorobenzene - mg/kg 0.1 ND 1,2,4-Trichlorobenzene - mg/kg 0.1 ND 1,2,3-Trichlorobenzene - mg/kg 0.1 ND 2,4,5-Trichlorotoluene - mg/kg 0.1 ND 2,3,6-Trichlorotoluene - mg/kg 0.1 ND 1,2,3,5-Tetrachlorobenzene - mg/kg 0.1 ND 1,2,4,5-Tetrachlorobenzene - mg/kg 0.1 ND 1,2,3,4-Tetrachlorobenzene - mg/kg 0.1 ND α,α,α,4-Tetrachlorotoluene - mg/kg 0.1 ND Pentachlorobenzene - mg/kg 0.1 ND Pentachlorotoluene - mg/kg 0.1 ND Hexachlorobenzene - mg/kg 0.1 ND Notes:

(1) The limit is quoted from client’s requirement

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Chlorinated Phenols

Test Method : With reference to LFGB § 64 BVL B 82.02.08:2001, analysis was performed by GC-ECD or GC-MS .

Test Item(s) Limit Unit MDL 001

2,3,4,5-Tetrachlorophenol (2,3,4,5-TeCP) - mg/kg 0.05 ND 2,3,5,6-Tetrachlorophenol (2,3,5,6-TeCP) - mg/kg 0.05 ND 2,3,4,6-Tetrachlorophenol (2,3,4,6-TeCP) - mg/kg 0.05 ND Tetrachlorophenol (TeCP) 0.5 mg/kg - ND Pentachlorophenol (PCP) 0.5 mg/kg 0.05 ND Notes:

(1) The limit is quoted from client’s requirement

Tris(2-chloroethyl)phosphate (TCEP)

Test Method : With reference to EPA 3550C :2007.Analysis was performed by HPLC-MS.

Test Item(s) CAS_NO Limit Unit MDL 001

Tris(2-chloroethyl) phosphate 115-96-8 ND mg/kg 5 ND (TCEP)

Notes:

(1) The limit is quoted from client’s requirement

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PAHs

Test Method : With reference to ZEK 01.4-08 of German ZLS and its amendments, analysis was performed by GC-MS.

Test Item(s) Limit Unit MDL 001

Naphthalene(NAP) - mg/kg 0.2 ND Acenaphthylene(ANY) - mg/kg 0.2 ND Acenaphthene(ANA) - mg/kg 0.2 ND Fluorene(FLU) - mg/kg 0.2 ND Phenanthrene(PHE) - mg/kg 0.2 ND Anthracene(ANT) - mg/kg 0.2 ND Fluoranthene(FLT) - mg/kg 0.2 ND Pyrene(PYR) - mg/kg 0.2 ND Benzo(a)anthracene(BaA) - mg/kg 0.2 ND Chrysene(CHR) - mg/kg 0.2 ND Benzo(b)fluoranthene(BbF) + - mg/kg 0.4 ND Benzo(j)fluoranthene(BjF) Benzo(k)fluoranthene(BkF) - mg/kg 0.2 ND Benzo(e)pyrene(BeP) - mg/kg 0.2 ND Benzo(a)pyrene(BaP) 1 mg/kg 0.2 ND Indeno(1,2,3-c,d)pyrene(IPY) - mg/kg 0.2 ND Dibenzo(a,h)anthracene(DBA) - mg/kg 0.2 ND Benzo(g,h,i)perylene(BPE) - mg/kg 0.2 ND Sum of 18 PAHs 10 mg/kg - ND To be continued…

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Notes:

(1) The limit is quoted from client’s requirement

Short Chained Chlorinated Paraffin (SCCP)

Test Method : With reference to US EPA 3550C: 2007, analysis was performed by GC-ECD.

Test Item(s) Limit Unit MDL 001

Short Chained Chlorinated Paraffin (SCCP) ND mg/kg 50 ND

Notes:

(1) The limit is quoted from client’s requirement

Nonylphenol (NP), Octylphenol (OP), Nonylphenol Ethoxylates (NPEOs) and Octylphenol Ethoxylates (OPEOs)

Test Method : With reference to US EPA Method 3550C:2007, analysis was performed by LC-MS.

Test Item(s) Limit Unit MDL 001

Nonylphenol ethoxylates (NPEOs) 1000 mg/kg 10 ND Octylphenol ethoxylates (OPEOs) 1000 mg/kg 10 ND

Nonylphenol(NP) 100 mg/kg 10 ND

Octyphenol(OP) 100 mg/kg 10 ND

Notes:

(1) The limit is quoted from client’s requirement

Hexabromocyclododecane (HBCDD)

Test Method : With reference to US EPA 3550C: 2007, analysis was performed by GC-MS.

Test Item(s) Limit Unit MDL 001

Hexabromocyclododecane (HBCDD) ND mg/kg 5 ND

Notes:

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Photo Appendix

Part B (SGS Ref No.: GZSL1212132419TX) Test Result:

Determination of Smell Development Of Shoes (SNV 195651: 1968)

Test Procedure: The samples was kept in a hermetically closed space with 37°C±1°C for a duration of 15 hours, in this status the smell independently judge by at least 3 persons and described by possibility of its type.

The judgement 1

End Result Weak odour

Sample blank

End Result Odourless

Photo Appendix

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Part C (SGS Ref No.: GZSL1212130190TX) Test Result:

Requirement

Colour Fastness To Water (ISO 105 E01:2010)

Change in shade 4-5 Min 3

Staining on multi-fiber stripe Min 3 Acetate 4-5 Cotton 4-5 Nylon 4-5 Polyester 4-5 Acrylic 4-5 Wool 4-5

Colour Fastness To Perspiration (ISO 105 E04:2008)

Acidic

Change in shade 4-5 Min 3-4

Staining on multi-fiber stripe Min 3-4 Acetate 4-5 Cotton 4-5 Nylon 4-5 Polyester 4-5 Acrylic 4-5 Wool 4-5 Alkaline

Change in shade 4-5 Min 3-4

Staining on multi-fiber stripe Min 3-4 Acetate 4-5 Cotton 4-5 Nylon 4-5 Polyester 4-5 Acrylic 4-5 Wool 4-5

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Photo Appendix

Remark: This test was conducted at 198 Kezhu Road, Scientech Park Guangzhou Economic & Technology Development District, Guangdong Province, China.

References

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