A New Method of Construction of Robust Second Order
Rotatable Designs Using Balanced Incomplete Block
Designs
Bejjam Re. Victorbabu, Kottapalli Rajyalakshmi
Department of Statistics, Acharya Nagarjuna University, Guntur, India Email: [email protected]
Received December 8,2011; revised December 30, 2011; accepted January 12, 2012
ABSTRACT
Das [1,2] studied robust second order rotatable designs (RSORD) and constructed second order rotatable designs with correlated errors (SORDWCE) under the auto correlated structure using central composite design. In this paper, a new method of construction of RSORD using balanced incomplete block designs (BIBD) is suggested. In this method the number of design points required is in some cases less than the number required in Das [1,2] method of construction of robust rotatable central composite designs (RRCCD). We may point out here that this RSORD using BIBD has 113 design points for 7-factors where as the corresponding RRCCD obtained by Rajyalakshmi and Victorbabu [3] needs 157 design points. Thus the new method leads to a 7-factor RSORD in less number of design points than the corre-sponding RRCCD. Here we also obtained the variance of the estimated response for the factors 3 ≤v≤ 8.
Keywords: Response Surface Designs; Rotatability; Second Order Rotatable Designs (SORD); Robust SORD;
Robustness; Balanced Incomplete Block Designs
1. Introduction
In response surface methodology, rotatability is a natural and highly desirable property. This was introduced and developed by Box and Hunter [4], assuming the errors to be uncorrelated and homoscedastic. Das and Narasim- ham [5], constructed second order rotatable designs (SORD) through balanced incomplete block designs (BIBD). Pan- da and Das [6] studied first order rotatable designs with correlated errors. Further, Rajyalakshmi and Victorbabu [3] extended the work of Das [1,2] and constructed RRCCD for 3 ≤v≤ 17.
In order to study the nature of robust rotatable designs, rotatability conditions for second order regression de- signs have been derived, assuming the errors to be corre- lated. These conditions have been further studied under different variance covariance structures of errors. Here we derive conditions for rotatability for a general corre- lated errors structure and specialize then to the auto- correlated structure.
In this paper, a new method of construction of RSORD using BIBD is suggested and also obtained the variance of the estimated response for factors 3 ≤v≤ 8.
2. Conditions of SORDWCE
Assuming that the response surface is of second order, we adopt the model:
1 0
1
v v
u i iu ij iu ju u
i
i j
y x x x e
2 0
1 1 1
ˆ ˆ v ˆ v ˆ v ˆ
(1) where Y is the vector of recorded observations on the study variable y,β’s are the vector of regression coeffi-cients, euare random errors with correlated errors.
2.1. Conditions of Rotatability The estimated response at x is given by
x ii i i i ij i j
i i i j
x x x x
y
ˆ
(2) The variance of estimated response at yx
is given by
4 2 2 2 2
0 0 0
1 1 1 1 1
3 2 2 2
1 1 1 1
ˆ ˆ 2 ( ,ˆ ˆ ) 2 ˆ ,ˆ ˆ 2 ˆ ˆ,
ˆ ˆ ˆ ˆ ˆ ˆ ˆ
2 , 2 , , 2
ˆ
2
v v v v v
x i ii i ii i j ii jj i i i i
i i i j i i
v v v v
i j i j i i ii i j ii j i j ij
i j i i j i j
V V x V x Cov x x Cov x V x Cov
x x Cov x Cov x x C v x x V
y
o
0 1
2
1 1 1 1 1 , ,
ˆ ˆ,
ˆ ˆ ˆ ˆ ˆ ˆ
2 , 2 , 2 ,
v
i j ij
i j v
s i j ss ij s i j s ij i j l t ij lt
s i j s i j i j l t i j l t
x x Cov
x x x Cov x x x Cov x x x x Cov
0. 1 2 . 1 v i i v ii j i j i j x v
x x v
. . 1 1 v
00 4 . 2 0.1 1
2 2 . 2 .
1 1
. 3 .
1 1
2 2 . 0.
1 1 2 1 1 2 2 2 2 2 2 2 ˆ 2 v v
ii ii ii
x i i
i i
v v
ii jj i i
i j i
i j i i
v v
i j i ii
i j i
i j i
v v
ij ij ij
i j i j
i j i j
v
s i j
s i j
V v x v x v
x x v x v
x x v x v
x x v x
x y x v x x
. 1 , ,2 2 ss ij s i v ij lt
i j l t
i j l t i j l t
x x x x v
s ijs i j
j
v x x x v
(4) The variance function in (3) will b tion of 2
1
v
i i e a func x
for rotatability for all x if v0.iv0.ij vi.j 0; 1 ≤i≠j≤
v; vii j. 0; 1≤i, j≤ v; vs ij. vss ij. 0; 1 ≤ s, i < j≤ v;
. 0
ij lt
v ; 1 0.ii constant
1 a
, say; 1≤ i ≤ v;
.ij constant ≤i, l < j, t≤v, (i, j)
≤ i ≤ v; vi i. = const
1
tant
v d , say; 1 ≤ i
≤i < j≤v; and
≠ (l, t); v ant = e
≠ j ≤ v; vij
, say; 1
cons
, say; 1
.
ii jj
c
ii ii.
1
2
c v constant d ; 1
≤
ability designs with corre
del (1 elements of th
.
i j
(iii) (1) v 0 .
i jl < l≤v
≤i v.
Below are given equivalent conditions for rotat in second order regression lated errors mo ) in terms of the e moment matrix:
0.j 0.jl 0
v v ; 1 ≤j < l ≤v ii) v 0; 1 ≤i≠j ≤v
; 1 ≤i, j≤v (I): (i)
(
.
ii j
(2) v 0; 1 ≤i, j (3) vii jl.. 0; 1 ≤i, j < l≤v
(4) vij lt. 0; 1 ≤i, l< j, t≤v, (i, j) ≠ (l, t) (II): (i) v0.jj constanta0, say; 1 ≤j≤v
(ii) vi i. constant e, sa 1
y; 1 ≤i≤v
(iii) vii.iiconstant 2 f c
, say; 1 ≤i≤v (III): (i) vii.jj constant f ; 1 ≤i≠j≤v
(ii) . ta
1 nt ij
v cons ; 1 ≤i < j≤v c
. ij ij. vii jj. ; 1 ≤i < j≤ v (5) e Function of SORDWCE
The estimated response at x is given by
2 0
1 1 1
ˆ ˆ ˆ ˆ
ˆ v v v
ij
(IV): vii ii 2v 2.2. Varianc
x i i ii i ij i j
i i i j
x x
y x x
(6)The variance function of a SORDWCE is given by
2 0 0 14 2 2
1 1
2 2 2
1 1
00
1 1
ˆ 2 ( ,ˆ ˆ )
ˆ 2 ˆ , ˆ
ˆ ˆ
2
ˆx v i ii
i
v v
i ii i j ii jj
i i j
v v
i i i
i i j
V V x Cov
x V x x Cov
x V x x V
v d
y
a e d
2 4
2 (c d )
j ij
(7) 2 1whi a function of i d
When the erro
reduce respectively to the usual second order rotatability iance
func-2.3. Conditions for Exact Rotatability Following (4), necessary and sufficient conditio se
it is si
0. 11 2
I * i j N ju N ju 0, 1 ;
u u
v x x j v
1 0.
1 2
0, 1 ;
N N
jl ju lu ju lu
u u
v x x x x j l v
2
ch is
vxiNote: rs are homoscedastic, (5) and (7)
conditions, non-singularity condition and var tion.
ns for cond order rotatability under auto-correlated structure,
mplifies to
1 2 . 1 2 1 1 1 1 1 1 ii0, 1 ;
N N
i j iu ju iu ju
u u
N N
iu j u i u ju
u u
v x x x x
x x x x i j v
1 1 1 iu j u 1 i u ju
u u
2 2 1 2.
1 2
1 1
2 2
iii 1
0, 1 , ;
N N
ii j iu ju iu ju
u u
N N
v x x x x
x x x x i j v
1 1 1
1 , ;
ju l u i u j u lu
i j l v
2 v Nx x x 2N1x x x .1 2
1 1
1 1
0,
ij l iu ju lu iu ju lu
u u
N N
iu
u u
x x x x x x
12 2 2
. 1 2 1 1 2 2 ( 1) 1 1 1 1 3 0, 1 , N N
ii jl iu ju lu iu ju lu
u u
N N
iu j u l u i u ju lu
u u
v x x x x x x
x x x x x x
1 2 . 1 2 1 11 1 1
1 1
4
1 , ,
N N
ij lt iu ju lu tu iu ju lu
u u
N N
iu ju l u t u i u j u
u u
v x x x x x x x
x x x x x x
i l j t
1 0,tu lu tu x x x 1 2 2 1 2 N N
2
2
1
0.
0
II * i 1 1
;1 ;
jj ju ju
u u x
v xa j v
. 12 2 2 2 2
1 1
1 1
1 1
1 2
1,1 ;
i i
N N N
iu iu iu i u
u u u
x x x x
i v e
ii v
. 1 1 2 2 1 1 iii 2 ii ii Niu i u u v x x
12 2 4 2 4
1 2
1
2 , 1 ;
N N
iu iu
u u
x x
d i v
c
1 2 2 1 12 2 2 2 2 2 2
1 2 1
1
(
, 1 ;
N N N
iu ju iu ju iu j u
u u u
.
1
2 2
1 1
1 III * i ii jj
N
ju i u u
v
x x x x x x
d i j v
x x
. 1ii vij ij
2 2
1 1
2 2 2 2 2
1 1
1 2 1
1
2
1, 1 ;
N N N
iu ju iu ju iu ju i u j u
u u u
x x x x x x x x
i j v c
IV *vii ii. 2vij ij. vii jj. ,1 i j v; (8)are as in (II)*(iii) and (III)*(i), ularity is given by,
(V)* :
where vii ii. ,vii jj. andvij ij. (ii).
The condition for non-sing 2 0 00
2 a 0
v f
c v
(9)
where N 2 2 1
00
v N and 0 1, ,f a c are as in (6).
ility, as stipu-nce ρ is
un-known unless special efforts are made regarding choice of the underlying robust design. Towards this, tremen-dous simplification obtains whenever all odd moments of various types vanish. These are listed below for ready re ference,
1 1
1 2 1 2
, ,1 ; , ,
N N N N
Note: The conditions fo lated above, are hard to satis
r exact rotatab fy in practice si
-
ju ju iu ju iu ju
u u u u
x x j v x x x x
1 1 1 1 1 1, ,1 ;
N N
iu j u i u ju
u u
x x x x i j v
1 12 2 2
1
1 2 1
, , ,
N N N
iu ju iu ju iu j u
u u u
x x x x x x
1 2 1 1 1;1 , ; ,
N N
ju iu ju lu
i u
u u
x x i j v x x x
1 1 1
, , ,
, ;
N N N
ju lu iu ju l
u 1 1 1
2 1 1
1
iu u i u j u lu
u u
x x x x x x x x x
i j l v
2 2 2
2 1
, iu ju lu, iu
u u u
x x x x x x x x x
1 2
1 ,1 , ;
N ju lu i u
1 ( 1)
1 iu ju lu j u l u
1 1
N N N
x
1
u
x x i j l v
1 , ,1 tu 2 iu ju lu tu
u u
N N
iu ju lu x x x x
x x x x 1 1 1 1 , N
iu ju l u t u u
x x x x
1 1 1 1;1 , , . N
lu tu i u j u u
x x x x i l j t v
(10) As to the even order moments (up to order 4) mere constancy of such moments (of various ty s) suffices to ensure exact rotatability. Specially, we sire to have each of the following terms independent of i and j:2 2 1 ,1 ; N iu u pe de
x constant N v
i
4 4 13 ,1 ;
N
iu u
x constant N i v
2 2 4 1 ,1 ; N iu ju ux x constant N i j v
Using the above relations, for the newly nstructed design, we get the following:
1 2 2 1 ,1 N iu u co
x constant N i v
1 4 4 13 ,1 ;
N
iu u
x constant N i v
2 2
4 1
N
iu ju u
,1 x x constant N
i j v (11)Thus, a design satisfying the conditions mentioned above may be successfully uti table design under violation of the homoscedasticity assumption sub-ject to the covariance structure being of the type (condi-tions of exact rotatability). Such a design is, therefore, robust, N, N1, 4
lized as a rota
where c, ,2 are constants.
3. New Method of Construction of RSORD
ts by incorporating (n + 1) central points in the foll wing way.
One central point is placed in between each pair of non- central design points in the sequence, resulting thereby in (n – 1) such central points. The other two central points are placed one at the beginning and one at the end.
If the number of central points of the usual SORD with which we started is greater than (n + 1), the remaining central points are placed in any manner, if the number is le
examine the non-singularity for the original design and the newly constructed design.
Let N be the number of design points of he original design (SORD) with which we started. Out of N, let n be the number of non-central design points an m be the number of central points i.e., N = n + m. In general m < n + 1, Let N1 be the number of design points of the newly constructed design, Where N1 = 2n + 1 > N.
original design with which we started, the follo th
Using Balanced Incomplete Block Design
Here we start with usual SORD using BIBD having “n” non-central design points involving v-factors. The set of n design points can be extended to (2n + 1) poin
o
ss, we need to include the requisite number of addi- tional central points. Here we
t d
For the wing are e moment relations:
Let (v, b, r, k, λ) denote a BIBD. 2t k denote a
frac-tional replicate of 2k in ±1 levels, in which no interaction
with less than five factors is confounded and m be the number of central points in the design.
The design points for the newly constructed design are obtained as follows:
3.1. Method I: When r < 3λ
( )
t k
Here, N b 2 2v m n m and N1 = 2n + 1, where ( )
2t k 2 n b v.
From the design points generated from the BIBD, simple symmetry conditions (10) and (11) are true. Con-ditions (10) are true obviously. ConCon-ditions (11) are true as follows:
2 2
2 1
2 2 ,
N
t k iu u
x r N
4 4
4
2 2 3 ,
N
t k iu
x r N
1
u
2 2
4 1
2 ,
N
t k iu ju u
x x N
Using the above relations, for the newly constructed design, we get the following:
1
2 2
2 1
2 2 ,
N
t k iu u
x r N
1
4 4
4 1
2 2 3 ,
N
t k iu u
x r N
1 2 2
N
t k
4 1
2
iu ju
u
x x N
(12) The results are given in Table 1.
3.2. Method II: When r = 3λ
Here, N b2t k( )m ( )
t k = n + m and N1 =2n + 1, where n=
2 b .
ted from the BIBD sim-metry conditions (10) a
0) are t obviously. C fo
From the design points genera
ple sym nd (11) are true. Condi-tions (1 rue onditions (11) are true as
llows:
2
2 1
2 ,
N
t k iu u
x r N
4
4 1
2 3 ,
N
t k iu u
x r N
2 2
4 1
2 ,
N
t k iu ju u
x x N
Using the above relations, for the newly constructed design, we get the following:
1 2
N
t k
2 1
2 ,
iu u
x r N
1
N
4
4 1
2t k 3 ,
iu u
x r N
1 2 2
4 1
2
N
t k
iu ju
u
x x N
(13) The results are given in Table 2.3.3. Method III: When r > 3λ Here, N b2t k( )2t v( )m = n +
( ) ( )
t k t v m and N1 = 2n + 1,
Where n = 2b 2
ed from the BIBD sim-metry condit
0) are true ob fo
From the design points generat
ple sym ions (10) and (11) are true. Condi-tions (1 viously. Conditions (11) are true as
llows:
2 ( ) 2
2 1
2 2 ,
N
t k t v iu
u
x r N
Table 1. Variance of the estimated response for the factors3 ≤v ≤8, when r < 3λ.
ˆ
V y
2, 2, 1
r k
ˆ
V y
,r
(v 4,b 4
ρ (v3,b3,
N1 = 37, N
= 24, n = 18, m = 6
) 3,k 3, 2
N1 = 81, N
= 48,
ˆ
V y
,r 4,k 4, 3
)
n = 40, m = 8
(v5,b5
N = 100,
)
n = 90, m = 10
1 = 181, N
–1 0 0 0
–0.9 0.0550σ2 – 0.1092σ2d2 + 0.0747σ2d4 0.0938σ2 – 0.117 4σd 0.0093 2 2 2 4
–0.8 0.0825σ2 – 0.1562σ2d2 + 0.1164σ2d4 0.0810σ2 – 0.0 5σ2d4 .0
–0.7 0.0862σ2 – 0.1496σ2d2 + 0.1294σ2d σ2 – 0.065
0.0
+ 0.1280σd 0.0388σ – 0.0
–0.4 0.0640σ2 – 0.0503σ2d2 + 0.0126σ2d4
0.0328σ2 – 0.0 286σ2d4
0.0131σ2 – 0.0007σ2d2 + 0.0084σ2d4
–0.3 0.0582σ2 – 0.0206σ2d2 + 0.1242σ 4
0.0287σ2 – 0.0017σ2d2 + 0.0289σ2d4
0.0120σ2 + 0.0024σ2d2 + 0.0090σ2d4
–0.2 0.0542σ2 + 0.0040σ2d2 + 0.1228σ2d4
0.0262σ2 + 0.0065σ2d2 + 0.0292σ2d4
0.0112σ2 + 0.0050σ2d2 + 0.0094σ2d4
–0.1 0.0520σ2 + 0.0230σ2d2 + 0.1200σ2 0.0247σ2 + 0.0126σ2d2 + 0.0292σ2d4 0.0108σ2 + 0.0070σ2d2 + 0.0096σ2d4
0 0.0515σ2 + 0.0365σ2d2 + 0.1152σ2d4
0.0243σ2 + 0.0167σ2d2 + 0.0286σ2d4
0.0107σ2 + 0.0082σ2d2 + 0.0095σ2d4
0.1 0.0529σ2 + 088σ2d2 + 0.009σ2d4
0.2 0.0562σ2 + 0.0478σ2 + 0.0986σ2d4
0.0263σ2 + 0.0194σ2 + 0.0251σ2d4 0.0117σ2 + 0.0087σ2 + 0.0085σ2d4
σ2 + 0.0469σ2d2 + 0.0872 4
0.0290σ2 + 0.0186σ2d2 + 0.0224 4
0.0130σ2 + 0.0082σ2d2 + 0.0076 4
0.4 0.0 4
0. d4
0
σ2 + 0.0371 2d2 + 0.0610σ2d4 0.0400σ2 d2 + 0.0158σ2d4 0.0181σ2 + 0.0062 2d2 + 0.0054σ2d4
1σd + 0.041 σ – 0.0071σd + 0.0029σd
960σ2d2 + 0.038 0 150σ2 – 0.0107σ2d2 + 0.0050σ2d4
7
2 2 2 4 2
4 0.0614 σ2d2 + 0.0329σ2d4 0.0167σ2 – 0.0103σ2d2 + 0.0063σ2d4
428σ2d2 + 0.0298σ2d4 0.0160σ2 – 0.0076σ2d2 + 0.0071σ2d4
256σ2d2 + 0.0287σ2d4
0.0145σ2 – 0.0041σ2d2 + 0.0078σ2d4
122σ2d2 + 0.0
–0.6 0.0799σ2 – 0.1196σ2d2 + 0.1302σ2d4 0.0478σ2 –
–0.5 0.0715σ2 – 0.0841σ2d2 2 4 2
2d
d4
0.0446σ2d2 + 0.1080σ2d4
0.0248σ2 + 0.0189σ2d2 + 0.0272σ2d4 0.0110σ2 + 0.0
d2 d2 d2
0.3 0.0620 σ2d σ2d σ2d
710σ2 + 0.0430σ2d2 + 0.0744σ2d 0334σ2 + 0.0167σ2d2 + 0.0192σ2 .0150σ2 + 0.0073σ2d2 + 0.0065σ2d4
0.5 0.0846 σ
σ2 + 0.0300σ2d2 + 0.0475σ2d4
+ 0.0142
0.0504σ2 σ2d2 + 0.0124σ2d4
σ2 σ
0.6 0.1055
0.1396σ2 + 0.0225σ2d2 + 0.0344σ2d4
+ 0.0114
0.06801σ2 + 0.0084σ2d2 + 0.0090σ2d4
0.0230σ2 + 0.0049σ2d2 + 0.0042σ2d4
0.7 0.0314σ2 + 0.0036σ2d2 + 0.0031σ2d4
0.8 0.2019σ2 + 0.0149σ2d2 + 0.0220σ2d4
0.1022σ2 + 0.0055σ2d2 + 0.0057σ2d4
0.0482σ2 + 0.0023σ2d2 + 0.0020σ2d4
0.9 0.3461σ2 + 0.0076σ2d2 + 0.0105σ2d4
0.1924σ2 + 0.0027σ2d2 + 0.0027σ2d4
0.0957σ2 + 0.0011σ2d2 + 0.0009σ2d4
1 0 0 0
ρ
ˆ
V y
(v6,b10,r5,k3,2)
N1 = 185, N = 104, n = 92, m = 12
ˆ
V y
(v7,b7,r4,k4,2)
N1 = 253, N = 140, n = 126, m = 14
ˆ
V y
(v8,b14,r7,k4,3)
N1 = 482, N = 257, n = 240, m = 17
–1 –0.9 0.0177
0
2 2 2 2 4
0
2 2 2 2 4
0
2 2 2 2 4
σ – 0.0218σd + 0.0112σd
0.0234σ2 – 0.0268σ2d2 + 0.0168σ2d4
0.0687σ – 0.0670σd + 0.0185σd
0.0347σ2 – 0.0312σ2d2 + 0.0115σ2d4
0.0210σ – 0.0201σd + 0.0062σd
0.0157σ2 – 0.0136σ2d2 + 0.0059σ2d4
–
σ2 + 0.016 2d2 + 0.0258σ2d4
0.0085σ2 + 0.010 2d2 + 0.0130σ2d4
0.0045σ2 + 0.006 2d2 + 0.0088σ2d4
0.3 0.0128σ2 + 0.0150σ2d2 + 0.0231σ2d4
0.0094σ2 + 0.0095σd2 + 0.0117σ2d4
0.0050σ2 + 0.0058σ2d2 + 0.0079σ2d4
σ2 + 0.0133σ2d + 0.0200σ2 4
0.0108σ2 + 0.0084σ2d + 0.0101σ2d4
0.0057σ2 + 0.0051σ2d + 0.0068σ2 4
0.5 0
0.0226σ + 0.008 d + 0.0129σd 0.0166σ + 0.005 d + 0.0065σd 0.0088σ + 0.003 d + 0.0044σd
1 0 0 0
0.8
–0.7 0.0218σ2 – 0.0213σ2d2 + 0.0191σ2d4
0.0226σ2 – 0.0172σ2d2 + 0.0101σ2d4
0.0112σ2 – 0.0080σ2d2 + 0.0058σ2d4
–0.6 0.0188σ2 – 0.0135σ2d2 + 0.0207σ2d4
0.0166σ2 – 0.0091σ2d2 + 0.0102σ2d4
0.0084σ2 – 0.0040σ2d2 + 0.0063σ2d4
–0.5 0.0159σ2 – 0.0061σ2d2 + 0.0226σ2d4
0.0130σ2 – 0.0034σ2d2 + 0.0110σ2d4
0.0067σ2 – 0.0011σ2d2 + 0.0070σ2d4
–0.4 0.0138σ2 + 0.0004σ2d2 + 0.0245σ2d4
0.0108σ2 + 0.0009σ2d2 + 0.0120σ2d4
0.0056σ2 + 0.0013σ2d2 + 0.0078σ2d4
–0.3 0.0123σ2 + 0.0059σ2d2 + 0.0263σ2d4
0.0094σ2 + 0.0043σ2d2 + 0.0130σ2d4
0.0049σ2 + 0.0031σ2d2 + 0.0086σ2d4
–0.2 0.0113σ2 + 0.0102σ2d2 + 0.0278σ2d4
0.0085σ2 + 0.0069σ2d2 + 0.0138σ2d4
0.0045σ2 + 0.0046σ2d2 + 0.0092σ2d4
–0.1 0.0108σ2 + 0.0134σ2d2 + 0.0286σ2d4
0.0080σ2 + 0.0088σ2d2 + 0.0143σ2d4
0.0042σ2 + 0.0056σ2d2 + 0.0096σ2d4
0 0.0106σ2 + 0.0154σ2d2 + 0.0286σ2d4
0.0079σ2 + 0.0100σ2d2 + 0.0144σ2d4
0.0041σ2 + 0.0063σ2d2 + 0.0096σ2d4
0.1 0.0109σ2 + 0.0163σ2d2 + 0.0276σ2d4
0.0080σ2 + 0.0104σ2d2 + 0.0139σ2d4
0.0042σ2 + 0.0065σ2d2 + 0.0094σ2d4
0.2 0.0116 1σ 2σ
2
3σ
0.4 0.0148 2 d
2
2 2 d
2
.0178σ2 + 0.0112σ2d2 + 0.0165σd4
2 2 2 2 4
0.0131σ2 + 0.0070σ2d2 + 0.0084σd4
2 2 2 2 4
2 0.0069σ2 + 0.0043σ2d2 + 0.0056σd4
2 2 2 2 4
0.6 9σ 6σ 4σ
0.7 0.0308σ2 + 0.0065σ2d2 + 0.0094σ2d4
0.0227σ2 + 0.0041σ2d2 + 0.0048σ2d4
0.0120σ2 + 0.0025σ2d2 + 0.0032σ2d4
0.8 0.0472σ2 + 0.0042σ2d2 + 0.0060σ2d4
0.0349σ2 + 0.0026σ2d2 + 0.0031σ2d4
0.0186σ2 + 0.0016σ2d2 + 0.0021σ2d4
0.9 0.0938σ2 + 0.0020σ2d2 + 0.0029σ2d4
0.0703σ2 + 0.0013σ2d2 + 0.0015σ2d4
0.0381σ2 + 0.0008σ2d2 + 0.0010σ2d4
Table 2. Variance of the estim v ≤8 ,
2, 1
ated response for the factors3 ≤ when r = 3λ.
ρ
ˆ
V y
(v4,b6,r3,k
25, m =
)
N1 = 51, N = 27, n = 2
ˆ
V y
(v7,b7,r3,k3,1)
N1 = 113, N = 57, n = 56, m = 1
–1 0 0
–0.9 + 0.0350 σ2 –
.8 + 0.0632 σ2 –
+ 0.0815 σ2 – 0.050
.6 + 0.0928 0365σ2 –
.5 + 0.1004 289σ2 –
.4 + 0.1065 241σ2 +
.3 + 0.1113 209σ2 +
.2 + 0.1145 190σ2 +
.1 + 0.1155 σ2 +
+ 0.1135 σ2 +
2 2 2 2 4 2 2 2 .0 σ2d4
0.2 1σ2d4
0.3 0.0452σ2 + 0.0492σ2 + 0.0893σ2d4
0.0209σ2 + 0.0285σ2 + 0.0468σ2d4
0.4 0.052 2 2 2 4
0.0241 2 2 2 4
0.0622σ + 0.037 d + 0.0631σd4
0.0289σ + 0.021 d + 0.0335σd4
0.0242σ2 – 0.0390σ2d2 σ2d4
0.1400 0.1820σ2d2 + 0.0677σ2d4
–0 0.0413σ2 – 0.0630σ2d2 σ2d4
0.0745 0.0890σ2d2 + 0.0445σ2d4
–0.7 0.0487σ – 0.0660σd
2 2 2
2 2 2 σd
0.0494
2 4
2 4 0σd + 0.0396σd
2 2 2 4
2 2 2 4
–0 0.0493σ – 0.0540σd σd 0. 0.0260σd + 0.0405σd
–0 0.0468σ2 – 0.0340σ2d2 σ2d4
0.0 0.0100σ2d2 + 0.0437σ2d4
–0 0.0434σ2 – 0.0130σ2d2 σ2d4
0.0 0.0031σ2d2 + 0.0478σ2d4
–0 0.0404σ2 + 0.0069σ2d2 σ2d4
0.0 0.0132σ2d2 + 0.0520σ2d4
–0 0.0382σ2 + 0.0240σ2d2 σ2d4
0.0 0.0209σ2d2 + 0.0553σ2d4
–0 0.0371σ2 + 0.0373σ2d2 σ2d4
0.0179 0.0266σ2d2 + 0.0573σ2d4
0 0.0370σ2 + 0.0463σ2d2 σ2d4 0.0175 0.0300σ2d2 + 0.0575σ2d4
0.1 0.0382σ + 0.0510σd + 0.1083σd 0.0179σ + 0.0313σd + 0
0.0408σ2 + 0.0518σ2d2 + 0.1001σ2d4
0.0190σ2 + 0.0307σ2d2 + 0.052
557
d2 d2
σ + 0.0442σd + 0.0767σ
2 2 2 2
2d σ + 0.0252σd + 0.0405
2 2 2 2
σ2d
0.5 6σ 1σ
0.6 0.0782σ2 + 0.0300σ2d2 + 0.0493σ2d4
0.0366σ2 + 0.0167σ2d2 + 0.0262σ2d4
0.7 0.1045σ2 + 0.0222σ2d2 + 0.0358σ2d4
0.0496σ2 + 0.0123σ2d2 + 0.0190σ2d4
0.8 0.1541σ2 + 0.0145σ2d2 + 0.0229σ2d4
0.0752σ2 + 0.0079σ2d2 + 0.0122σ2d4
0.9 0.2759σ2 + 0.0072σ2d2 + 0.0109σ2d4
0.1454σ2 + 0.0038σ2d2 + 0.0058σ2d4
1 0 0
( ) 4 4
1
2 iu u
x r 4
N
2 3 ,
t k t v N
2 2
N
( ) 4
2t k 2t v N ,
4 1
iu ju u
x x
Using the above relations, for the newly constructed desi e get the follo
1
2 (
gn, w wing:
) 2
2
N
1 2
iu u
x r t k 2t v N ,
1 4
N
t k 2t v( ) 4 3N ,
4 2
x r 1 iu
u
1 2 2
N
iu ju
( ) 4 4 2t k 2t v
1
u
x x N (
The results are given in Table 3
(These expression follow easi
14).
ly from the definition of points sets generated from BIBD and the consequent multiplication with factorial combinations as explained in Raghavarao [7], pp. 298-300)
Using (5) and (12), (13), (14) the design p ameters of the newly constructed design are the following:
ir
ar
2 2
2 4
(1 ) (1 )
,
N N
0 2 2 2 2
1 1
2 2
2 1
a f
N N
e
4 (1 ) 1 (1 )
2 1 2 ,c 2 1 2
(15)
Using (15) a
nd noting
1 1 2
N N
v00 2
1 2 1
,
the expression
2 2 v f a0
c v00 simplifies to
3
2 2
1
2
1 v
2 2
2
2 1
2 1 N4 vN
1 1
N N
Hence the n above
de-signis
on-singularity condition of the
3 1 4
2 2
2 1
1
2 2 1
N v
v N N
Let f (N, N1, ρ) =
(16)
3
2
1 1
1
2 1
N
N N
Table 3. Variance of the timated response for the factors3 ≤v ≤8 , when r > 3λ.
ˆ
V y
4, 2,
r k
es
ρ (v 5,b 10, 1
ˆ
V y
5, 2,
r k
(v 6,b 15, 1
N1= 113, N
= 72, n = 56, m
) = 16
ˆ
V y
1,r 6,k 2, 1
) (v 7,b 2
N1= 253, N = 140, n = 126, m = 14
)
m = 17
N1= 482, N = 257, n = 240,
–1 0 0 0
–0.9 0.0825σ2 – 0.165σ2d2 + 0.0949σ2d4
0.0746σ2 – 0.1420σ2d2 + 0.0768σ2d4
0.0345σ2 – 0.0640σ2d2 + 0.0368σ2d4
.0790σ2d2 + 0.0536σ2d4
0.0254σ2 – 0.0440σ2d2 + 0.0330σ2d4
.0460σ2 2 2 4 2 2 2 2 4
.026
.0673σ2d4`
0.0177σ2 – 0.01 465σ2d4
0.0109σ2 – 0.0050σ2d2 + 0.0349σ2d4
.0010σ2d2 + 0.0497σ2d4
0.0091σ2 + 0.0017σ2d2 + 0.0383σ2d4
0.0128σ2 + 0.0072σ2d2 + 0.0530σ2d4
0.0080σ2 + 0.0072σ2d2 + 0.041
–0.2 0.0189σ2 + 0.0157σ2d2 + 0.0756σ2d4
0.0116σ2 + 0.0137σ2d2 + 0.0558σ2d4
0.0072σ2 + 0.0115σ2d2 + 0.0442σ2d4
–0.1 0.0178σ2 + 0.0232σ2d2 + 0.0769σ2d4
0.0110σ2 + 0.0185σ2d2 + 0.0574σ2d4
0.0068σ2 + 0.0146σ2d2 + 0.0458σ2d4
0 0.0175σ2 + 0.0281σ2d2 + 0.0761σ2d4 .0214σ2d2 0.0067σ2 + 0.0165σ2d2 + 0.0460σ 4
0.1 0.0179σ2 + 0.0305σ2d2 + 0.0731σ2d4
0.0110σ2 + 0.0227σ2d2 + 0.0553σ2d4
0.0068σ2 + 0.0172σ2d2 + 0.0446σ2d4
0.2 0.019σ2 + 0.0306σ2d2 + 0.0679σ2d4
0.0116σ2 + 0.0225σ2d2 + 0.0515σ2d4
0.0073σ2 + 0.0169σ2d2 + 0.0416σ2d4
0.3 0.0209σ2 + 7σ2d2 + 0.0375σ2d4
0.4 0.0241σ2 + 0.0257σ2d2 + 0.0524σ2d4
0.0148σ2 + 0.0186σ2d2 + 0.0400σ2d4
0.0092σ2 + 0.0138σ2d2 + 0.0324σ2d4
0.0289σ2 + 0.0217σ2d + 0.0432 2 4
0.0178σ2 + 0.0157σ2d + 0.0330σ2 4
0.0111σ2 + 0.0116σ2d + 0.0268σ2 4
0.6 0 4
0.0496σ2 + 0.012 d2 + 0.0245σ2d4
0.0308σ2 + 0.009 2d2 + 0.0188σ2d4
0.0194σ2 + 0.006 2d2 + 0.0152σ2d4
–0.8 0.0635σ2 – 0.1193σ2d2 + 0.0816σ2d4
0.0445σ2 – 0
–0.7 0.0461σ2 – 0.0765σ2d2 + 0.0706σ2d4
0.0300σ2 – 0
–0.6 0.0352σ2 – 0.0467σ2d2 + 0.0668σ2d4
0.0223σ2 – 0
–0.5 0.0283σ2 – 0.0248σ2d2 + 0
d + 0.0458σd 0.0181σ – 0.0260σd + 0.0311σd
0σ2d2 + 0.0447σ2d4
0.0137σ2 – 0.0140σ2d2 + 0.0323σ2d4
20σ2d2 + 0.0
–0.4 0.0238σ2 – 0.0080σ2d2 + 0.0698σ2d4
0.0147σ2 – 0
–0.3 0.0208σ2 + 0.0053σ2d2 + 0.0729σ2d4
6σ2d4
0.0107σ2 + 0 + 0.0573σ2d4 2d
0.0288σ2d2 + 0.0608σ2d4
0.0128σ2 + 0.0210σ2d2 + 0.0463σ2d4
0.008σ2 + 0.015
0.5 2 σd 2 d 2 d
.0366σ2 + 0.0173σ2d2 + 0.0338σ2d 0.0226σ2 + 0.0124σ2d2 + 0.0258σ2d4
0.0142σ2 + 0.0092σ2d2 + 0.0209σ2d4
0.7 7σ2 1σ 7σ
0.8 0.0752σ2 + 0.0082σ2d2 + 0.0157σ2d4 0.0472σ2 + 0.0059σ2d2 + 0.0120σ2d4 0.0299σ2 + 0.0043σ2d2 + 0.0098σ2d4
0.9 0.1454σ2 + 0.0040σ2d2 + 0.0075σ2d4
0.0938σ2 + 0.0028σ2d2 + 0.0057σ2d4
0.0605σ2 + 0.0021σ2d2 + 0.0047σ2d4
1 0 0 0
readi
It is ly seen that
N, N , 2,1
1 1
N n
0 f 1
ow start w
SORD in th
2N N 1
We n argue as follows, the design, to ith, is a e usual sense so that 4 v
2
2 2
.
cond revise
tio 6) de re of a
of nclud gh to
v
This ition indeed does satisfy the d condi- n (1 rived here for ρ≥ 0. To take ca ll values
ρ, i ing negative values, it is enou demand 4
2 v
2 2
2 v
3.4 arian
The varianc nder t
correlated structure constructed by the above method is btained by using (7), and (16) and noting the following:
.
. V ce Function
e function of SORDWCE u he auto- o
N1v00 21 2
2 1
1
N
2 2 1
v N 4
00
2 1 2 v
T
2 (1 ) N 2
2 1 2 T, 1
a
3
1 N 2
2 2
2 4 1 2 1
4 1 1
1 2 2 2
1 T
1 N N
d
4 v 2 N1
2
1
N 2
1
vN2
1
2 1 2
3
2 2
1 N
T
7) ance fu
(1 Hence the vari nction is given by,
21
, , ,
B N N v d
,
1
1
, , , ,
v N v
where,
4
)d
, ˆx
V y A N N
( ,
C N say,
2 2 2
0
2 1 ˆ
1
v
V T
4 1
1 , , ,
A N N v
1
2 2
2
1 2 4
2 1
1
, , , 2 1
1
B N N v v
N T
i 2Cov
ˆ ˆ0, ii
2
2 2
1 1 2 2 1 1 2 1 ˆ
N N N v V
3 2
2
4 1
1 1 2 ( 1) 1
1 ˆ
λ 1 ii
v N N N v
V
2 2 2
4 1 1 2
1 , , ,
C N N v
2N T
1
3
2 2
2 1 .
T
vN
thod with the h the help of BIBD. Consider the BIBD (v = 7, b = 7, r = 3, k = 3, λ = 1).Here we have, N = 57, N1 = 113, n = m = 1.
1 1 1
2 4 2 2
4 1
8
N N N
ju u
where
4 v 2 1 N1 N1 2
Example: We illustrate the above me construction of RSORD for 7-factors w
it 56,
2 4
1 1
24 , 24 3 ,
iu iu iu
u u
x N x N x x N
Plan of B
B1 1 2 4
BI D:
B2 2 3 5
3 4 6
B4 4 5 7
B5 5 6 1
B6 6 7 2
B7 7 1 3
B3
The design (denoted by d0) is displayed here for rea y ference (column being runs).
d0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20
d re
x1 0 1 0 1 0 1 0 1 0 –1 0 –1 0 –1 0 –1 0 0 0 0
x2 0 1 0 1 0 –1 0 –1 0 1 0 1 0 –1 0 –1 0 1 0 1
x3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 1
x4 0 1 0 –1 0 1 0 –1 0 1 0 –1 0 1 0 –1 0 0 0 0
x5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 –1
x6 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
x7 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
d0 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40
x1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
x2 0 1 0 1 0 –1 0 –1 0 –1 0 0 0 0 0 0 0 0
x 0 0 0 1 0 1 0 1
0 0 0 1 0 –1 0 –1
0 0 0 0 0 0 0 0
0 0 0 0 –1 0 1 0 –1
0 0 0 0 0 0 0 0 0 0
–1 0
3 0 –1 0 –1 0 1 0 1 0 –1
x4 0 0 0 0 0 0 0 0 0 0
x5 0 1 0 –1 0 1 0 –1 0 1
x6 0 0 0 0 0 0 0 0 0
x7 0 0 0 0 0 0 0 0
–1 1
0 1
–1 0
0 1
0 0
d0 41 42 43 44 45 46 47 48 49 0 51 525 53 54 55 56 57 58 59
x1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
x2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
x3 0 –1 0 –1 0 –1 0 –1 0 0 0 0 0 0 0 0 0 0 0
1 0 –1 0 –1 0 1 0 1 0 1 0 1 0 –
0 0 0 0 0 0 1 0 1 0 –1 –1 0 1
0 1 0 –1 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 1 0 –1 0 1 0 –1 0 1
x4 0 1 0 1 0
x5 0 0 0 0 0
x6 0 1 0 –1 0
x7 0 0 0 0
2 3 64 65 66 67 68 69 70 71 72 7 7 7 7 7
d0 60 61 6 6 3 4 5 6 7 78
x1 0 0 0 0 0 1 0 1 0 1 0 1 0 –1 0 –1 0 –1 0
x2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
x3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0
1 0 1 0 1 0 –1 0 –1 0 1 0 1 0 –1
1 0 –1 0 1 0 –1 0 1 0 –1 0 1
x7 –1 0 1 0 –1 0 0 0 0 0 0 0 0 0 0 0 0 0 0
0 0
x4 –1 0 –1 0 –1 0 0 0 0 0 0 0
x5 1 0 – 0 –1