ICP Test Report Certification Packet

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1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: 3.6 x 10 mm Fuse

Product #: 875xxx Series

Issue Date: February 19, 2013

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued :

(1) Parts, sub-materials and unit parts

This document covers the 3.6 x 10 mm Fuse, RoHS-Compliant series products manufactured by Littelfuse, Inc.

＜ Raw Materials Used Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1 Remarks：

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2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s)

1 Y50/ YJM (909-444) Ceramic Base - Body 3-13

2 934-065 Cap & Lead Assembly 14-17

3 082xxx Element- 5% by weight Ag Clad Cu 18-22

4 11-0803 (497xxx) Element – Ni42Fe58MCuAg5% 23-27 5 10-1185 (497xxx-001) Element – Ni42Fe58MCuMSn 28-33

6 7132 (425672) Ink-Black 34-42

7 692481 Solder Wire 43-48

8 063012 Element - Sn Plated Cu Clad Cu55 Ni45 49-56

Form 585-047 Rev. A 2/21/06

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Customer: Suzhou FuHong Electronjc InduslrialCo., Lld.

Addres!: NO.89 WEIDU ROAD, WANGTINGTOWN, XIANGCHENG DlsTRlCT, SUZHOU, CHINA Report on ths submitred s.mplesald to be

S.mple name: CoppeJ,shell M o d € h /

Item/LoiNo.:/

M e t a r l a l : / , Buyer: / , Suppli€r: /

Samplo recaivsd d.te: Ocl. 08. 2012

Testins period: Ffom oct os, 20!€ 1o'O4r'10, 2012

. . ,,

' \ l '

E9S!.s-Ecs!ed9!f

NO.: 4002R12100802+1 R02

As specified by dient, to determine ihe Lead, cadmlun, accordance with Dircctive 2002/95/EC {RoHS).

AOV"BPFS,U

LiTingting, Maggie Chemic€l Test Direcror

TEST REPORT

Dare: ocr.10, 2012

Mercury & Hexavalent Chrcmium content in the submitled sample in

Ylan Qi, lrickey

Ec!!!s-ee$9!.:

Testing ltem Measunng instrumeni I\4QL

Lead (Pb) IEC 62321: 2008, s€ction 9 ICP€ES 2-'nglkg Cadmium (cd) |EC62321: 2008, seclion I ICP-OES 2 mg/kg [4ercury (Hg) lEc 62321 2008, seclron 7 tcP-oEs 2 mg/kg

Chromum (Cr\rl) IEC 62321 2008 Annex B 0.02m9/k9'

Ieq

r 0.02 mg/kg reE|s to the MQL ofsample extfaction liquid

SsElcge!:

-when tesled as speci{i€d the submitted sample complied with the requirements of commission Decision ol 18 Aug 2005 amending Directjve 2002/95/Ec noiilied under document 2005/618/Ec

ILS, PLEASE REFER TOTHE FOLLOWNG PAGE(S)***

signed lor and on behalfof

Shenzhen AOV Tesling Technology Co., Ltd, Kunshan Brcncn

caeateaaer: /blfil **n"oor, We-r k] n ooo,',or44.

S I t E N 2 H E N A O V T f S I I N G T € C H N O I , O 6 Y C O . , I " T O . K U N S N A N B R A N C T I

/// \ Noll ne

, J a,t 7tt) 9€'t'o

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AOV'*F#S,[

NO.: 4002R121008024-1 R02

TEST REPORT

O a t e : O d . 1 0 , 2 0 1 2

Conte

nt i|retb.r

_.

sulit€le)

_\ _.

Cooling the vess€|, nlter;washed and Rlled 10 the mark with distill€d wat€r.

The sample is digested in the microwave oven following a specific decomposrlon program

Test the sample solution and lhe 0.02 ng/kg standard solltion by uv-vls.

F;;1.-

SH€NZH€N AOV TESTITIG lCCINOLOGY CO.,LTD.KUNSIIAN BSANCH

( :

H o t l r n e

'tL)0 700 8600 1. To Determiney'.ead, C€dmium Contenli (Metal subslrate)

Iredby (y'a04

Add ihe digestion solulioni the vessel is heated unlil the sample Weigh ihe sample into

Add HrOruntilthe sample is clear

To Dete

Weigh ihe sample

Cooling the vessel, tiltei washed and filled lothe maiK wilh dislilled water.

Tested by lcP-oES

Chromium Contenl (boiling- wat€F €xtlaclion): ([4etal Eubstrate)

Remove lhe sample, and cool the beak€r to room temperature,

and do the color reaction Take the (50i5) cm,

sample in the beaker.

Heat 50 mL of Olwater in the be6ker to boiling for 1o

(16)

nov'Bpf,F,il

NO.: 4002R121008024-1R02

5. To oetemine Hexavalenl Chromium Contonl in

_ .. -i\

: va'hu't'

TEST REPORT

Daie: Ocl.10, 2012

colorless and colored chromate coating on metats: iPtating)

5.2 Boiling-wateF enradion

lfthe lest result is positive, the sample is considered to have hexavalent chmmium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extraotion procedu€ shall be used to

lflhee is interference or it is hard to decide whetherlhe sample have lhe hexavalent

Remove the sample, and cool the beaker lo room temperalure,

and do lhe color reaction sample in the beaker.

Heat 50 mlof Dlwaier in the beaker to boiling for 10 min

Test tne sample solution and lhe 0.02 mg/kg standad solulion by UV-VIS.

Sample Delcriptlon:

Code Sample Descndion

1-1 Substrate

Plating

Te3t R63ulb:

Unit RoHS Limit

Lead (Pb) msfts 1 0 0 0 N . D . 1 0

Cadmium (Cd) mg/K9 1 0 0 N . D . N . O . Merorry (Hg) ms/Kg 1 0 0 0 N . D , N . D . Chromium {Crl,ll) m9/kg 1 0 0 0 Negative Negative

s8€NZh€N AOV T€SrtNG TECHNOlOSY CO,,tTD,TUNSHAI!ARANCH

H o t l i n e .100 700 B6a0

,.r

(17)

nov'F"Ff"qn

No.: A002R1210o602:L1 R02

neoatve.,

-"The te8t is bas€d on lhe followins d!!{mplifi:

maybe cannot stand lor the physical lrdh 6t s€r

TEST REPORT

Coppershell

-The new RoHS dircclive 2011/6tEU, on Jul. 21, 2011 come into forc€, on Jan. 03, 2013lhe formal implementation, Direclive 2002r'95/EC ahall be repealed simultaneously.

Sp€cimens, which r€Slested lo detemine Lead, Cadmium and Mercury Content, have been dissolved completely, -mg/kg=ppm ,

-N.D.=not

i",, ,,,,

( The iested sample result is uncertain or

SH€NZII AOVTIST|n|G TECHNOIOCV CO.,ITD.KUNSHAN AFANCH

H o t l i n e

400 /00 8600

(18)

Test Report Number： SHAH0036227401

Authorized by：

For intertek testing services Ltd., Shanghai

Jacob Lin General Manager

Page 1 Of 5

Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

Applicant： ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date： JAN 18, 2013

GM BH

GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY

Sample Description：

Two(2) pieces of submitted samples said to be ： (1) Mixed all kinds of metal substrates.

(2) Mixed all kinds of plating layers.

Item Name ： Silver Plated & Pure Silver Wires.

Item No. ： (B-1) 101.014 -. ----

– silver plated copper wire – Cu, Ag--%

(B-2) 101.0131.---- – pure silver wire – Ag 1000 (B-3) 101.0123.0---

– silver plated purest nickel wire – Ni99.98%, Ag1%

(B-4) 101.0182.0---

– silver-copper alloy plated copper plated iron nickel alloy wire – ElconD, AgCu5%

(B-5) 101.0120.0---

– silver plated constantan wire – CuNi44, Ag5%

(B-6) 101.0151.0---

– silver plated copper - nickel 44 alloy wire – CuNi44, Ag10%

(B-7) 1050--31.---

– pure silver strips – Ag 1000 pure

Country Of Origin ： Germany.

************************************************************************************************************************************************************

Tests Conducted：

As requested by the applicant, for details refer to attached page(s).

************************************************************************************************************************************************************

To Be Continued

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Test Report Number： SHAH0036227401 Tests Conducted

Page 2 Of 5 Intertek Testing Services Ltd., Shanghai

(A) Test result of RoHS Directive：

Result Testing item

(1)

Cadmium (Cd) content (mg/kg) ND

Lead (Pb) content (mg/kg) ND

Mercury (Hg) content (mg/kg) ND

Chromium (VI)(Cr⁶⁺) result (by boiling water extraction on metal) (mg/kg

with 50cm²) ND

Result Testing item

(2)

Cadmium (Cd) content (mg/kg) /Plating ND

Lead (Pb) content (mg/kg) /Plating ND

Mercury (Hg) content (mg/kg) /Plating ND

Chromium (VI)(Cr⁶⁺) result (by boiling water extraction on metal) (mg/kg

with 50cm²) /Plating ND

Remark：mg/kg with 50cm² = milligram per kilogram with 50 square centimeter ND = not detected

(B) RoHS Requirement：

Restricted substances Limits

Cadmium (Cd) 0.01% (100 mg/kg)

Lead (Pb) 0.1% (1000 mg/kg)

Mercury (Hg) 0.1% (1000 mg/kg)

Chromium (VI) (Cr⁶⁺) 0.1% (1000 mg/kg)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(C) Test method：

Testing item Testing method Reporting limit

Cadmium (Cd) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and

determined by ICP-OES. 2 mg/kg

Lead (Pb) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and

Mercury (Hg) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and

Chromium (VI) (Cr⁶⁺) content(for metal)

With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS

Spectrophotometer.

0.02mg/kg with 50cm² (in testing solution) Date sample received： Jan.14, 2013

Testing period： Jan.14, 2013 To Jan.17, 2013

************************************************************************************************************************************************************

To Be Continued

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(D) Measurement flowchart：

Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008

Remarks：

*1: list of appropriate acid：

Material Acid added for digestion

Polymers HNO 3,HCL,HF,H2O2,H3BO3

Metals HNO 3,HCL,HF

Electronics H NO3,HCL,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

************************************************************************************************************************************************************

To Be Continued Sampling/grinding or cutting

Weigh sample and for different material, digest

the sample with appropriate acid^*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp.

Extraction

Make up with deionized water and add diphenyl-carbazide

solution Cr⁶⁺

Weigh sample and add organic

solvent

Soxhlet extraction Solvent extractionor

Concentrate the extract and make

up with organic solvent PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD Spot test

Get 50cm² samples

Boiling water extraction

Metal

Polymers / electronics

Positive^*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract Yes

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************************************************************************************************************************************************************

To Be Continued

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************************************************************************************************************************************************************

End Of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or

representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

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Test Report Number : TWNC00294417

Authorized by:

On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

THJ0294417

Page 1 of 5

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司

11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jan 17, 2013 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be :

Part Description : Ni42Fe58MCuAg5% Element Part Number : 497226 (497xxx)

Date Sample Received : Jan 11, 2013 Date Test Started : Jan 11, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

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Number : TWNC00294417

Test Conducted

THJ0294417

Page 2 of 5

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary:

Result

Test Item Unit Test Method Silvery

metal wire

RL

Heavy Metal

Cadmium (Cd) content ppm

With reference to IEC 62321: 2008, by

microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) content ppm

ND 2

Mercury (Hg) content ppm

ND 2

Chromium VI (Cr⁶⁺) content

mg/kg with 50 cm²

With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.

Negative 0.02

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm² = milligram per kilogram with 50 square centimeter

Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result.

Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 11, 2013

Test Period : Jan 11, 2013 To Jan 15, 2013 (Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm)

Lead (Pb) content 0.1% (1000ppm)

Mercury (Hg) content 0.1% (1000ppm)

Chromium VI (Cr⁶⁺) content 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

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Test Conducted

THJ0294417

Page 3 of 5

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI)

Reference Standard：IEC 62321 edition 1.0:2008

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid^*1

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp.

extraction

Make up with deionized water and add diphenylcarbazide solution

Cool and filter the extract Cr⁶⁺

Analyzed by UV-VIS By spot test

Get 50cm²sample

Metal Polymers /

Electronics

Negative^*2 Confirm the tested

samples are totally dissolved

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Test Conducted

THJ0294417

Page 4 of 5

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Remarks:

*1: List of Appropriate Acid：

Material Acid Added for Digestion Polymers HNO_3,HCl,HF,H₂O_2,H₃BO₃

Metals HNO_3,HCl,HF

Electronics HNO3,HCl,H2O2,HBF4

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

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Test Conducted

THJ0294417

Page 5 of 5

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo

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Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·

Durch die DAkkS nach DIN EN ISO/IEC 17025 akkreditiertes Prüflaboratorium Die Akkreditierung gilt für die in der Urkunde aufgeführten Prüfverfahren.

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] USt-IdNr. DE169317871 Rainer Mast

Polyfil AG Gina Gregorio

Oberallmendstrasse 20A 6300 Zug / Switzerland

Fürth, 2012-12-19

Test report No. FUHL1236938

Testing of a material sample according to the RoHS directive 2011/65/EC

Sample description: Ni42Fe58MCuMSn wire; part no. 4500237197; batch 0380.6025

Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10 Head of Inorganic Lab: Claudia List

Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item.

This report consists of 6 page(s).

The test methods signed with * are not listed in the attachment of the accreditation certificate.

Conclusion based on tested item

Test order Status

testing according to the RoHS directive 2011/65/EC conform^°

° Please see overview of test results

- Test results see next pages -

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Page 2 of 6 page(s) of our test report No. FUHL1236938 dated 2012-12-19

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer

Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

nM = non Metal M = Metal

cM = composite Material

List of component parts:

Sample No. Part No. Material Description

236938 1 M Ni42Fe58MCuMSn wire; part no. 4500237197; batch 0380.6025

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Comment

LOD = Limit of Detection BL = Below Limit OL = Over Limit

X = Inconclusive, further test necessary σ = Standard deviation

CS = Composite sample

Remark:

Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb), AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration exceeds the below warning value according to IEC 62321.

Element Unit non - metal metal

Cd mg / kg BL ≤ (70-3σ) < X < (130+3σ) ≤ OL BL ≤ (70-3σ) < X < (130+3σ) ≤ OL Pb mg / kg BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL Hg mg / kg BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL

Br mg / kg BL ≤ (300-3σ) < X --

Cr mg / kg BL ≤ (700-3σ) < X BL ≤ (700-3σ) < X

Element Unit composite material Cd mg / kg LOD < X < (150+3σ) ≤ OL

Pb mg / kg BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL Hg mg / kg BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL

Br mg / kg BL ≤ (250-3σ) < X Cr mg / kg BL ≤ (500-3σ) < X

(31)

1. XRF screening

Method: XRF according to IEC 62321:2008*

Sample No. Part No. Pb Hg Cd Crtotal Br Status

236938 1 BL BL BL BL -- conform

Comment:

Elements RoHS-limit value

Lead (Pb) 1000 mg/kg

Mercury (Hg) 1000 mg/kg

Cadmium (Cd) 100 mg/kg

Chromium VI (Cr VI) 1000 mg/kg

Polybrominated Biphenyle (PBBs) 1000 mg/kg

Polybrominated Diphenyl ether (PBDEs) 1000 mg/kg

- Flow charts see next page(s) -

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Page 5 of 6 page(s)

Test procedure

Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast YES

YES

YES NO

NO NO

NO

NO samples

metallic materials,

polymer materials,

electronics (PCB / component)

mechanical sample preparation

mechanical sample preparation screening

by XRF ?

sample

uniform ? screening

procedure by XRF

chemical test procedure (verification)

various methods (please see verification test

procedure below)

meets limits ?

further testing ?

meets limits ?

pass entity based conforming

sample

fail entity based non conforming

sample

pass entity based conforming

sample

fail entity based non conforming

sample non-destructive

sample preparation

(33)

Page 6 of 6 page(s)

Verification test procedure

Sample Preparation

Sample Measurement

Sample solvent extraction

Concentration/

Dilution of extraction solution

Filtration

GC/MS

DATA Acid digestion with

microwave / hotplate

Filtration

Residue

Total digestion Solution

ICP-OES/AAS

DATA

Non-metallic material

Alkaline extraction Adding extraction

solution

Alkaline extraction Heating to 90~95°C

for extraction

Filtration and pH adjustment

Adding 1,5- diphenylcarbazide for color development

UV-VIS or IC-UV/VIS

DATA

Metallic material

Spot test

Adding 1,5- diphenylcarbazide for color development

A red color indicates the presence of Cr⁶⁺

If necessary, confirm with UV-VIS or

IC-UV/VIS

DATA

Pb/Cd/Hg PBBs/PBDEs Cr⁶⁺

Positive

Negative

(34)

Authorized By:

On Behalf Of Intertek Testing Services Taiwan Limited

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Applicant: Littelfuse Philippines Inc. Date : May 16, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Ink

Part Number : 425672

Date Sample Received : May 10, 2012 Date Test Started : May 10, 2012

Test Conducted :

(35)

Number : TWNC00256916 Test Conducted

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅰ) Test Result Summary :

Result (ppm) Test Item

Black Paste Heavy Metal

Cadmium (Cd) content ND

Lead (Pb) content ND

Mercury (Hg) content ND

Chromium VI (Cr⁶⁺) content ND

Polybrominated Biphenyls (PBBs)

Monobrominated Biphenyls (MonoBB) ND

Dibrominated Biphenyls (DiBB) ND

Tribrominated Biphenyls (TriBB) ND

Tetrabrominated Biphenyls (TetraBB) ND

Pentabrominated Biphenyls (PentaBB) ND

Hexabrominated Biphenyls (HexaBB) ND

Heptabrominated Biphenyls (HeptaBB) ND

Octabrominated Biphenyls (OctaBB) ND

Nonabrominated Biphenyls (NonaBB) ND

Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs)

Monobrominated Diphenyl Ethers (MonoBDE) ND

Dibrominated Diphenyl Ethers (DiBDE) ND

Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND Halogen Content

Fluorine (F) ND

Chlorine (Cl) ND

Bromine (Br) ND

Iodine (I) ND

(36)

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Black Paste Phthalates

Di(2-ethylhexyl) Phthalate (DEHP) ND

Dibutyl Phthalate (DBP) ND

Benzyl Butyl Phthalate (BBP) ND

Others

Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg

ND = Not detected

Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : May 10, 2012

Test Period : May 10, 2012 To May 16, 2012

(Ⅱ) RoHS Requirement:

Cadmium (Cd) Content 0.01% (100ppm)

Lead (Pb) Content 0.1% (1000ppm)

Mercury (Hg) Content 0.1% (1000ppm)

Chromium VI (Cr⁶⁺) Content 0.1% (1000ppm)

Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

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(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by

microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent

extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent

extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content

With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates

With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

10 ppm

Hexabromocyclodode cane (HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

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Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks:

Material Acid Added for Digestion

Polymers HNO_3,HCl,HF,H₂O_2,H₃BO₃

Metals HNO3,HCl,HF

Electronics HNO_3,HCl,H₂O_2,HBF₄

Sample preparation

Cd/Pb/Hg

Analyzed by ICP-OES

Definite temp.

extraction

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make up with organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD By spot test

Get 50cm²sample

By boiling water extraction

Metal Polymers /

electronics

Negative ^*2 Confirm the tested

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component For non-metal part For metal part

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Test for Halogen Content Reference Standard：EN 14582

Add absorbent in a combustion flask &

place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room

temperature

Transfer the absorbent into a volumetric flask

Analyzed by ion chromatography

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Test For Phthalates Contents Reference Method: EN 14372: 2004

By solvent extraction

Concentrate the extract and make up with

organic solvent

Analyzed by GC-MSD

(41)

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Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C

End of Report

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

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Photo

(43)

Authorized By:

On Behalf Of Intertek Testing Services Taiwan Limited

THJ0289673

Page 1 of 6

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Applicant: Littelfuse Philippines Inc. Date : Dec 13, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Solder

Part Number : 692481

Date Sample Received : Dec 06, 2012 Date Test Started : Dec 07, 2012

Test Conducted :

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THJ0289673

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Silvery metal Heavy Metal

Cadmium (Cd) content ND

Lead (Pb) content 260

Mercury (Hg) content ND

Chromium VI (Cr⁶⁺) content (mg/kg with 50cm²) Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg

ND = Not detected

< = Less than

mg/kg with 50cm² = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received : Dec 06, 2012

Test Period : Dec 07, 2012 To Dec 12, 2012

(Ⅱ) RoHS Limits:

Cadmium (Cd) Content 0.01% (100ppm)

Lead (Pb) Content 0.1% (1000ppm)

Mercury (Hg) Content 0.1% (1000ppm)

Chromium VI (Cr⁶⁺) Content 0.1% (1000ppm)

(45)

THJ0289673

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(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

2 ppm

Lead (Pb) content

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm²

Remark: Reporting limit = Quantitation limit of analyte in sample

(46)

THJ0289673

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Test For Cd/Pb/Hg/Chromium (VI)

Cd/Pb/Hg

Analyzed by ICP-OES

Definite temp.

extraction

Get 50cm²sample

Metal Polymers /

Electronics

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THJ0289673

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Remarks:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3

Metals HNO3,HCl,HF

Electronics HNO3,HCl,H2O2,HBF4

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

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THJ0289673

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Photo

(49)

Authorized by:

THJ0296620

Page 1 of 8

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Applicant: Elschukom Elektroschutzkomponentenbau Date : Jan 30, 2013 GmbH

Gewerbestrasse 87, D-98669 Veilsdorf, Germany

Sample Description:

One (1) group of submitted samples said to be : Sample Description : Tin plated Wires

Style / Item No. : Please see page two to three.

Country of Origin : Germany Date Sample Received : Jan 23, 2013 Date Test Started : Jan 23, 2013

Test Conducted :

(50)

Authorized by:

THJ0296620

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Sample Description:

Style / Item No. : (A-1)101--271.0---

– tin plated copper wire – Cu, Sn--%

(A-2)101--283.0---

– tin plated, copper plated copper nickel alloy wire – Elcon30, Sn--%

(A-3)101--272.0---

– tin plated, copper plated steel wire – ElconF, Sn--%

(A-4)101--281.0---

– tin plated, copper plated iron nickel alloy wire – ElconD, Sn--%

(A-5)101--221.0---

– tin plated copper nickel alloy wire - CuNi44, Sn--%

(A-6)101--24-.0---

– tin plated, silver plated copper wire – Cu, Ag--%, Sn--%

(A-7)101--257.0---

– tin plated brass wire – Cu80Zn20, Sn--%

(51)

Authorized by:

THJ0296620

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Sample Description:

Style / Item No. : (A-9)101--234.0---

- tin plated silver copper alloy wire – AgCu90, Sn--% (ElCu90, Sn--%)

(A-10)101--255.----

– tin plated copper zinc alloy wire – Cu70Zn30, Sn--%

(A-11)101--229.----

– tin plated copper nickel alloy wire – CuNi12, Sn--%

(A-12)101--235.----

– tin plated silver copper alloy wire – Ag72Cu28, Sn--%

(A-13)101--231.----

– tin plated silver wire – Ag1000, Sn--%

(A-14)101--236.----

– tin plated silver copper alloy wire – Ag45Cu55, Sn--%(AgCu55, Sn)

(A-15)101--266.----

– tin plated silver copper alloy wire – AgCu70, Sn--%(ElCu70, Sn)

(A-16)101--238.----

– tin plated silver copper alloy wire – AgCu80, Sn--%(Elcu80, Sn)

(A-17)101--228.0---

– tin plated tungsten wire – W, Sn

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THJ0296620

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(Ⅰ) Test Result Summary:

Result

Test Item Unit Test Method Mixed all

kinds of metal wire

RL

Heavy Metal

Cadmium (Cd) content ppm

ND 2

Lead (Pb) content ppm

37 2

Mercury (Hg) content ppm

ND 2

mg/kg with 50 cm²

With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.

Negative

(#) 0.02

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm² = milligram per kilogram with 50 square centimeter

Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result.

# = Due to the insufficient sample area, reduced total sample surface of 10 cm² was used and the dilution factor was adjusted accordingly.

Responsibility of Chemist: Kevin Liu/ Irene Chiou

Date Sample Received : Jan 23, 2013

Test Period : Jan 23, 2013 To Jan 29, 2013

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THJ0296620

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(Ⅱ) RoHS Limits:

Cadmium (Cd) content 0.01% (100ppm)

Lead (Pb) content 0.1% (1000ppm)

Mercury (Hg) content 0.1% (1000ppm)

Chromium VI (Cr⁶⁺) content 0.1% (1000ppm)

(54)

THJ0296620

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(Ⅲ) Measurement Flowchart:

Test for Cd/Pb/Hg/Chromium (VI)

Cd/Pb/Hg

Analyzed by ICP-OES

Definite temp.

extraction

Get 50cm²sample

Metal

Polymers / Electronics

ICP Test Report Certification Packet