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(1)

UNIVERSITY OF LONDON University College London

Department of Electronic and Electrical Engineering

Fast Waveform Metrology:

Generation, Measurement and Application of Sub-

picosecond Electrical Pulses

Andrew JA Smith

November 1995

(2)

This thesis describes work performed at the National Physical Laboratory to improve the electrical risetime calibration of instruments such as fast sampling oscilloscopes. The majority of the work can be divided into four sections: development of an ultrafast optoelectronic pulse generator; measurement of fast electrical pulses with an electro- optic sampling system; de-embedding of transmission line and transition effects as measured at different calibration reference planes; and calibration of an oscilloscope.

The pulse generator is a photoconductive switch based on low-temperature Gallium Arsenide, which has a very fast carrier recombination time. Sub-picosecond electrical pulses are produced by illuminated a planar switch with 200 fs optical pulses from a Ti: sapphire laser system.

The pulses

are measured

using a sampling

system

with an external

electro-optic

probe in

close proximity to the switch. The electro-optic sampling system, with a temporal

resolution better than 500 fs, is used to measure

the electrical pulse shape at various

positions along the planar transmission

he. The results are compared to a pulse

propagation

model for the line. The effects of different switch geometries

are examined.

Although the pulse generator produces sub-picosecond

pulses near to the point of

generation, the pulse is shown to broaden to 7 ps after passing along a length of

transmission

line and a coplanar-coaxial

transition. For a sampling

oscilloscope

with a

coaxial input connector,

this effect is significant.

Frequency-domain

measurements

with

a network analyser,

further electro-optic

sampling

measurements,

and the transmission

line

model are combined

to find the network transfer function of the transition.

Using the pulse generator,

the electro-optic

sampling

system

and the transition knowledge,

a 50 GHz sampling

oscilloscope

is calibrated.

The determination

of the instrument

step

response

(nominal risetime 7 ps) is improved from an earlier value of 8.5 -3.5 / +2.9 ps

to a new value of 7.4 -2.1 / +1.7 ps with the calibration techniques

described.

(3)
(4)

CONTENTS

Page

ABSTRACT

...

2

CONTENTS

...

4

ILLUSTRATIVE MATERIAL

...

8

INTRODUCTION

1.1

The sampling

oscilloscope ...

12

1.1.1 History

...

12

1.1.2 Recent developments ... 12

1.2 Introduction to waveform metrology ... 14

1.2.1 Impulse response ... 14

1.2.2 Optoelectronic

approach

...

15

1.3 Organisation of thesis ... 16

1.4

Thesis

Terminology

...

17

1.4.1 Domains

and FFT ...

18

1.4.2 BSI/ IEC standards

...

18

1.4.3 Definition of oscilloscope response ... 19

1.4.4 Convolution

and deconvolution

...

21

1.5

References

to Chapter 1

...

22

2

BACKGROUND THEORY

2.1

2.2

Introduction

...

Principle of the photoconductive

switch ...

23

23

2.3 Modelling the photoconductive switch ... 24

2.3.1 Voltage considerations ...

24

2.3.2 Speed considerations ... 26

2.4

Photoconductive

material selection ...

28

2.5

Properties

of LT-GaAs ...

31

2.6

Wafer growth ...

33

2.7

Conclusions

...

38

2.8

References

to Chapter

2

...

39

3 DESIGN, FABRICATION AND ELECTRICAL CHARACTERISATION

3.1

Introduction

...

41

3.2 Coplanar waveguide and stripline transmission lines ... 41

3.2.1 Design equations for CPW ... 42

3.2.2 Design equations for CPS ... 45

3.3

Mask design

...

46

3.3.1 Packaging issues ... 46

(5)

3.3.2 Taper

...

48

3.3.3 Example

of devices

- design

A

...

49

3.3.4 Features

on a mask ...

50

3.4

Device fabrication

...

51

3.5

D. C. and low frequency

measurements

...

56

3.6

Conclusions

...

62

3.7

References

to Chapter

3

...

63

4 SAMPLING OSCILLOSCOPE AND ELECTRO-OPTIC SAMPLING MEASUREMENTS

4.1

Introduction

...

65

4.2

Photoconductive

switch configurations

...

65

4.2.1 CPW sliding contact

...

66

4.2.2 CPW Ruston switch ... 66 4.2.3 CPS sliding contact ...

4.2.4 Approximate response of configurations ...

67 68

4.3

Theory of EOS

...

4.3.1 Pockets effect ...

4.3.2 Sampling and detection ...

69 69 71

4.4

4.5

The dye laser EOS system

The Ti: sapphire

laser EOS system ...

...

4.5.1 Prism probe

...

4.5.2 Probe station

...

73

75

75

78

4.6

4.7

4.5.3 Calibration of voltage ... Dye laser measurements ...

4.6.1 CRO results ... 4.6.2 EOS results ...

Ti. sapphire laser measurements ... ... ... '... 4.7.1 CRO results ...

79 79 79 84 85 85

4.8

4.9

4.7.2 EOS results

...

4.7.2.1 CPW sliding contact

...

...

4.7.2.2 CPW Auston switch ...

4.7.2.3 CPS sliding contact

...

CRO measurements

of SI-GaAs ...

EOS system limitations and response

of LT-GaAs ...

4.9.1 Noise and voltage limitations

...

4.9.1.1 Laser noise

...

4.9.1.2 EOS S/N

...

86

86

89

90

91

92

92

92

93

4.10

4.11

4.9.1.3 Dynamic range ...

4.9.1.4 Probe height sensitivity ... 4.9.2 Dye laser system resolution ...

4.9.3 Ti: sapphire laser system resolution ... 4.9.4 Temporal response of LT-GaAs ... Conclusions

... References to Chapter 4

(6)

5

DE-EMBEDDING THE TRANSMISSION LINE AND TRANSITION

5.1

Introduction

...

104

5.1.1 Approach to de-embedding

- organisation

of chapter ...

105

5.1.2 Transmission

he components

of the pulse generator

...

105

5.2 Transmission line modelling ... 107

5.2.1 Modal dispersion

ß.

...

109

5.2.2 Conductor

loss a. and conductor phase ß. ...

III

5.2.3 Dielectric loss aa ...

113

5.2.4 Radiation

loss a, . ...

114

5.2.5 Summary of terms in model ... 115

5.3 Frequency-domain measurements ... 115

5.3.1 The automatic network analyser ...

116

5.3.2 Two transition measurements

with an ANA ...

118

5.3.2.1 Alumina line

...

119

5.3.2.2 GaAs line

...

122

5.3.3 Single transition measurements with an ANA ... 124

5.3.4 Results of transmission line model in the frequency-domain ... 127 5.3.5 Comparison of model with ANA results ... 132

5.4

Time-domain

measurements

...

134

5.4.1 Two transition measurements

with a CRO ...

134

5.4.2 Results

of transmission

line model in the time-domain ... 139

5.4.2.1 Modelling of Gaussian

pulses ...

139

5.4.2.2 Summary

of Gaussian

pulses ...

143

5.4.2.3 Effect of taper

...

144

5.4.3 Comparison

of model with EOS results ...

145

5.4.3.1 GaAs line

...

145

5.4.3.2 Alumina line

...

147

5.5

The impulse

response

of a single transition ...

148

...

5.5.1 EOS measurement

of two transitions

...

148

5.5.2 Derivation of single-transition

response ...

150

5.6

...

Conclusions

152

5.7

...

.

References

to Chapter

5

153

.

...

6

THE OSCILLOSCOPE RESPONSE

6.1

Introduction

...

155

6.2

Deconvolution

...

6.2.1 Quadrature

approximation ...

155

155

6.3

6.4

6.5

6.6

6.2.2 Deconvolution

and filtering ...

6.2.3 Example

of deconvolution ...

6.2.4 Example

of uncertainties

in deconvolution

...

Jitter

...

6.3.1 Measurement

and removal of jitter ...

Deriving the oscilloscope

response ...

(7)

6.7

References

to chapter 6 ...

174

7

CONCLUDING COMMENTS AND FUTURE WORK

7.1 Introduction ... 175

7.2

Concluding

comments ...

175

7.2.1 Pulse generator

...

175

7.2.2 Electro-optic sampling

...

176

7.2.3 De-embedding

...

177

7.2.4 Oscilloscope calibration ... 178

7.3 Future work and opportunities ... 178

7.3.1 Oscilloscope calibration ... 178

7.3.2 Opportunities ... 180

7.4

References

to Chapter

7

...

182

APPENDICES A Measurement of bias tees and attenuators ... 183

A. 1

Introduction

...

183

A. 2

Measurements

...

183

A. 3

Conclusions

...

184

B List of publications during project ... 185

ACKNOWLEDGEMENTS

(8)

Table 1.1

Recent

history of oscilloscope

risetimes

and NPL calibration

facilities.

Table 2.1 Some typical photoconductive semiconductors.

Figure 2.1

Simple photoconductor

circuit.

Figure 2.2 Equivalent circuit of photoconductive switch. Figure 2.3 Structure of LT-GaAs wafer.

Figure 2.4 Example of room-temperature photoluminescence of LT-GaAs- Figure 2.5 Example of X-ray analysis of LT-GaAs wafer.

Figure 2.6 X-ray analysis of SI-GaAs wafer.

Chapter 3

Table 3.1

Frequency-dependent

effect of line size and metal thickness

on impedance.

Table 3.2

Summary

of important devices.

Table 3.3

Measured

device resistances

and derived metallisation

resistivities.

Figure 3.1

Geometry

of coplanar

waveguide

(CPW).

Figure 3.2 Geometry of coplanar stripline (CPS).

Figure 3.3

Central line taper from small to large CPW.

Figure 3.4

Device A with tapers.

Figure 3.5

Example

of features

on NPL-designed

mask.

Figure 3.6 Schematic of I-V contact measurements.

Figure 3.7 I-V curve of unannealed S. I. GaAs device TL4. Figure 3.8 I-V curve of annealed S. I. GaAs device TLS.

Figure 3.9 I-V curve of unannealed LT-GaAs device PG4.

.

Chapter

Table

4.1

Laser amplitude noise.

Table 4.2

System

resolution

of dye laser and Ti: sapphire

laser EOS.

Table 4.3

Deconvolved

response

of LT-GaAs.

Figure 4.1

CPW sliding contact measurement

configuration.

Figure 4.2

CPW Auston switch measurement

configuration.

Figure 4.3

CPS sliding contact measurement

configuration.

Figure 4.4

Approximating

the capacitance

of the CPW gap by a CPS line. Dimensions

(9)

are in µm.

Figure 4.5

Schematic

of an electro-optic

modulator.

Figure 4.6

Transmission

of an electro-optic

modulator.

Figure 4.7

Dye laser electro-optic sampling

system.

Figure 4.8 Structure of LiTaO3 probe.

Figure 4.9

Ti: sapphire

EOS system.

Figure 4.10 Photograph of probing station, showing optical arms for the generation,

sampling

and CCD imaging

systems

around a device mounted

in a UTF.

Figure 4.11

Schematic

of sampling

oscilloscope

measurement

system.

Figure 4.12 Oscilloscope measurement of PG1.

Figure 4.13 Linearity of photoconductive switch with respect to bias voltage. Figure 4.14 Location of excitation points.

Figure 4.15 Oscilloscope measurement

of pulse generator at various excitation

locations.

Points 2,3, and 4 correspond

to Figure 4.13.

Figure 4.16 Dye laser EOS of PG1 with 200 pm generate-sample separation:

sampled same side of CPW as excited; sampled opposite side. Figure 4.17 Oscilloscope measurement of PG4.

Figure 4.18 EOS of CPW sliding contact with generate-sample spacing of 200 µm: sampled same CPW side as generated; sampled opposite side. Figure 4.19 EOS of CPW sliding contact with generate-sample spacing of 1.5 mm:

sampled

same

CPW side as generated;

sampled

opposite

side.

Figure 4.20 EOS of Auston switch with 200 pm generate-sample

spacing:

measurement

of top CPW slot;

measurement

of bottom slot.

Figure 4.21 Ti: sapphire

EOS measurement

of CPS sliding contact.

Figure 4.22 CRO measurement

of SI-GaAs.

Figure 4.23 Variation of EOS signal with probe height.

Figure 4.24 Background-free

autocorrelations:

measured

Ti: sapphire

trace;

x Gaussian

model; o sech2

model.

Table 5.1 Comparison of 3 mm alumina CPW S21 attenuation. Table 5.2 Comparison of 3 mm alumina CPW S21 phase.

Figure 5.1

Transmission

line components

of the photoconductive

switch.

Figure 5.2

Picture of UTF showing coax-CPW transition.

Figure 5.3

Schematic

of ANA.

Figure 5.4

Reference

planes

of two transition ANA measurements.

Figure 5.5

ANA S21

attenuation

measurement

of UTF1 and alumina

CPW.

Line lengths:

10 mm,

13 mm,

19 mm.

Figure 5.6

ANA S21

phase

measurement

of UTF1 and alumina

CPW.

Line lengths: 10 mm, 13 mm, 19 mm.

Figure 5.7 Re-plotted ANA S2, phase measurement of UTF1 and alumina CPW after

subtracting

linearities.

Line lengths:

-10

mm,

13 mm,

19 mm.

Figure 5.8 ANA S21 attenuation of GaAs lines: -- PG4, ---- TL3. Figure 5.9 ANA S21 phase of GaAs lines: - PG4, TL3.

(10)

Figure 5.10 Reference

planes

of single transition ANA measurements.

Figure 5.11 ANA S21'

attenuation

measurements

of UTF1:

de-embedded

single

transition and 5 mm CPW;

(double transition and 10 mm CPW).

Figure 5.12 ANA S21' phase measurements

of UTF1:

dc-embedded

single

transition

and 5 mm CPW;

(double transition and 10 mm CPW).

Figure 5.13 Modelled conduction loss a, for CPW lines.

Figure 5.14 Modelled dielectric loss ad for CPW lines.

Figure 5.15 Modelled radiation loss a, for CPW lines.

Figure 5.16 Modelled total attenuation factor a for CPW lines.

Figure 5.17 Modelled phase factor ß of CPW lines: small GaAs; large GaAs; alumina.

Figure 5.18 Re-plotted modelled change of phase per mm of CPW line, after

subtracting

linearities:

small GaAs;

large GaAs;

alumina.

Figure 5.19 Schematic

of photodiode

transmission

line measurement

system.

Figure 5.20 Recorded waveforms on oscilloscope: without UTF2; with UTF2 and 10 mm alumina CPW.

Figure 5.21 Recorded waveforms of GaAs circuits in UTF2: device TU (unannealed); device TL3 (annealed).

Figure 5.22 Attenuation result for UTF2 and 10 mm alumina line: deconvolved CRO; ANA.

Figure 5.23 Phase

result for UTF2 and 10 mm alumina

line:

deconvolved

CRO;

ANA.

Figure 5.24 Results of model for initial Gaussian

pulses

along GaAs CPW lines after

Figure 5.25 Figure 5.26 Figure 5.27 Figure 5.28 Figure 5.29

propagation distance: 0 mm, 1 mm, 2 mm. Results of propagation model for small GaAs CPW.

Results

of propagation

model for large GaAs CPW.

Results

of propagation

model for alumina

CPW.

Modelled effect of splitting taper into segments.

Example of EOS results showing

position

z from the generation

point:

z1 mm, FWHM=2.2ps; z=2mm, FWHM=4.8ps.

pulse evolution along GaAs line at

z= 0.3 mm, FWHM = 1.3 ps;

z= 1.5 mm, FWHM = 3.7 ps;

Figure 5.30 EOS results and propagation model along GaAs pulse generator, comprising a1 mm length of small GaAs CPW, a 0.5 mm taper and a 2 mm length of large GaAs.

Figure 5.31 EOS results and propagation model along alumina line.

Figure 5.32 EOS two-transition measurement

schematic.

Figure 5.33 Two-transition EOS waveform.

Figure 5.34 Derived single transition.

Table 6.1

Effect of filter on various parameters.

Table 6.2

Uncertainties

due to filter.

Table 6.3 Contributions to uncertainty in oscilloscope calibration. Table 6.4 Improvement in oscilloscope response.

(11)

Figure 6.1

Example of deconvolution:

effect of filter on various parameters

of the

deconvolved

result.

Figure 6.2 Example of deconvolution: filter 4 in the time-domain. FWl-1M = 9.4 ps, risetime = 5.4 ps, falltime = 5.4 ps.

Figure 6.3

Example

of deconvolution:

time-domain

results with filters 1-4.

Figure 6.4

Example

of deconvolution

in the frequency-domain:

deconvolved

result,

filter 4.

Figure 6.5 Measurement of jitter with oscilloscope histogram. Figure 6.6 SD32 impulse response. FWI M=7.7 +1.31-1.9 ps. Figure 6.7 SD32 step response. Risetime = 7.4 +1.6/-2.1 ps.

No tables or figures.

Appendix A

Table A. 1

Broadening

and bandwidth

of bias tees and attenuators.

(12)

I 1mI IR/L/Nr @ mow.

1.1 The sampling oscilloscope

1.1.1 History

In the early 1960s, a major advance was made by Hewlett-PackardI Rd 11 and Tektronix in improving the measurement of repetitive time-domain pulses and transients by the development of the sampling oscilloscope. This provided short duration time measurements by a method known as equivalent time sampling, where a single sample from a successive repetition of a train of similar pulses is captured on an instrument display, with the next sample being acquired and displayed at a slightly different time relative to the starting pulse, so building up a picture or waveform of the pulses in the time-domain. The advantage of such an instrument readily became apparent - the measurement time to acquire and display a waveform was decoupled from the actual duration of the pulses (for example, a train of nanosecond pulses could be acquired over milliseconds, the time corresponding to multiples of the pulse repetition frequency) - and the temporal resolution limit of the real-time cathode-ray oscilloscope was surpassed.

1.1.2 Recent developments

Sampling oscilloscopes

and electrical pulse generators

are now commercially

available

with bandwidths

greater than 50 GHz or risetimes

less than 7 ps. The drive behind the

development

of such

high-bandwidth

systems

has been rapid advances

made in the fields

of optoelectronics,

computing

and telecommunications.

Traceability

of such systems

to

national

standards

is important,

supporting

market sectors

whose emerging

technologies

rely on such systems

and encouraging

growth by the provision of a sound metrological

base.

Research

to provide electrical risetime measurements

traceable

to national standards

has

been active at the National Physical Laboratory (NPL) in the United Kingdom, the

National

Institute for Standards

and Technology

(NIST) - formerly the National Bureau

(13)

I nm wucnuN

of Standards

(NBS) - in the United States and other world class standards

laboratories.

It is worth emphasizing

that the provision of a facility to calibrate sampling

oscilloscopes

and pulse

generators

to specification

is not a trivial problem.

If a 50 GHz oscilloscope

has

a specified

risetime

of less than 7 ps, then in theory one requires

a risetime

measurement

capability

of 5±2 ps, 611 ps or 6.5 ± 0.5 ps etc.

Table 1.1 shows some of the oscilloscopes

available

in recent years and contrasts their

risetimes

with the level of calibration

NPL has been able to attain since starting a service

in 1988. The author of this thesis has been closely involved with the research work at

NPL since 1989. This text outlines the applied research which culminated in the improved 1994 facility, with NPL close to being able to calibrate a 50 GHz oscilloscope to specification.

Table 1.1 Recent history of oscilloscope risetimes and NPL calibration facilities.

Example

of

Typical Risetime

NPL Calibration facility

Oscilloscope

/ ps

year

response

/s

Tektronix S4

HP 1430A

<28

1988

25 t4

HP 54120

Tektronix SD26

<16

1990

18 f 3.5

HP 54121

Tektronix SD32

<7

1992

10: L2

1994

8±2

(14)

I INTROWCRON

1.2

Introduction to waveform metrology

A waveform - defined fully in the thesis terminology - is a measured pulse or transient. Metrology is the science of measurement. The core theme of this text is waveform metrology, where measurements are described, typically shorter than 20 ps, of pulses or transients associated with the development of standards to calibrate sampling oscilloscopes.

1.2.1 Impulse response

The performance of an oscilloscope is usually described by its response to one of two mathematical concepts: an electrical impulse, with infinitesimal short pulse duration; 21 or a Heaviside step, with infinitesimal short risetime. l'l

In theory, if an infinitesimal short pulse generator were available and connected

to an

"ideal" oscilloscope

- with perfect lossless

and distortion-free connectors

- then the

oscilloscope

would display such a function. A real oscilloscope

would, however, not

reproduce

the function perfectly, due to the inherent limitations of the oscilloscope

(and

indeed

any measuring

instr unent). The impulse

response

of the oscilloscope

describes

the

extent to which the instrument does not behave in an idealized manner. In this

hypothetical

case,

the oscilloscope

measurement

of the infinitesimal

pulse would define

the impulse

response

of the instrument.

In practice,

a pulse

generator

capable

of producing

an infinitesimal

pulse is not required.

As long as the pulse generator has a duration significantly shorter than the nominal

response

time of the oscilloscope,

then accurate characterisation

of the oscilloscope

is

possible.

However,

the technology

to make state-of-the-art

electrical

pulse generators

has

often been similar to that used to make state-of-the-art

oscilloscopes.

One example of

such a pair of instruments,

still much in use today, is the Tektronix S4 sampler

and S52

pulse generator. Throughout most of the history of the sampling oscilloscope,

the

temporal resolution of the best commercial electrical pulse generators has not been

(15)

I UrrawuCnci

significantly faster than the response

of oscilloscopes

of the same era. The current

situation is very similar. Although convolution techniques (addressed

later) can

compensate

to a certain extent, alternative

methods

are needed

to enable

the accurate

characterisation

of sampling

oscilloscopes

to provide traceability.

1.2.2 Optoelectronic approach

The pulsed electrical measurement system developed at the NPL uses a picosecond optoelectronic technique to generate electrical pulses that are faster than can be generated by purely electrical means. The fast electrical pulses are generated by illuminating photodiodes or photoconductive switches with femtosecond lasers. The resultant waveform recorded on an oscilloscope (CRO) is the convolution of the oscilloscope impulse response with the pulse generator signal, together with the response of the interconnecting transmission lines. The pulse generator signal is measured, independently of the CRO, using electro-optic or photoconductive sampling techniques with sub- picosecond resolution. The oscilloscope response is obtained by deconvolution of the test

signal from the recorded waveform, normally performed with associated windowing and filtering techniques.

The pulse generator used in the calibration system at the outset of this project was a

commercially

available

50 GHz Schottky

barrier photodiode,

1'l capable of producing 9 ps

pulses. Using such a system, the NPL established

facilities to calibrate sampling

oscilloscopes

and electrical pulse generators

with risetimes

down to below 10 ps or

bandwidths

of 35 GHz and above.

1'] To improve the temporal resolution of the system

and to reduce

the uncertainties

in the existing measurements,

a faster pulse generator

was

required.

It was to meet this, and other requirements,

that the pulse generator

project at

the NPL was initiated, on which some of this thesis is based.

To achieve the stated aim, various options were considered, such as advanced

photodiodes

and non-linear

transmission

lines.

l'1 However, the photoconductive

switch

appeared

to offer the simplest and most cost-effective

route to achieve

the target. This

(16)

I n«RODUCCION

switch

works on the principle

of changes

in the conductance

of a material,

induced

by the

injection

of a large number

(>1017

cm 3) of electron-hole

pairs. If the electron-hole

pairs

are produced by illumination with photons from a femtosecond

laser, and the carrier

characteristics

of the material are fast, then rapid changes

in the conductance

of the

material may be produced

which provide a mechanism

for a fast pulse generator.

1.3 Organisation of thesis

This introductory chapter concludes

in section 1.4 by introducing and defining some of

the terminology used in this thesis. The content and organisation of the rest of the thesis follows below.

The principle of the photoconductive

switch is investigated

in section 2.2 and a simple

model developed

(section 2.3). The relative merits of semiconductor

photoconductive

materials are discussed

in section 2.4 and the growth and properties of the favoured

material for waveform metrology, low-temperature

GaAs, are described

in sections 2.5

and 2.6 respectively.

Chapter 3

In section 3.2, design equations for coplanar transmission lines are discussed and photoconductive devices using such lines are designed (section 3.3) and fabricated

(section 3.4). The devices

are electrically

characterised

in section 3.5.

Photoconductive

switch measurement

configurations

are described

in section 4.2. The

theory of electro-optic sampling

(EOS) is summarised

in section 4.3, and EOS systems

with a dye laser (section 4.4) and a Ti: sapphire laser (section 4.5) are described.

Measurements

made with a sampling

oscilloscope

and the EOS systems

are explored

in

section 4.6 (dye laser) and section 4.7 (Ti: sapphire laser). The chapter concludes

by

(17)

I IM'RWUC ON

describing

the EOS system

limitations and deriving the response

of the photoconductor

(section 4.9).

Section S. 1 introduces the concept of de-embedding. A transmission line model is developed in section 5.2. In section 5.3, frequency-domain measurements of planar lines and transitions are performed with a network analyser, and the results compared with the model. Time-domain measurements of planar lines and transitions are also made with a sampling oscilloscope and the EOS system, and the results compared to the model (section 5.4). Using a two-transition measurement scheme and previous results in the chapter, the impulse response of a transition is derived and uncertainties are calculated (section 5.5).

Chapter 6

In section 6.2, a deconvolution technique and the uncertainties

associated

with it are

described

with the aid of an example.

The measurement

of jitter is described

in section

6.3, again with the aid of an example. Using the previous sections and the results of

chapter

4 and chapter 5, the response

of a sampling

oscilloscope

is determined

(section

6.4). The uncertainties

in the impulse and step response

are calculated

in section 6. S.

Chapter 7

The thesis concludes

with closing comments

and suggested

future work

Appendix A

Some results and remarks on the measurement

of bias tees and attenuators are

summarised.

1.4 Thesis Terminology

A key issue

in metrology is precision.

Because

of this, there is a need to be specific about

(18)

I n4 RcWCfl 4

definitions

and terminology.

1.4.1 Domains and FFT

This thesis uses the two domains most applicable in describing the electrical and

optoelectronics

work associated

with the calibration

of sampling

oscilloscopes,

namely

the time and frequency-domains.

Time-varying

changes

in electrical voltages are represented

by the electrical waveform

V(t). The frequency

spectrum, S(w), of the time-domain

waveform is defined as its

Fourier transformm21:

40

S(o) .f V(t) eýý''` s (1.1)

40

and conversely,

V(t) is defined

as the Fourier transform of S((j):

40

V(t)

.

2ir

fS() eM do

, (1.2)

where co is the frequency

in radians.

In practice, measurements

consist of discrete

numbers

of points defined within limited

ranges. Therefore,

discrete

transforms,

such as the Fast Fourier Transform (FFT), are

used to approximate the above integrals.

1.4.2 BSI/ IEC standards

Further details of some of the following terms and definitions are found in the relevant

standards

publications.

11

A wave is a modification of the physical state of a medium which propagates in that

medium as a function of time as a result of one or more disturbances.

Pulses and

(19)

I IMRwuCfON

transitions are included in the wave definition. A waveform is a manifestation,

representation

or visualization of a wave, pulse or transition. Put succinctly - the

measurement

process

yields a waveform from a (physical)

pulse.

A single pulse waveform (i. e. one that departs from, and then returns to, a nominal state) has a large number of terms associated with it. The pulse start time is defined as the instant specified by a magnitude referenced point, usually the mesial or 50 per cent point of the first transition. The pulse stop time is similarly defined for the last transition. The pulse duration is the duration between the pulse start and stop times. An alternative term for the pulse duration, used in this text, is the Full-Width-at"Half"Maximum (FWHM).

The proximal and distal points are usually specified to be at the 10 and 90 per cent reference magnitudes respectively. The first transition duration is the duration between the first proximal and distal points of the pulse transition. This thesis uses previous BSI

notation, and defines the "risetime" to be the first transition duration, as defined above, and the "falltime" to be the last transition duration

It should be noted that for comparison

purposes

it is occasionally

useful to quote the

proximal

and distal points defined

at 20 and 80 per cent respectively,

giving an alternative

transition duration. These

are clearly referred to as the 20%-80% risetime or falltime.

1.4.3 Definition of oscilloscope response

The expression

"measurement

of the response

of an oscilloscope"

is imprecisely

defined

and can include many possibilities.

Descriptions

such as "a 50 GHz oscilloscope"

are

frequently

used.

Whilst not incorrect, the use of single parameter

definitions

in either the

time or frequency-domains

can be misleading,

and may not be helpful to the user. Such

terminology can also encourage

manufacturers

to raise the published bandwidth. For

example, higher frequency components

can be tweaked to the detriment of lower

frequencies,

providing

an instrument

whose

time-domain

performance

is less well-behaved

than before the tweaking. National standards

laboratories

encourage

good practice by

(20)

I INiRwUCIlON

providing waveforms

which describe

more fully the performance

or response

of the

sampling oscilloscope than can be provided by parametric definitions. However,

parametric

definitions

can still be useful, providing the above is taken into account.

The risetime of an oscilloscope

is the single parameter

quoted by many to describe

the

step response

of an oscilloscope

to an Heaviside

step functioni'l input. The step response

is the integral of the impulse response,

as previously

defined.

For a Gaussian

impulse

response,

duration Tom, it can be shown °l that

-"1.089 (1.3)

TPWMI

where Z,, is the risetime (of the step response).

The bandwidth,

or -3 dB frequency,

of the oscilloscope

is defined

to be the frequency

at

which the power spectrum

decreases

by a factor of two from the d. c. value. The power

bandwidth should not be confused with the frequency at which the voltage drops by a

factor of two (sometimes

loosely referred to as the voltage bandwidth); the frequency

at

the -3 dB power point is equivalent to the frequency at the -6 dB voltage point.

For a Gaussian

impulse

response,

0.34 0.31

sK t

IPWMW

(1.4)

where

fo is the (power) bandwidth.

It is worth noting that such a relation depends

on the

shape of the response. Although a practical oscilloscope response often has a similar shape to a Gaussian, an exponential decay (RC time constant) is frequently assumed. For

an exponential

decay,

0.35

(1.5)

(21)

I INMOVUCf ON

where Tt is the risetime of the integrated

decay.

1.4.4 Convolution and deconvolution

Convolution is best described here in the context - fast waveform metrology - in which it is to be used. When an instrument such as a sampling oscilloscope is used to measure a time-domain pulse or transient, the recorded waveform, h(t), is not a true representation of the original pulse, at), but is affected by the non-perfect oscilloscope, represented by the system response. The signal fit) is convolved with the oscilloscope system response g(t), to provide the measured waveform h(t) recorded on the oscilloscope - see equation (1.6); x is a dummy variable. Convolution is ubiquitous in measurement as all measuring instruments have a finite system response or resolving limitation.

ob

h (t) " ff(x) g (t-x) dc (1.6)

The symbol 0 is used to represent

a convolution,

such that equation

(1.7) is equivalent

to equation (1.6):

h (ý) - f(t) 0g (t)

(t. 7)

Deconvolution

is the inverse of convolution. Deconvolution is required to recover the

desired

signal

from an instrument-limited

measurement

process.

In the example,

a known

oscilloscope

system

response

may be deconvolved

from the recorded data waveform to

obtain

the original signal. The result of jitter, noise and filtering on practical examples

of

deconvolution

is addressed

in chapter 6.

It is worth noting that in chapter 6 the application is reversed - the oscilloscope

system

response

is the desired

quantity,

which is found by deconvolving

a known pulse generator

signal from the recorded

data waveform

(22)

I INiRODUC110N

1.5 References to Chapter 1

1

Hewlett Packard

Co, "Time Domain Reflectometry",

Application Note 62, Palo

Alto, CA, USA, 1964.

2

R.

N. Bracewell,

"The Fourier

Transform

and Its Applications",

McGraw-Hill Inc,

1986.

3 P. E. Stuchert, "Pulse Standards: Basic Tools for Waveform Analysis", IEEE Trans. Instr. Meas. IM-31,1982, pp 192-198.

4

D. G. Parker, "Indium Tin oxide/GaAs Photodetectors for M llimetric-wave

Applications",

Electr. Lett., Vol. 22,1986, pp 1266-1267.

5 D. Henderson, A. G. Roddie and A. J. A. Smith, "Recent Developments in the Calibration of Fast Sampling Oscilloscopes", IEE Proc. A, VoL JA No. 5, Sept

1992, pp 254-260.

6 M. J. Rodwell and M. Kamegana, "GaAs Nonlinear Transmission Lines for

Picosecond

Pulse Generation

and Millimetre Wave Sampling", IEEE Trans.

4, No. 7, July 1991, pp 1194-1204.

7

British Standard guide to "Pulse Techniques

and Apparatus", BS-5698 BSI,

London, 1989 (identical to IEC 469.1).

8

D. Henderson, "Measurement

of the Temporal Response

of a Picosecond

Oscilloscope

by Optoelectronic

Techniques",

Ph.

D. Thesis,

University College

London, July 1989.

(23)

2 13ACKGROUND THEORY

2.1 Introduction

This chapter provides some theoretical and experimental background to the photoconductive switch. The principle of the photoconductive switch is first summarised and the principle further explored by the development of a simple model. Criteria to select a suitable photoconductive material - from which a pulse generator for metrology can be fabricated

- are explored, and after considering the criteria a semiconductor material, low- temperature (LT) GaAs, is chosen. The published properties of the material are summarised. Finally, the growth of LT-GaAs is described.

2.2 Principle of the photoconductive switch

A photodetector or optoelectronic converter is defined here to be a rectifying device

which converts

a.

c. light to d. c. current. Photodiodes

and photoconductors

are classes

of

photodetector. A photodiode consists of a semiconductor

junction (p-n, p-i-n, etc. )

operating under reverse bias. Details are provided in a wide range of literature.

UJ

A

photoconductor

usually consists

of two contacts separated

by a semiconductor

region

(Figure

2.1). Optical illumination of the semiconductor

material

results in the generation

of electron-hole

pairs, which increases

the conductivity of the material.

The conductivity o is given by:

Q"9(pen"NtP) . (2. l)

where n and p are the number densities of free electrons and holes, P. and µp their

respective

mobilities,

and q the electronic

charge.

A voltage source connected

across

the

two contacts drives a current through a load resistor. Changes

in optical illumination

produce

changes

in the conductivity of the semiconductor,

and thus change

the electrical

current generated

in the load. The optical illumination for ultrafast photoconductive

(24)

2 BACKGROUND 1 HEUK r

switches is usually provided by a laser, as an intense source with ultrafast changes in

illumination is required.

V

load

resistor

Figure 2.1 Simple photoconductor circuit.

A pulse generator suitable as a calibration source may have two alternative output shapes:

a pulse, starting and returning to zero amplitude; or a step, consisting of a rising edge

followed by a flat top. In practice, the output of a photoconductive step generator displays

a slow exponential decay in signal after the initial step. The application of step generators

to oscilloscope calibration has previously been addressed121 and this thesis concentrates on

developing a photoconductive impulse generator.

2.3 Modelling the photoconductive switch

2.3.1 Voltage considerations

A model for the voltage produced by a photoconductive switch can initially be obtained using a quasi-stationary treatment. The photons illuminating the semiconductor are all assumed to absorb uniformly within the thickness of the semiconductor active layer, except for the photons which are reflected.

24

(25)

2 DACKGROU D TI WOR?

Illumination of the semiconductor

with a modeloeked

laser generates

N` free carriers

(electron-hole

pairs) per optical pulse:

Ns - rý " f p'" hu . (1-R)"(1-. "4) (2.2)

where q is the quantum efficiency for production of free carriers, P,,, is the average optical power, f, is the repetition frequency of the laser, by is the energy of one photon, R is the optical reflectivity, a. is the optical absorption coefficient, and d the thickness of the semiconductor layer. The generated carrier density ng is determined from

nN t (2.3)

ldw

where 1 is the gap separation and w is the gap width.

For example, assuming r=1, an illumination of 5 mW at 800 nm and 80 MHz onto a

2 pm thick GaAs layer produces a value of N. = 1.5 x 108. If the optical beam diameter

is 20 pm then ng = 2.4 x 10" cm 3. This is quite a significant value, larger than typical

doping levels, and so may be expected

to alter the properties

of the material.

The photo-induced change in conductivity in the semiconductor can be estimated by substituting equation (2.3) into equation (2.1), assuming µb « µQ and N=P for excitation levels greater than the intrinsic doping. The resistance across the switch, ý, is calculated from the conductivity:

R 1. ý2

.

1. jo dw

qµß tý

hu

(2.4)

In the example, the above terms are known except the electron mobility µa A simple

equivalent circuit of the photoconductive

switch is shown in Figure 2.2. Zo is the

impedance

of the transmission

line before and after the switch, F., is the total metal-

semiconductor

contact

resistance

in the circuit, Ra(t) is the gap or switch resistance

(which

will later be described

as a function of time), and C. is the capacitance

of the gap. The

(26)

2 BACKGROUND 71 CORY

circuit acts as a potential divider such that the switched

voltage V(t) is given by

Z V(r) . tip` "

2Z@. R. R, (1)

where Vb is the d. c. bias

voltage.

If it is assumed that a switching efficiency of 5% of the bias voltage enables accurate sampling oscilloscope

Zo

Rg(t)

vb I

(2ä)

Zo

Figure 2.2 Equivalent circuit of photoconductive switch.

Rc

V(t)

and electro-optic

sampling analysis (e. g. a 10 V bias produces a 20 mV photoconductively-generated peak), then for typical 50 A geometry, R, and RQ(t) must together be lower than approximately

900 Q. Usually F, « Ra(t). To achieve such a gap resistance, a minimum intensity of

optical illumination

and gap length 1 are defined,

given the material's

mobility.

The above quasi-stationary treatment enables a change of switch resistance from a known number of incident photons to be estimated in the static case. The photoconductive switch is to be used to generate ultrafast electrical pulses from ultrafast optical pulses provided by the laser. Therefore, the factors which affect the speed of performance must also be discussed.

2.3.2 Speed considerations

The bulk photoconductor shown in the previous section (Figure 2.1) is ideal for low- speed, high-power applications. However, if ultrafast changes in photoconductivity are to be used to produce fast electrical pulses then an alternative faster geometry is required,

such as the coplanar transmission lines introduced and described in chapter 3. Coplanar photoconductive devices can be fabricated from semiconductor substrates or substrates

(27)

2 aAQCCRWND n ffCRY

with appropriate

active semiconductor

layers,

usually on the substrate

top. Suitable

fast

semiconductor materials are discussed in section 2.4.

The coplanar photoconductive switch consists a pattern of metallisation deposited on the top of the semiconductor. Various geometries are possible, including the coplanar waveguide sliding contact, coplanar waveguide series-gap, and the coplanar striplinc sliding contact, referenced, discussed and measured in chapter 4. All the devices used in this thesis assume complete optical illumination across the gap in the metallisation defined

on the semiconductor. Alternative photoconductive mechanisms such as the non-uniform illumination or covered-gap technique'31, where fast pulses are obtained from a partially- illuminated gap across a slow semiconductor, are not further discussed here.

Two properties which affect the temporal response of a photoconductor are the dielectric relaxation time and the free carrier lifetime. Given an infinitely short optical excitation, electron-hole pairs in the semiconductor are generated extremely quickly, in the short time

it takes for particles to separate physically. The field distribution, and hence conductivity, do not simultaneously change since initially the space charge of the electrons and holes are neutralised. Drift in opposite directions to the applied field creates a space charge field. The dielectric relaxation time, rd, is defined as the time taken for the space charge dependent field in the photoconductor to evolve and is a complicated function of the semiconductor, geometry and illumination. t1

The photo-generated carriers recombine at a rate given by the free carrier lifetime, z&, causing a corresponding decrease in photoconductivity. The free carrier lifetime of a semiconductor depends on the semiconductor and the recombination mechanism. For example, impurities can act as recombination centres by trapping free carriers and shortening the lifetime. The decay time depends on the type and cross-section of the impurity, but the decay is non-radiative. Such a recombination is frequently used when ultrafast photoconductive switches are required.

Two further recombination

mechanisms

are summarised

below, but are not as important

(28)

2 1ACKGROUND 11 ECRY

for the operation of an ultrafast photoconductor. Radiative recombination, or luminescence, involves the excess energy being given up by emitting photons. Such a process is relatively slow, often in the order of tens of nanosecond. )51 Another non- radiative (but slow) carrier decay mechanism is three-particle Auger recombination. The excess energy raises other free carriers to higher states in their bands which subsequently relax by the emission of phonons. 15'

Other factors which affect the temporal response of the photoconductor include the

parasitics

associated

with the switch geometry

(estimated

in chapter 4) and the ability of

the transmission

line to propagate fast pulses (estimated

in chapter 5).

Returning to equations (2.4) and (2.5), the quasi-stationary approximation to the switched voltage can be extended to apply to the fast photoconductor. The switch resistance was calculated from the energy of one optical pulse. As a first approximation, this resistance can be multiplied by the ratio of the optical pulse duration to the free carrier lifetime, providing a value for the average switch resistance over the duration the switch is "closed". an effect this adds tifr to the denominator of equation (2.4) and replaces P,,, and f with the peak power of the optical pulse. )

A useful figure of merit for photoconductors

is the lifetime-mobility product, 1s' which

describes

the sensitivity

of the photoconductor

to photoexcitation.

In the above paragraph,

the estimated

switch resistance

is inversely

proportional to this product.

In summary, the risetime of a pulse generated by a photoconductor depends mainly on the

rising edge

of the optical excitation

and td, and the falltime depends

mainly on the falling

edge of the optical pulse and zf,.

2.4 Photoconductive material selection

The following properties are important in the selection of a semiconductor material

(29)

2 DACKGROUNU III MY

suitable for use in a metrological

photoconductive

switch: band-gap;

wavelength;

free

carrier lifetime; mobility, responsivity, contacting and ageing.

The band-gap, E., of a semiconductor

is the energy separating the bottom of the

conduction band and top of the valence band. The optically-induced

generation

of

electron-hole pairs in an intrinsic semiconductor

requires incident photons to have

sufficient energy to transfer an electron or hole between the two bands. The availability

of a laser with suitable

wavelength

is therefore an important consideration

in the design

Table 2.1 Some typical photoconductive semiconductors.

Band-gap Equivalent Free Carrier Estimated Semiconductor Es Wavelength Lifetime ti f, Mobility

e A Mn s em2Ns

Cr-doped

1.42

870

50 - 200

1000

GaAs

MBE LT-

1.42

870

<1

200

GaAs

Amorphous

1.12

1110

1-10

1

Si

Ion-damaged

1.12

1110

<1

20

SOS

MOVPE 1.56 800 <1 150

CdTe

of photoconductive

switches. Table 2.1 shows examples of some semiconductors

previously

utilised for fast photoconductive

switches

along with various properties.

The

equivalent wavelength

defines the cut-off wavelength above which the photons have

insufficient energy for absorption in the semiconductor. Below the wavelength, the

number

of photons absorbed

is estimated

in the previous section.

(30)

2 nA(XCRCUND 11 JEORY

Many materials, included those in Table 2.1, have sub-picosecond dielectric relaxation times. However, specialised semiconductor growth techniques are needed to achieve sub- picosecond recombination lifetimes, r f, Such techniques introduce recombination centres

or traps into the semiconductor by various methods, including: doping (Cr-doped GaAs); '61 the use of grain boundary defects (amorphous Si); t71 ion-implantation damage (silicon-on sapphire); '81 epitaxial growth (CdTe); ' 1 or by low-temperature epitaxial growth (LT-GaAs). Properties of LT-GaAs are described in section 2.5.

In addition to time-resolved carrier dynamics, the responsivity of a photoconductive device is an important consideration. The pulse amplitude needs to be sufficient to provide adequate signal-to-noise in the metrological application. Factors which affect the responsivity include the semiconductor mobility, resistivity, and contact resistance, as

shown in the previous section.

Mobility is an important

consideration

for charge transport because

it describes

the effect

an applied

electric

field has on the motion of an electron or hole. A material with a higher

mobility will, given similar device conditions, produce pulses of larger amplitude. An

unfortunate consequence

of the introduction of traps/recombination

centres in many

materials

is the subsequent

decrease

in mobility. Materials which maintain a relatively high

mobility and short free carrier lifetime are therefore ideal.

The interface, or contact between a semiconductor and metal has been the subject of much research. '101 The ohmic contact can be defined as a contact with a linear I-V characteristic, that is stable in time and temperature, and contributes as little parasitic resistance as possible. This ideal contact is not always possible to fabricate. Placing a metal on a wide band-gap semiconductor, such as GaAs, depletes a region of the semiconductor (beneath the metal) of carriers, producing a rectifying junction known as a blocking or Schottky contact. The I-V characteristic of such a junction is non-linear, as the applied voltage can alter the depth of the depletion region.

Most semiconductor

devices

require

an ohmic contact for effective operation unless non-

(31)

2 UAaCGROUND 11 M MY

ohmic behaviour

is particularly advantageous.

For a photoconductive

device which is

transit-time-limited

- i. e. when the free carrier lifetime is much longer than the time of

travel between

the two contacts or electrodes

- then ohmic contacts

will decrease

the

series

resistance,

R,,, of the device, and in the external circuit produce higher-amplitude

pulses.

For devices in this thesis, where the free carrier lifetime is shorter than the transit-time, some carriers will reach one electrode and must be replaced by carrier injection from the other electrode. An ohmic contact is more efficient at carrier replacementts1 and therefore

increases the device responsivity, although careful consideration is required further to define the relative merits of the ohmic contact. This is not further discussed here.

One further property to consider is ageing. It has been found with some silicon-on- sapphire devices that ion-induced damage can vary significantly over time-periods of months. There is no evidence to suggest LT-GaAs suffers similar ageing problems. In addition to this, some contact metallurgies have been found to be unstable over similar time scales. Clearly such factors require consideration in choosing a suitable photoconductor for metrological application.

Considering

all the above

factors,

and referring back to Table 2.1, it was decided

to grow

LT-GaAs as a photoconductive

material, due to its published

fast carrier recombination

time, relatively high mobility and expected

long-term performance

stability in a switch.

2.5

Properties of LT-GaAs

MBE growth of GaAs is usually performed at a substrate

temperature

of around 600 °C.

It has been found, however, that GaAs grown at lower temperatures (LT-GaAs) has some useful properties. LT GaAs was first grown as a buffer layer to eliminate side-gating and back-gating effects in GaAs MESFET devices, taking advantage of the high resistivity of the annealed material. 1111 When initially used as the photoconductive material in a

Figure

Table 1.1 Recent history of oscilloscope risetimes and NPL calibration facilities.
Figure 2.1 Simple photoconductor circuit.
Table 2.1 Some typical photoconductive semiconductors.
Figure 2.3 Structure of LT-GaAs wafer.
+7

References

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