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IDENTIFICATION AND CHARACTERIZATION OF E, Z ISOMERS FOR ACID DEGRADENTS OF SECONDARY ALCOHOL IN API BY HS/GC/ EI MS

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Figure

FIG.1: SCHEMATIC REPRESENTATION OF 1-ENE, E ISOMER AND Z ISOMER FORMATION.
FIG. 4: CHROMATOGRAM SHOWING DEGREDENTS OF 2-BUTANOL IN PRESENCE OF DMSO AND  SULPHURIC ACID BY GC-HS
FIG. 8: MASS SPECTRUM OF 2-BUTANOL DEGREDENT (Z) BUT-2-ENE ELUTING AT RT 7.8 MINUTE.
FIG. 11: ACTIVE PHARMACEUTICAL INGREDIENT TIC SHOWING ABSENCE OF DEGREDENT PEAKS
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