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One Step Synthesis of Titanium Oxyhydroxy Fluoride Rods and Research on the Electrochemical Performance for Lithium ion Batteries and Sodium ion Batteries

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Figure

Fig. 1 XRD pattern of titanium oxyhydroxy-fluoride. The HTB structural frame is shown as inlet
Fig. 3 SEM images of titanium oxyhydroxy-fluoride, TiO0.9(OH)0.9F1.2 · 0.59H2O with different morphologies: long rods (a), short rods (b) and hexagonalrods (c); TEM image (d), HRTEM image (e) and the corresponding FFT image (f) of long TiO0.9(OH)0.9F1.2 · 0.59H2O rods; the arrows in the HRTEM image(e) indicate the 0.38 nm interfringe spacing, and the arrows in the corresponding FFT image (f) indicate the spots which represent different latticeplanes of the product
Fig. 5 a Charge and discharge curves of TiO0.9(OH)0.9F1.2 · 0.59H2O for SIBs in the potential range of 2.9–0.5 V; several selected cycles are shownfor clarity; b first discharge curve of TiO0.9(OH)0.9F1.2 · 0.59H2O in the potential range of 2.9–0.05 V; c the former 5 cycles of hexagonal TiOF2 half-cell for SIBs; all the half-cells are performed at 25 mA g−1; d cycling performance of TiO0.9(OH)0.9F1.2 · 0.59H2O for SIBs; and e rate capacity of oneTiO0.9(OH)0.9F1.2 · 0.59H2O half-cell for SIBs between 2.9 and 0.5 V, different current densities are labeled

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