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Measuring 19F shift anisotropies and 1H–19F dipolar interactions with ultrafast MAS NMR

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Figure

Figure 1. 19F MAS spectra of PVDF, recorded at a Larmor frequency of 564.7 MHz. Experimental spectra for
Figure 2. (a) shows a 19F anisotropic-isotropic correlation spectrum of PVDF recorded at a Larmor frequency
Figure 3. SIMPSON simulations of 19F CSA lineshapes recoupled using a  R1254 sequence for a 1H – 19F spin
Table 1. Values of 19F chemical shift parameters in PVDF (with 95% confidence limits) measured in this work
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