3.2 to 3.4 eV
![4′ (4 Chlorobenzoyl) 1′ methyldispiro[indole 3(2H),2′ pyrrolidine 3′,3′′(2′′H) indole] 2,2′′ dione](data:image/gif;base64,R0lGODlhAQABAIAAAP///wAAACH5BAEAAAAALAAAAAABAAEAAAICRAEAOw==)
4′ (4 Chlorobenzoyl) 1′ methyldispiro[indole 3(2H),2′ pyrrolidine 3′,3′′(2′′H) indole] 2,2′′ dione
... isatin (indole-2,3-dione) (1 mmol), and sarcosine (N-methylglycine) (1 mmol) was refluxed in aqueous methonal for 3 h. On completion of the reaction the solvent was evaporated in vacuo and the resulting crude ...
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4′ (4 Methoxyphenyl) 1 methylchroman 3 spiro 3′ pyrrolidine 2′ spiro 2′′ indan 4,1′′,3′′ trione
... A solution of 3-p-methylbenzylidene-4-chromanone (0.5 mmol), ninhydrin (0.5 mmol) and sarcosine (0.5 mmol) in aqueous methanol (20 ml) was refluxed until the disappearance of the starting material. The ...
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4′ (4 Bromobenzoyl) 1′ methyldispiro[indole 3(2H),2′ pyrrolidine 3′,3′′(2′′H) indole] 2,2′′ dione
... isatin (indole-2,3-dione) (1 mmol), and sarcosine (N-methylglycine) (1 mmol) was refluxed in aqueous methonal for 3 h. On completion of the reaction, the solvent was evaporated in a vacuum and the resulting crude ...
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4′ (4 Methylbenzoyl) 1′ methyldispiro[indole 3(2H),2′ pyrrolidine 3′,3′′(2′′H) indole] 2,2′′ dione
... isatin (indole-2,3-dione) (1 mmol), and sarcosine (N-methylglycine) (1 mmol) was refluxed in aqueous methanol for 3 h. On completion of the reaction the solvent was evaporated in a vaccum and the resulting crude ...
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N (3 Chlorophenyl) 2 cyano 3 (4 hydroxy 3 methoxy 2 nitrophenyl)prop 2 enamide
... To a solution of 4-hydroxy-3-methoxy-2-nitrobenzaldehyde (1.0 g, 5.1 mmol) and N-(3-chlorophenyl)-2-cyanoacetamide (1.0 g, 5.2 mmol) in acetonitrile (10 ml), 1 drop of piperidine and ...
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(E) 3 (4 Methylphenyl) 3 [3 (4 methylphenyl) 1H pyrazol 1 yl] 2 propenal
... 1.360 (2) Å, which are shorter than a C—N single bond length of 1.443 Å, but longer than a double bond length of 1.269 Å, (Jin et al., 2004), indicating electron delocalization. The pyrazole ring A and ...
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4 [3 Benzoyl 4 (4 chlorophenyl) 1 methylpyrrolidin 2 yl] 1 (4 methoxyphenyl) 3 phenylazetidin 2 one
... A solution of cis-4-formyl-2-azetidinone (1 mmol), sarcosine (1 mmol) and chlorochalcone (1 mmol) was refluxed in toluene (15 ml) using a Dean–Stark apparatus. The completion of the reac- tion was evidenced ...
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4′ (4 Methoxybenzoyl) 1′ methyldispiro[indole 3(2H),2′ pyrrolidine 3′,3′′(2′′H) indole] 2,2′′ dione
... isatin (indole-2,3-dione) (1 mmol), and sarcosine (N-methylglycine) (1 mmol) was refluxed in aqueous methonal for 3 h. On completion of the reaction the solvent was evaporated in a vacuum and the resulting crude ...
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Crystal structures of (E) 3 (4 hydroxybenzylidene)chroman 4 one and (E) 3 (3 hydroxybenzylidene) 2 phenylchroman 4 one
... Compound II was synthesized according to the procedure described by Pijewska et al., (1993). A mixture of 2-phenyl- chroman-4-one (0.01 mol), 3-hydroxybenzaldehyde (0.01 mol) and five drops of ...
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5′′ Benzylidene 1′ methyl 4′ phenylindole 3 spiro 2′ pyrrolidine 3′ spiro 3′′ piperidine 2(3H),4′′ dione
... A mixture of dipolarophile (dibenzylidine-N-methylpiperidone), isatin and sarcosine was re¯uxed in aqueous methanol until the starting materials had disappeared (about 3±4 h), as evidenced by thin-layer ...
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(E) 4 (4 Hydroxy 3 methoxyphenyl)but 3 en 2 one
... 4-Hydroxy-3-methoxybenzaldehyde (3.04 g, 20 mmol) was dissolved in 25 ml of acetone and 12 ml of dilute aqueous NaOH solution (10%) was added to the acetone solution with stirring. The mixture was allowed ...
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4 Hydroxy 3 [(4 hydroxy 2 oxo 2H 3 chromenyl)(3 thienyl)methyl] 2H chromen 2 one
... To a well-stirred solution of 4-hydroxycoumarin (6.17 mmol, 1.0 g) in ethanol (10 ml) containing two drops of acetic acid, thiophene-3-carboxaldehyde (3.1 mmol, 0.345 g) was added. The reaction mixture was ...
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Crystal structure of 2 (4 chlorophenyl) 3 (4 methoxyphenyl) 3 (methylsulfanyl)acrylonitrile
... (C C—C N) is planar to within 0.003 (2) A ˚ , with the S atom and the methyl C atom displaced from this plane by 0.2317 (6) and 0.637 (2) A ˚ , respectively. In the crystal, molecules are linked via pairs ...
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1 [3 (Morpholin 4 yl)propyl] 3 [(naphthalen 2 yl)oxy] 4 (3 nitrophenyl)azetidin 2 one
... N3 0.0670 (17) 0.0656 (16) 0.0528 (13) −0.0176 (12) −0.0016 (12) −0.0164 (11) C1 0.084 (2) 0.074 (2) 0.0428 (15) −0.0215 (19) −0.0004 (16) −0.0171 (15) C2 0.071 (2) 0.086 (2) 0.0449 (15) ...
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4 (3 Methoxyphenyldiazenyl) 2 methylphenol
... used to solve structure: SHELXS97 Sheldrick, 1997; programs used to refine structure: SHELXL97 Sheldrick, 1997; molecular graphics: ORTEP-3 for Windows Farrugia, 1997; software used to p[r] ...
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SYNTHESIS, SPECTRAL AND THEORETICAL CHARACTERIZATION OF 5,6-DICHLORO/DIMETHYL-2-(2´,3´/2´,4´/2´,5´/3´,4´/3´,5´-DIMETHOXYPHENYL)-1H-BENZIMIDAZOLES
... Various benzimidazole derivatives display a wide range of biological activity. For instance, vitamin B12 has 5,6-dimethylbenzimidazole moiety as coordinated to the Co(II) ion [1,2]. On the other hand, various drugs and ...
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4 (2 Benzoylhydrazinothiazol 4 yl) 3 phenylsydnone
... To a stirred suspension of 4-bromoacetyl-3-phenylsydnone (2.83 g, 0.01 mol) in absolute ethanol (20 ml) was added a solution of 1- benzoyl thiosemicarbazide (1.9 g, 0.01 mol) in absolute ethanol (20 ml) and ...
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(Z) Ethyl 3 (4 chlorobenzamido) 2 cyano 3 (4 fluorophenyl)acrylate
... Cl1 0.0849 (7) 0.0965 (7) 0.1095 (8) 0.0329 (6) 0.0085 (6) 0.0214 (6) F1 0.226 (3) 0.0791 (16) 0.0970 (18) 0.0063 (18) −0.0458 (19) 0.0293 (14) N1 0.0694 (18) 0.0653 (16) 0.0443 (14) 0.0139 (14) 0.0072 (13) 0.0055 ...
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2 [1 (4 Bromophenyl) 3 hydroxy 3 (4 methoxyphenyl)propyl]cyclohexanol
... C13 0.045 (2) 0.075 (3) 0.046 (2) −0.0012 (19) 0.0297 (19) 0.0007 (19) C14 0.053 (2) 0.058 (2) 0.048 (2) 0.0022 (19) 0.033 (2) 0.0056 (18) C15 0.053 (2) 0.062 ...
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3 Mesityl 2 oxo 1 oxaspiro[4 4]non 3 en 4 yl 2 (4 chlorophenyl) 3 methylbutyrate
... Data collection: PROCESS-AUTO (Rigaku, 1998); cell refine- ment: PROCESS-AUTO; data reduction: CrystalStructure (Rigaku/ MSC, 2002) and Larson (1970); program(s) used to solve structure: SIR97 (Altomare et al., 1999); ...
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