Phosphorus-31 NMR spectroscopy
P 31 nuclear magnetic resonance spectroscopic study of obstructive uropathy in the rat
... (NMR) spectroscopy of the rat kidney with ureteral ligation resulted in a rapid and major increase in a peak resonating at ...Further NMR studies performed with in vivo kidneys and tissue extracts ...
7
H NMR, 13 C NMR, 31 P NMR and Mass spectroscopy and investigated their antimicrobial activity.
... reaction was monitored by TLC and product was purified by column chromatography using hexane: ethyl acetate (70:30) as an eluent, gummy oily product was obtained, scratched it in hexane at 0ºC to obtained a white solid ...
6
Effects of thyroid hormones on skeletal muscle bioenergetics In vivo phosphorus 31 magnetic resonance spectroscopy study of humans and rats
... The pathophysiology of the myopathy in dysthyroid states is poorly understood. We therefore tested the effects of thyroid hormones on muscle bioenergetics in humans and rats, using in vivo 31P NMR. Two hypothyroid ...
8
The clinical use of nuclear magnetic resonance spectroscopy for studying human muscle metabolism.
... For 31 P-NMR investigations, great benefit is obtained from the fact that most surface tissues do not contain detectable amounts of phosphorus metabolites, and simple muscle studies can[r] ...
15
Linking the depletion of rhizosphere phosphorus to the heterologous expression of a fungal phytase in Nicotiana tabacum as revealed by enzyme labile P and solution 31P NMR spectroscopy
... each in 5 mL distilled water) to blank extract samples, prepared in the same manner as all other soil extracts. Compounds from Sigma-Aldrich included phytic acid dodecasodium salt hydrate (myo- InsP6; P3168), D ...
32
Protein Ligand Interactions by NMR and EPR Spectroscopy
... available NMR data thus indicate that a structural change occurs between substrate-free and glutamate-bound DEBP, which involves a displacement of the small and large domains of the protein relative to each ...
206
Quantification of Valsartan by Uv-Visible and NMR Spectroscopy.
... Standard analytical techniques are not available in the pharmacopoeias for newer drugs. So it becomes necessary to develop new analytical techniques for the newer drugs. Valsartan is one of the new drugs launched ...
86
Recent applications of NMR spectroscopy in plant metabolomics
... heteronuclear NMR for a true metabolomics approach has recently been published ...HSQC-type NMR experiment to track changes in N-containing metabolites during the onset of ...
7
Species and Bio-Availability of Inorganic and Organic Phosphorus in Primary, Secondary and Digested Sludge
... Turner. B.L. Optimizing phosphorus characterization in animal manures by solution phosphorus‐ 31 325. nuclear magnetic resonance spectroscopy. J[r] ...
11
Weinrich, Sabine (2003): Tri(alkyl)silylsubstituierte Pentelide und Penteldiide der ersten und dritten Hauptgruppe. Dissertation, LMU München: Fakultät für Chemie und Pharmazie
... den 31 P-NMR-Spekteren ...protonenentkoppelten 31 P- NMR-Spektrum ein ...im 31 P-NMR-Spektrum durch die doppelt negative Ladung am Phosphoratom eine starke Verschiebung zu tiefem ...
205
Exploiting NMR spectroscopy for the study of disorder in solids
... predict NMR parameters for a structure or structural ...solid-state NMR community since the advent of approaches able to calculate NMR parameters for periodic systems, ...unexpected NMR ...
135
More Insight on Structure of New Binary Cerium Borate Glasses
... DOI: 10.4236/njgc.2018.81002 14 New Journal of Glass and Ceramics used of 0.5 - 1.0 ms with a pulse delay of 2.5 s, and an accumulation of 200 - −300 scans. All Samples were grinded to fine powders then filled into ...
10
Combining Sustainable Synthesis of a Versatile Ruthenium Dihydride Complex with Structure Determination Using Group Theory and Spectroscopy
... Student instructions, laboratory teacher notes, and the list of questions used in the structural analysis are included in the supporting information along with information about the course in Sheffield, greater detail ...
13
Translucent Voices: Creating Sound Pedagogy And Safe Spaces For Transgender Singers In The Choral Rehearsal
... diverted from landfills (10 to 100% diversion). Figure 3.10 shows the average percentages of nitrogen and phosphorus fertilizers that can be replaced with nutrients available from the hydrochar. Table 3.3 presents ...
78
New technology acquisition 3α,14α,22r,25-tetrahydroxy-5α(H)-cholest-7-en-6-one and biological research anti-inflammatory activities
... Research NMR spectrscopy and biological ...to NMR spectroscopy, mass spectrometry, and microanalysis, the structure of 3α,14α,22R,25-tetrahydroxy-5α(Н)-cholest-7-en-6-one ...to NMR ...
5
Perspective : current advances in solid state NMR spectroscopy
... with NMR spectroscopy in the solid state will remain the subject of ongoing research effort and technological ...for NMR, and for solid-state NMR in ...solid-state NMR will continue to ...
27
Protein folding on the ribosome studied using NMR spectroscopy
... NMR spectroscopy is a powerful tool for the investigation of protein folding and misfolding, providing a characterization of molecular structure, dynamics and exchange processes, across a very wide range of ...
20
Studies of high molecular weight systems by NMR spectroscopy
... In this situation, O-tert-butyltyrosine (Tby) provides an exceptional solution to address many of the issues associated with structural studies of high-molecular weight systems by NMR spectroscopy (Chen et ...
144
Design of New Scaffolds for Peptidic Foldamers and Their Structural Studies Using NMR Spectroscopy
... In the present chapter we have investigated the oligomers 4.1-4.6 of β 3 -Caa derived from Allose sugar, with alternating L-Ala, in anticipation to result in novel secondary structures. The structural properties of these ...
12
Solid-State NMR Spectroscopy of Unreceptive Nuclei in Inorganic and Organic Systems
... sample) NMR spectra were acquired at both moderate and ultra-high magnetic field strengths ...anisotropic NMR interactions. There are very few reports of 115 In MAS NMR in the literature; 29,32,36,37 ...
352