3.4 to 4.2 GHz

Top PDF 3.4 to 4.2 GHz:

Design and Characterization of a 5 2 GHz/2 4 GHz Fractional  Frequency Synthesizer for Low Phase Noise Performance

Design and Characterization of a 5 2 GHz/2 4 GHz Fractional Frequency Synthesizer for Low Phase Noise Performance

the ΣΔ modulator. The ΣΔ noise shaping can be modeled as a linear gain stage with an additive quantization noise source, which is shaped by a highpass transfer function. Hence, the quantization error component at the synthesizer output is composed of mostly high-frequency noise that can be fil- tered by the PLL. A block diagram of a typical ΣΔ modulator that is widely used in synthesizer applications is shown in Figure 3 [3]. This three-loop sigma-delta topology is called a MASH 1-1-1 structure, because it is a cascaded ΣΔ struc- ture with three first-order loops. Each of the three loops is identical. The input of the second loop is taken from the quantized error E q1 of the first loop, while the input of the
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A Survey on Interference Mitigation Techniques for 2 4 GHz ISM Band

A Survey on Interference Mitigation Techniques for 2 4 GHz ISM Band

technique to mitigate interference in the environment. From various study, it is found that usage of common spectrum suffers from interference and effective interference mitigation mechanism is needed for the co-existence of WPAN and WLAN [1] [2] [3]. In order to support the co- existence of WPAN and WLAN devices, various researchers have proposed various interference mitigation techniques. This paper aims to explore some of the notable interference mitigation techniques proposed by the researchers for the effective design and implementation of Mobile Adhoc Network.
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MIMO Reconfigurable Antennas for Wi Fi 2 4 GHz Communication

MIMO Reconfigurable Antennas for Wi Fi 2 4 GHz Communication

The most common and frequent use of local wireless communication is Wi-Fi technology for the purpose of accessing any type of document, audio, video from Internet through smartphones, tablets or laptops. From 2018 to 2019, there is a rapid 82% increase in mobile data traffic as number of smartphone users are growing in India and China [2]. A significant portion of this mobile traffic is generated in indoor environments or in short range communications with the help of Wi-Fi.Due to emergence of various new applications, the consumption of traffic is growing rapidly. But to accommodate this high demand of data traffic from many users the corresponding data rate should also be high requiring more of scarce resources like spectrum and energy. Keeping the user’s demands of increased data rate and low frame error rate for 3G and 4G communication in mind, the enabling technology behind Wi-Fi which is IEEE 802.11ax needs to enhance the information rate and area throughput in highly populated Wi-Fi zones [3].
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QuickSpecs. At A Glance. HP Integrity rx Server. Overview

QuickSpecs. At A Glance. HP Integrity rx Server. Overview

A9738A–Supports from 4 to 16 DIMMs (1- to 64-GB); 12.8 GB/s memory bandwidth A9739A–Supports from 4 to 32 DIMMs (1- to 128-GB); 12.8 GB/s memory bandwidth Both memory carrier boards provide the same bandwidth to the CPUs. The primary difference between the two boards is in total memory capacity.

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N [4 Cyano 3 (tri­fluoro­meth­yl)phen­yl] 3 (4 fluoro­phenyl­sulfon­yl) 2 hydr­­oxy 2 methyl­propionamide

N [4 Cyano 3 (tri­fluoro­meth­yl)phen­yl] 3 (4 fluoro­phenyl­sulfon­yl) 2 hydr­­oxy 2 methyl­propionamide

Sheldrick, G. M. (1997). SHELXS97. University of Go¨ttingen, Germany. Sepp-Lorenzino, L. & Slovin, S. (2000). Expert Opin. Ther. Pat. 10, 1833–1842. Tetsuya, S., Tadashi, K. & Nobushige, I. (2003). US Patent 2003 191 337. Tucker, H., Crook, J. W. & Chesterson, G. J. (1988). J. Med. Chem. 31, 954–959. Thurlow, R. J. (1998). Emerging Drugs, 3, 225–246.

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2 (Biphen­yl 4 yl) 3 (4 meth­oxy­phen­yl) 1,3 thia­zolidin 4 one

2 (Biphen­yl 4 yl) 3 (4 meth­oxy­phen­yl) 1,3 thia­zolidin 4 one

4-Methoxyaniline (5 g, 1 mol), 4-biphenylcarboxaldehyde (7.39 g, 1.0 mol) and anhydrous -ferrite (12.96 g, 2 mol) were refluxed with constant stirring in dry benzene for 30 min, after which thioglycolic acid (2.82 ml, 1 mol) was added to the reaction mixture. Reflux and

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3 (2 Amino­ethyl) 2 (4 fluoroanilino)­quinazolin 4(3H) one

3 (2 Amino­ethyl) 2 (4 fluoroanilino)­quinazolin 4(3H) one

To a solution of 2-ethoxycarbonyliminophosphorane (1.27 g, 3 mmol) in 10 ml anhydrous THF, 4-chlorophenyliso- cyanate (0.46 g, 3 mmol) was added dropwise at room temperature. The reaction mixture was left unstirred for 6 h at 273–278 K, whereafter the above resulting solution was added dropwise to a solution of ethylenediamine (0.18 g, 3 mmol) in 5 ml anhydrous THF. After that, the reaction mixture was stirred overnight, the reaction mixture was cooled and the reaction product was recrystallized from CH 3 OH—CH 2 Cl 2 to give colorless crystals of the title compound in yield
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2 (4 Fluoro­anilino) 3 (2 hy­droxy­ethyl)quinazolin 4(3H) one

2 (4 Fluoro­anilino) 3 (2 hy­droxy­ethyl)quinazolin 4(3H) one

C15 0.0535 (7) 0.0494 (7) 0.0348 (6) 0.0053 (6) 0.0160 (5) −0.0031 (5) C16 0.0621 (8) 0.0616 (8) 0.0327 (6) 0.0034 (6) 0.0092 (6) −0.0009 (6) F1 0.0736 (6) 0.0599 (5) 0.0592 (5) −0.0229 (4) 0.0116 (4) −0.0068 (4) N1 0.0521 (6) 0.0494 (6) 0.0297 (5) −0.0036 (5) 0.0092 (4) 0.0026 (4) N2 0.0434 (5) 0.0436 (5) 0.0316 (5) 0.0037 (4) 0.0104 (4) −0.0013 (4) N3 0.0436 (5) 0.0456 (6) 0.0331 (5) 0.0000 (4) 0.0077 (4) 0.0028 (4) O1 0.0601 (6) 0.0639 (6) 0.0450 (5) −0.0115 (5) 0.0123 (4) −0.0152 (4) O2 0.0629 (6) 0.0552 (6) 0.0421 (5) 0.0091 (4) 0.0062 (4) 0.0055 (4)
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3 Eth­­oxy 4 [2 (2 eth­oxy 4 formyl­phen­­oxy)eth­­oxy]benzaldehyde

3 Eth­­oxy 4 [2 (2 eth­oxy 4 formyl­phen­­oxy)eth­­oxy]benzaldehyde

C6 0.0379 (8) 0.0383 (8) 0.0399 (8) −0.0016 (6) 0.0088 (6) 0.0033 (6) C7 0.0373 (8) 0.0359 (8) 0.0446 (8) −0.0070 (6) 0.0100 (6) 0.0067 (6) C8 0.0610 (12) 0.0725 (13) 0.0546 (11) 0.0148 (10) 0.0195 (9) −0.0044 (10) C9 0.0754 (13) 0.0474 (10) 0.0675 (12) −0.0184 (9) 0.0284 (10) 0.0050 (9) C10 0.117 (2) 0.0469 (12) 0.119 (2) −0.0236 (12) 0.0425 (17) −0.0063 (12)

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4 [2 (4 Fluoro­phen­yl)furan 3 yl]pyridine

4 [2 (4 Fluoro­phen­yl)furan 3 yl]pyridine

The analysis of the crystal structure of the title compound is shown in Fig. 1. The furan ring makes dihedral angles of 40.04 (11)° and 25.71 (11)° to the pyridine ring and the 4-fluorophenyl ring, respectively. The pyridine ring makes a dihedral angle of 49.51 (10)° to the 4-fluorophenyl ring. Non-conventional C—H···X H-bonds seem to be effective in stabilization of the crystal structure. By intermolecular hydrogen bonds C5—H5···F1 (2.32 Å) and C8—H8···N15 (2.60 Å) a two-dimensional network parallel to the ab plane (Fig. 2) is formed.

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2 (4 Chloro­phenyl) 3 cyclo­hexyl­thia­zolidin 4 one1 1

2 (4 Chloro­phenyl) 3 cyclo­hexyl­thia­zolidin 4 one1 1

S1 0.0430 (4) 0.0896 (6) 0.0808 (5) 0.0129 (4) 0.0002 (3) −0.0059 (5) C2 0.0405 (13) 0.0515 (16) 0.0565 (15) 0.0016 (12) 0.0073 (11) 0.0039 (13) N3 0.0439 (11) 0.0568 (13) 0.0463 (12) 0.0012 (11) 0.0015 (9) −0.0004 (10) C4 0.0549 (17) 0.0598 (18) 0.0556 (18) −0.0145 (14) −0.0069 (14) 0.0023 (14) C5 0.0517 (17) 0.084 (2) 0.082 (2) 0.0014 (17) −0.0110 (15) 0.0130 (18) C6 0.0395 (13) 0.0483 (16) 0.0451 (14) 0.0090 (12) 0.0069 (10) 0.0009 (12) C7 0.0498 (15) 0.0530 (16) 0.0441 (14) 0.0053 (13) 0.0023 (11) 0.0040 (13) C8 0.0463 (15) 0.0547 (16) 0.0620 (17) 0.0044 (13) 0.0059 (13) −0.0004 (14) C9 0.0461 (15) 0.066 (2) 0.0532 (17) 0.0068 (14) −0.0016 (12) −0.0103 (14) C10 0.0615 (17) 0.077 (2) 0.0438 (15) 0.0167 (17) −0.0028 (13) 0.0042 (15) C11 0.0530 (16) 0.0578 (17) 0.0517 (15) 0.0088 (14) 0.0111 (13) 0.0047 (13) C12 0.0485 (15) 0.0537 (16) 0.0547 (15) −0.0035 (14) 0.0079 (12) −0.0071 (13) C13 0.0467 (16) 0.063 (2) 0.116 (3) −0.0045 (15) 0.0127 (16) −0.0204 (18) C14 0.0474 (17) 0.070 (2) 0.115 (3) −0.0027 (16) 0.0103 (17) −0.0280 (19) C15 0.065 (2) 0.076 (2) 0.109 (3) 0.0181 (19) 0.0023 (18) −0.007 (2) C16 0.071 (2) 0.0542 (19) 0.124 (3) −0.0016 (17) 0.019 (2) −0.0078 (19) C17 0.0544 (17) 0.0560 (18) 0.089 (2) −0.0083 (15) 0.0069 (15) 0.0014 (16) O18 0.0921 (15) 0.0864 (16) 0.0500 (12) −0.0093 (12) −0.0077 (10) 0.0022 (11) Cl19 0.0716 (5) 0.0996 (7) 0.0783 (5) 0.0010 (5) −0.0200 (4) −0.0226 (5)
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Methyl 2 benzyl 5 [1 (4 meth­oxy­phen­yl) 4 oxo 3 phenyl­azetidin 2 yl] 4 nitro 3 phenyl­pyrrolidine 2 carboxyl­ate

Methyl 2 benzyl 5 [1 (4 meth­oxy­phen­yl) 4 oxo 3 phenyl­azetidin 2 yl] 4 nitro 3 phenyl­pyrrolidine 2 carboxyl­ate

C34 0.0576 (11) 0.0546 (10) 0.0370 (9) 0.0031 (8) 0.0038 (7) 0.0007 (7) C35 0.0508 (10) 0.0430 (9) 0.0480 (9) −0.0006 (8) 0.0117 (8) −0.0037 (7) C36 0.0572 (11) 0.0418 (9) 0.0508 (10) 0.0072 (8) 0.0096 (8) 0.0077 (7) C37 0.0459 (9) 0.0437 (9) 0.0373 (8) 0.0029 (7) 0.0056 (7) 0.0050 (7) C38 0.131 (2) 0.0645 (14) 0.0560 (13) −0.0010 (14) 0.0233 (13) −0.0162 (10)

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2 [1 (4 Bromo­phen­yl) 3 hy­dr­oxy 3 (4 meth­­oxy­phen­yl)prop­yl]cyclo­hexa­nol

2 [1 (4 Bromo­phen­yl) 3 hy­dr­oxy 3 (4 meth­­oxy­phen­yl)prop­yl]cyclo­hexa­nol

2-(1-(4-Bromophenyl)-3-hydroxy-3-(4-methoxyphenyl)propyl)cyclohexanol was synthesized from 2-(1-(4-bromo- phenyl)-3-(4-methoxyphenyl)-3-oxopropyl)cyclohexanone (1,5-diketone) (Ceylan & Gezegen, 2008; Gezegen et al., 2010). To a solution of 2-(1-(4-bromophenyl)-3-(4-methoxyphenyl)-3-oxopropyl)cyclohexanone (1 mmol) in THF- MeOH (12 ml 5:1) was added NaBH 4 (3 mmol) and stirred for 16 h at room temperature. After completion of the

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Crystal structure of 2 (4 chloro­phen­yl) 3 (4 meth­­oxy­phen­yl) 3 (methyl­sulfanyl)­acrylo­nitrile

Crystal structure of 2 (4 chloro­phen­yl) 3 (4 meth­­oxy­phen­yl) 3 (methyl­sulfanyl)­acrylo­nitrile

Cl7 0.0571 (3) 0.0760 (5) 0.0789 (4) 0.0308 (3) 0.0114 (3) 0.0093 (4) S12 0.0507 (3) 0.0523 (3) 0.0385 (3) 0.0136 (2) 0.0150 (2) 0.0035 (2) O20 0.0451 (8) 0.0666 (11) 0.0699 (10) 0.0192 (7) 0.0125 (7) −0.0035 (9) N10 0.0579 (11) 0.0707 (14) 0.0479 (10) 0.0082 (10) 0.0199 (8) 0.0068 (10) C1 0.0436 (10) 0.0401 (11) 0.0362 (9) −0.0011 (8) 0.0104 (8) 0.0014 (9) C2 0.0594 (12) 0.0383 (11) 0.0421 (10) 0.0073 (9) 0.0120 (9) 0.0045 (9) C3 0.0447 (10) 0.0491 (12) 0.0376 (10) 0.0149 (9) 0.0049 (8) −0.0006 (9) C4 0.0348 (9) 0.0585 (14) 0.0548 (12) 0.0010 (9) 0.0065 (8) 0.0081 (11) C5 0.0393 (10) 0.0412 (12) 0.0532 (11) −0.0006 (8) 0.0033 (8) 0.0103 (10) C6 0.0369 (9) 0.0369 (10) 0.0293 (8) 0.0019 (8) 0.0033 (7) −0.0004 (8) C8 0.0344 (9) 0.0353 (10) 0.0336 (9) −0.0007 (7) 0.0051 (7) −0.0027 (8) C9 0.0374 (9) 0.0437 (12) 0.0377 (10) 0.0035 (8) 0.0033 (8) 0.0013 (9) C11 0.0360 (9) 0.0346 (10) 0.0351 (9) −0.0002 (7) 0.0064 (7) −0.0039 (8) C13 0.0608 (13) 0.0651 (16) 0.0479 (12) 0.0059 (11) 0.0171 (10) 0.0161 (11) C14 0.0368 (9) 0.0365 (10) 0.0321 (8) 0.0022 (7) 0.0078 (7) 0.0015 (8) C15 0.0423 (10) 0.0408 (11) 0.0370 (9) −0.0008 (8) 0.0063 (8) −0.0078 (9) C16 0.0358 (9) 0.0521 (13) 0.0437 (10) −0.0014 (9) 0.0036 (8) −0.0044 (10) C17 0.0405 (10) 0.0420 (12) 0.0409 (10) 0.0071 (8) 0.0118 (8) 0.0077 (9) C18 0.0552 (11) 0.0366 (11) 0.0405 (10) 0.0078 (9) 0.0091 (9) −0.0052 (9) C19 0.0434 (10) 0.0434 (12) 0.0396 (10) 0.0022 (9) 0.0013 (8) −0.0049 (9) C21 0.0776 (17) 0.0797 (19) 0.0691 (15) 0.0403 (15) 0.0239 (13) 0.0036 (15)
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4′ Methyl 3 (4 nitro­phen­yl) 4 phenyl 4,5,1′,2′,3′,4′ hexa­hydro­spiro­[isoxazole 5,2′ naphthalen] 1′ one

4′ Methyl 3 (4 nitro­phen­yl) 4 phenyl 4,5,1′,2′,3′,4′ hexa­hydro­spiro­[isoxazole 5,2′ naphthalen] 1′ one

In a 100 ml flask, 2 mmoles (0.5 g) of (I) and 0.4 g (2.4 mmoles) mmoles of (II) were dissolved in 20 ml of chloroform. The mixture was cooled to 0°C under magnetic stirring in an ice bath. Then 15 ml of bleach at 18° was added in small doses without exceeding 5°C. The mixture was left under magnetic stirring for 16 h at room temperature, then washed with water until the pH was neutral. It was then dried on sodium sulfate. The solvent was evaporated with a rotating evaporator and the oily residue obtained dissolved in ethanol. The precipitated cycloadduct was then analysed by TLC, which indicated the limited formation of two of the 4 stereoisomers for (III) in a 9:1 ratio. The major stereoisomer, (III), was then crystallized in ethanol giving colourless block-like crystals (61% yield), M.p. = 150–153 °C.
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4 (3 Meth­oxy­phenyl­diazen­yl) 2 methyl­phenol

4 (3 Meth­oxy­phenyl­diazen­yl) 2 methyl­phenol

used to solve structure: SHELXS97 Sheldrick, 1997; programs used to refine structure: SHELXL97 Sheldrick, 1997; molecular graphics: ORTEP-3 for Windows Farrugia, 1997; software used to p[r]

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Methyl 3 (2 chloro­phenyl) 2 (1H indol 3 ylmethyl) 5 [1 (4 methoxyphenyl) 4 oxo 3 phenylazetidin 2 yl] 4 nitropyr­rolidine 2 carboxylate

Methyl 3 (2 chloro­phenyl) 2 (1H indol 3 ylmethyl) 5 [1 (4 methoxyphenyl) 4 oxo 3 phenylazetidin 2 yl] 4 nitropyr­rolidine 2 carboxylate

C26 0.057 (2) 0.062 (3) 0.060 (2) 0.032 (2) 0.0248 (18) 0.017 (2) C27 0.059 (2) 0.064 (3) 0.085 (3) 0.044 (2) 0.032 (2) 0.027 (2) C28 0.057 (2) 0.080 (3) 0.071 (3) 0.047 (2) 0.0166 (19) 0.031 (2) C29 0.0485 (18) 0.064 (3) 0.056 (2) 0.0327 (19) 0.0065 (16) 0.013 (2) C30 0.0435 (16) 0.041 (2) 0.0355 (17) 0.0263 (15) −0.0031 (13) 0.0077 (15) C31 0.057 (2) 0.052 (2) 0.045 (2) 0.0381 (19) 0.0046 (15) 0.0036 (17) C32 0.074 (3) 0.080 (3) 0.059 (3) 0.056 (3) −0.004 (2) −0.008 (2) C33 0.106 (4) 0.064 (3) 0.090 (4) 0.067 (3) −0.025 (3) −0.019 (3) C34 0.093 (3) 0.041 (3) 0.093 (4) 0.039 (3) −0.020 (3) 0.007 (2) C35 0.057 (2) 0.037 (2) 0.062 (2) 0.0219 (17) −0.0066 (17) 0.0126 (18) C36 0.0404 (16) 0.053 (2) 0.0320 (17) 0.0278 (17) 0.0102 (13) 0.0177 (16) C37 0.052 (2) 0.097 (4) 0.061 (3) 0.004 (2) 0.024 (2) 0.027 (3)
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3 [3 (4 Chloro­phen­yl) 4 oxo­thia­zolidin 2 yl] 6 meth­yl 4H benzo­pyran 4 one

3 [3 (4 Chloro­phen­yl) 4 oxo­thia­zolidin 2 yl] 6 meth­yl 4H benzo­pyran 4 one

C1 0.107 (2) 0.0602 (14) 0.0852 (17) 0.0015 (13) 0.0566 (17) −0.0136 (12) C2 0.111 (2) 0.0625 (14) 0.0649 (14) −0.0052 (14) 0.0436 (15) −0.0106 (11) C3 0.0684 (13) 0.0472 (10) 0.0547 (12) −0.0082 (9) 0.0263 (10) −0.0041 (9) C4 0.0568 (11) 0.0422 (9) 0.0563 (11) −0.0088 (8) 0.0250 (9) −0.0038 (8) C5 0.0605 (12) 0.0524 (11) 0.0658 (13) −0.0023 (9) 0.0256 (10) −0.0070 (10) C6 0.0778 (15) 0.0497 (11) 0.0931 (17) −0.0011 (11) 0.0444 (14) −0.0072 (12) C7 0.0904 (19) 0.0806 (18) 0.121 (2) 0.0184 (15) 0.0482 (18) −0.0154 (17) C8 0.0468 (9) 0.0482 (10) 0.0430 (10) −0.0087 (7) 0.0140 (8) −0.0033 (7) C9 0.0446 (9) 0.0428 (9) 0.0437 (9) −0.0099 (7) 0.0139 (8) −0.0002 (7) C10 0.0549 (11) 0.0491 (10) 0.0464 (10) −0.0076 (8) 0.0139 (9) 0.0005 (8) C11 0.0412 (9) 0.0473 (10) 0.0460 (9) −0.0051 (7) 0.0136 (8) 0.0033 (8) C12 0.0632 (12) 0.0746 (14) 0.0433 (10) 0.0026 (10) 0.0212 (9) 0.0020 (9) C13 0.0467 (10) 0.0544 (11) 0.0461 (10) 0.0070 (8) 0.0153 (8) −0.0035 (8) C14 0.0442 (9) 0.0375 (8) 0.0472 (9) −0.0035 (7) 0.0156 (8) −0.0056 (7) C15 0.0393 (9) 0.0632 (12) 0.0579 (11) −0.0027 (8) 0.0132 (8) 0.0082 (9) C16 0.0538 (11) 0.0619 (12) 0.0551 (12) −0.0038 (9) 0.0114 (9) 0.0106 (9) C17 0.0618 (12) 0.0496 (10) 0.0501 (11) −0.0118 (9) 0.0245 (9) −0.0073 (8) C18 0.0482 (10) 0.0572 (12) 0.0736 (14) −0.0056 (9) 0.0301 (10) −0.0062 (10) C19 0.0424 (9) 0.0488 (10) 0.0561 (11) 0.0011 (8) 0.0138 (8) −0.0015 (8) Cl1 0.0929 (5) 0.0925 (5) 0.0693 (4) −0.0208 (3) 0.0422 (4) 0.0058 (3) N1 0.0444 (8) 0.0453 (8) 0.0407 (8) −0.0039 (6) 0.0120 (6) −0.0017 (6) O1 0.0536 (8) 0.0795 (10) 0.0478 (8) 0.0087 (7) 0.0109 (7) −0.0079 (7) O2 0.0756 (10) 0.0631 (9) 0.0442 (8) −0.0029 (7) 0.0176 (7) −0.0059 (6) O3 0.0557 (8) 0.0698 (9) 0.0472 (7) −0.0035 (7) 0.0083 (6) −0.0137 (7) S1 0.0587 (3) 0.0748 (4) 0.0582 (3) −0.0101 (2) 0.0274 (3) 0.0077 (2)
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Ethyl 4 (4 bromo­phen­yl) 6 (4 eth­oxy­phen­yl) 2 oxo­cyclo­hex 3 ene­carboxyl­ate

Ethyl 4 (4 bromo­phen­yl) 6 (4 eth­oxy­phen­yl) 2 oxo­cyclo­hex 3 ene­carboxyl­ate

C20 0.073 (3) 0.077 (3) 0.068 (4) 0.016 (3) 0.022 (3) −0.004 (3) C21 0.068 (3) 0.049 (2) 0.063 (3) −0.002 (2) 0.034 (3) 0.001 (2) C22 0.081 (3) 0.081 (3) 0.079 (4) −0.006 (3) 0.041 (3) −0.016 (3) C23 0.094 (4) 0.090 (4) 0.091 (4) −0.013 (3) 0.056 (3) −0.027 (3)

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4 [3 Benzoyl 4 (4 chloro­phen­yl) 1 methyl­pyrrolidin 2 yl] 1 (4 meth­oxy­phen­yl) 3 phenyl­azetidin 2 one

4 [3 Benzoyl 4 (4 chloro­phen­yl) 1 methyl­pyrrolidin 2 yl] 1 (4 meth­oxy­phen­yl) 3 phenyl­azetidin 2 one

A solution of cis-4-formyl-2-azetidinone (1 mmol), sarcosine (1 mmol) and chlorochalcone (1 mmol) was refluxed in toluene (15 ml) using a Dean–Stark apparatus. The completion of the reac- tion was evidenced by thin-layer chromatography. The solvent was then removed in a vacuum. The crude product was subjected to column chromatography using petroleum ether–ethyl acetate (4:1) to afford the title compound. The compound was recrystallized from methanol to obtain diffraction quality crystals.

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