[PDF] Top 20 Crystal structure of 4 [(2 hydroxy 3 methoxybenzyl)amino]benzoic acid hemihydrate
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Crystal structure of 4 [(2 hydroxy 3 methoxybenzyl)amino]benzoic acid hemihydrate
... ethyl 4-{[(2-hydroxy- phenyl)methyl]amino}benzoate, (I) (WEFQEG; Salman et ...ethyl 4-[(3,5-di-tert-butyl-2-hydroxybenzyl)amino]- benzoate, (II) ...n-propyl ... See full document
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Crystal structure and Hirshfeld surface analysis of 4 {[(anthracen 9 yl)methyl]amino}benzoic acid
... (Table 1 and Fig. 3), forming a supramolecular three-dimen- sional structure. The NH hydrogen atom (H1A) is not involved in hydrogen bonding but is directed towards the benzene ring (C2–C7). Approximate ... See full document
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Crystal structure of 4 (2 hydroxy 3 methoxybenzylamino)benzoic acid dimethylformamide monosolvate monohydrate
... Crystal data, data collection and structure refinement details are summarized in Table 2. The N—H and O—H hydrogen atoms were located in difference-Fourier maps and were freely refined, while the ... See full document
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Crystal structure and Hirshfeld surface analysis of 2 [(2 oxo 2H chromen 4 yl)oxy]acetic acid dimethyl sulfoxide monosolvate
... The crystal structure features O—H O and C—H O hydrogen bonds (Table 1; ...Fig. 3). In the crystal, the A and B molecules are linked by O—H O hydrogen bonds, forming chains running along the ... See full document
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Crystal structure of 2 (4 chlorobenzamido)benzoic acid
... The crystal structure determination of 2-(4-chlorobenzamido)benzoic acid, (I), was investigated in a continuation of our studies on substituted N-phenyl benzamides which have ... See full document
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Crystal structure of hexaprop 2 en 1 yl 4,4′,4′′,4′′′,4′′′′,4′′′′′ [1,3,5,2λ5,4λ5,6λ5 triazatriphosphinine 2,2,4,4,6,6 hexaylhexakis(oxy)]hexabenzoate
... A mixture of hexachlorocyclotriphosphazene (1.04 g, 3 mmol), allyl 4-hydroxybenzoate (3.75 g, 21 mmol), and activated potassium carbonate (3.5 g, 253 mmol) in tetrahydrofuran (50 ml) was stirred at 66 °C ... See full document
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Crystal structure of 4 [4 (ethoxycarbonyl)piperazin 1 yl]benzoic acid
... privileged structure (Dinsmore & Beshore, ...in crystal engineering via hydrogen-bonded assembly of organic acids and organic bases (Grossel et ...the crystal structure is reported ... See full document
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Crystal structure of 4 [(3 methoxy 2 oxidobenzylidene)azaniumyl]benzoic acid methanol monosolvate
... based Schiff bases have also been synthesized and reported (Faizi et al., 2015a,b; 2016b; 2017a,b,c). The present work is a part of an ongoing structural study of Schiff bases and their utilization in the synthesis of ... See full document
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Crystal structure of N [4 amino 5 cyano 6 (methylsulfanyl)pyridin 2 yl]acetamide hemihydrate
... A solution of 0.5 g (2.7 mmol) of 4,6-diamino-3-cyano-2-methylthiopyridine-2(1H)-thione in 30 ml glacial acetic acid was refluxed for 3 h. The reaction mixture was allowed to cool and ... See full document
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Crystal structure of 4 [1 (2 hydroxypropyl) 4,5 diphenyl 1H imidazol 2 yl]benzoic acid
... solve structure: SHELXS2013 (Sheldrick, 2008); program(s) used to refine structure: SHELXL2013 (Sheldrick, 2008); molecular graphics: ORTEP-3 for Windows (Farrugia, 2012); software used to prepare ... See full document
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The crystal structures of two new coumarin derivatives: 2 (4 {2 [(2 oxo 2H chromen 4 yl)oxy]acetyl}piperazin 1 yl)acetamide and N (2,4 dimethoxybenzyl) 2 [(2 oxo 2H chromen 4 yl)oxy]acetamide
... Compound (II) N,N-Diisopropylethylamine (DIPEA; 1.82 g, 3.1 equiv.) was added to a mixture of 2-(2-oxo-2H- chromen-4-yloxy)acetic acid (1.0 g, 1.0 equiv.), 1-ethyl-3-(3- ... See full document
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Crystal structure of 2 {[(naphthalen 1 yl)oxy]methyl} 5 (2,4,5 trifluorophenyl) 1,3,4 oxadiazole
... Iodobenzene diacetate (2.0 mol eq) was added to a solution of naphthalen-1-yloxy-acetic acid (2, 4, 5-trifluoro-benzyl- idene)-hydrazide (1.0 mole eq) in dioxane (10mL) at 25-30 ° C and stirred at ... See full document
9
Crystal structure of 3 [(2 acetylphenoxy)carbonyl]benzoic acid
... Isopthaloyl chloride (25 mmol) and 2′-hydroxyacetophenone (35 mmol) were refluxed in the aquauos solution of pyridine for 30 min. The mixture was cooled to room temperature and added to a beaker containing ... See full document
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Synthesis, Characterization and Biological Activity of Cu(II) and Ni(II) Complexes of 3-Hydroxy- 4- (Pyridine-2-yl-Methylene Amino) Benzoic Acid
... Cu(II) and Ni(II) complexes are recorded in DMSO. The ligand has signals at δ 9.60 , 12.52, 8.73, 7.55- 7.97 and 8.73 ppm, which are due to Ar-OH, carboxylic acid-OH, pyridine ring, phenyl and N=CH respectively. ... See full document
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Crystal structure of 5 [(4 carboxybenzyl)oxy]isophthalic acid
... was added and the resulting solution was refluxed for 24 h. The solution was pored into ice-cold water and the solid precipitate obtained was filtered and dried in air (yield: 2.8 g, 86%). The title compound (CIA) was ... See full document
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2 [(3 Oxo 1 benzofuran 6 yl)oxy]acetonitrile
... As a continuation of our progress in the development of hybrid drug candidates against tuberculosis, malaria and cancer (Morphy et al., 2004), the title compound was identified as a promising starting material. The ... See full document
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Methyl 3,5 bis[(3 chloropyrazin 2 yl)oxy]benzoate
... N4 0.0418 (8) 0.0467 (9) 0.0483 (9) −0.0107 (7) −0.0114 (7) 0.0056 (7) O1 0.0592 (8) 0.0332 (6) 0.0397 (7) −0.0130 (6) −0.0035 (6) −0.0006 (5) O2 0.0352 (6) 0.0316 (6) 0.0607 (8) −0.0030 (5) −0.0107 (6) 0.0111 (6) O3 ... See full document
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4 [(1,3 Dioxo 2 azaspiro[4 5]decan 2 yl)amino]benzoic acid
... respectively. In all N-aminophenyl-substituted succinimides there are at least four distinct phenyl-ring orientations, distinguishable by the values of these two torsion angles. The conformation of (I) is different from ... See full document
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Crystal structure of 4 [(E) (2 carbamothioylhydrazinylidene)methyl]benzoic acid
... solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL2014/6 (Sheldrick, 2015); molecular graphics: ORTEP-3 for Windows (Farrugia, 2012) and PLATON (Spek, 2009); ... See full document
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3 {2 [(3 Phenylquinoxalin 2 yl)oxy]ethyl} 1,3 oxazolidin 2 one
... solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: X-SEED (Barbour, 2001); software used to prepare material for publication: ... See full document
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