[PDF] Top 20 Redetermination of cis bis(ethylenediamine κ2N,N′)bis(nitrito κN)cobalt(III) (ethylenediamine κ2N,N′)tetrakis(nitrito κN)cobaltate(III) monohydrate
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Redetermination of cis bis(ethylenediamine κ2N,N′)bis(nitrito κN)cobalt(III) (ethylenediamine κ2N,N′)tetrakis(nitrito κN)cobaltate(III) monohydrate
... Although the crystal structure of the compound (I) has been determined previously from visually estimated photographic data (Kushi et al., 1976), it is of rather low quality (R = 0.13) compared to today's standard, and ... See full document
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Crystal structure of bis[cis (1,4,8,11 tetraazacyclotetradecane κ4N)bis(thiocyanato κN)chromium(III)] dichromate monohydrate from synchrotron X ray diffraction data
... cis-arranged thiocyanate anions, displaying a distorted octahedral coordination sphere. The Cr—N(cyclam) bond lengths are in the range 2.080 (2) to 2.097 (2) A ˚ while the average Cr—N(NCS) bond length is 1.985 ... See full document
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Crystal structure of cis bis[4 phenyl 2 (1,2,3,4 tetrahydronaphthalen 1 ylidene)hydrazinecarbothioamidato κ2N1,S]nickel(II) monohydrate tetrahydrofuran disolvate
... Thiosemicarbazone ligands are N,S-donors that show a wide range of coordination modes (Lobana et al., 2009). As a part of our ongoing project on the synthesis and structures of thio- semicarbazone derivatives and their ... See full document
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Crystal structure of cis aquachloridobis(1,10 phenanthroline κ2N,N′)chromium(III) tetrachloridozincate monohydrate from synchrotron data
... been determined from synchrotron data. The Cr III ion is bonded to four N atoms from two 1,10-phenanthroline (phen) ligands, one water molecule and a Cl atom in a cis arrangement, displaying an overall distorted ... See full document
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cis Bis(2,2′ bipyridine 4,4′ dicarboxylic acid κ2N,N′)dichlororuthenium(II) monohydrate
... The crystal structure of the title compound, [RuCl2C12H8N2O42]H2O, which is a precursor of the dye for dyesensitized solar cells, is composed of a rutheniumII complex molecule containing[r] ... See full document
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A redetermination of cis aquabis(glycinato κ2N,O)copper(II)
... Hot ethanol (3 ml) was added to an aqueous solution (3 ml) of copper(II) acetate monohydrate (0.2 g). Glycine (0.15 g) dissolved in water (2.5 ml) was then added to the solution. This mixture was gently heated to ... See full document
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trans 1,2 Bis(4 pyridyl)ethylene monohydrate
... 1,2-Bis(4-pyridyl)ethylene is a bidentate ligand in terms of coordination chemistry and to date a large number of struc- tures involving this molecule have been reported. Both cis and trans isomers have ... See full document
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Crystal structure of zwitterionic 3 (2 hydroxy 2 phosphonato 2 phosphonoethyl)imidazo[1,2 a]pyridin 1 ium monohydrate (minodronic acid monohydrate): a redetermination
... the monohydrate form is preferred, giving more stable crystals with respect to the anhydrous and polyhydrate ...that monohydrate crystals include two crystal forms, named D and E, having the same powder ... See full document
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Redetermination of cis,cis 1,2,3,4 tetraphenylbuta 1,3 diene
... Interplanar angles differing by up to 30 from the values observed in (I) are found in the crystal structures of 2,3- diphenyl-1,4-bis(p-methoxyphenyl)butadiene (Yamaguchi et al., 2000) and a ... See full document
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Bis(4 aminopyridinium) tetraiodidocadmate monohydrate
... The [CdI4]2 anion and the water molecule are bisected by a crystallographic mirror plane perpendicular to the c-axis direction, with the CdII atom, two of the I atoms and the atoms of th[r] ... See full document
9
Bis(L tyrosinium) sulfate monohydrate
... The crystal structures of l-tyrosine hydrobromide (Srinivasan, 1956), l-3,4-dihydroxyphenylalanine (Mostad et al., 1971), l-tyrosine (Mostad et al., 1972), dl-tyrosine (Mostad & Rùmming, 1973), l-tyrosine ... See full document
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Bis(D phenylglycinium) sulfate monohydrate
... The asymmetric unit of the title compound, I, consists of two crystallographically independent protonated phenylglycinium cations, a sulfate anion and a water molecule.. In the phenylgly[r] ... See full document
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Bis(DL phenylalaninium) sulfate monohydrate
... 1992), bis(l-phenyl- alanine) nitrate (Srikrishnan et al., 1984), bis(l-phenylalanine) sulfate monohydrate (Nagashima et ...sulfate monohydrate, (I), has been investi- gated ... See full document
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Bis(L threoninium) sulfate monohydrate
... A four-centre hydrogen bond is observed in the case of N11—H11C involving the sulfate O atom and the double-bonded O atom of the carboxyl group of both molecules, connecting all the moie[r] ... See full document
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Bis(dimethylammonium) aquadioxalatocuprate(II) monohydrate
... 0.96 A Data collection: SMART Bruker, 2002; cell refinement: SAINT Bruker, 2002; data reduction: SAINT; programs used to solve structure: SHELXS97 Sheldrick, 1997; programs used to refin[r] ... See full document
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Crystal structure of bis[bis(4 azaniumylphenyl) sulfone] tetranitrate monohydrate
... Data collection: APEX2 (Bruker, 2006); cell refinement: SAINT (Bruker, 2006); data reduction: SAINT (Bruker, 2006); program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: ... See full document
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Bis{1 [(E) 2 pyridinylmethylidene]semicarbazide}cobalt(II) diperchlorate monohydrate
... complexes with 2,6-diacetylpyridine bis(semicarbazone) (Carcelli et al., 1999; Palenik & Wester, 1978). The carbonyl O atoms that are involved in bonding [C7ÐO1 = 1.245 (3) AÊ and C14ÐO2 = 1.253 (3) AÊ] do not ... See full document
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Bis(2 pyrimidinyl) disulfide dihydrate: a redetermination
... (s), 1427 (m), 1376 (s), 1196 (m), 1165 (s), 800 (m), 767 (m), 741 (m), 626 (m), 448 (m); CHN elemental analysis indicated a bis-pyrimidine- substituted disul®de dihydrate. The previously reported synthesis of (I) ... See full document
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cis 9,10 Bis(bromomethyl) 1,4,5,8 tetraoxadecalin
... The same paper Fuchs et al., 1972 gives detailed structural information for a related compound which has hydrogen atoms in place of the bromomethyl groups of the title compound.. That st[r] ... See full document
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cis Bis(2,2′ bipyridine)diiodocadmium(II)
... The highest density peak is located 1.18 A Data collection: TEXRAY Molecular Structure Corporation, 1999; cell refinement: TEXRAY; data reduction: TEXSAN Molecular Structure Corporation,[r] ... See full document
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