• No results found

In this review, the update progress of biochar, regarding the structural characterization, reactivity investigation, and functionalization and device of biochar, as well as their applications in environmental fields were summarized. For the first time, structural properties of biochar were discussed at macroscopic and microscopic levels. From the macro-scopic view, biochar is made of particles with different sizes including bulk biochar, dissolved biochar and nano biochar. From the microscopic view, the multilevel struc-tures of elements, phases, surface chemistry, and molecular were proposed. The structure and properties of biochar play an important role in determining its reactivity, which con-sisted of chemical activity, such as sorption, catalyst, and redox reaction, and biological activity in terms of interac-tion with microbes. There is a close relainterac-tionship between biochar structure and its reactivity. Particularly, how the qua-ternary structure of biochar influences the chemical activity is discussed. To overcome the shortages (weak mechanical strength, difficult to separate, easy transportation, and poten-tial toxicity) of direct environmental application of pristine biochar particles, functionalization and device of biochar are highlighted. The synthesis methods and environmental application of magnetic biochar, biochar-based 2D mem-brane and 3D macrostructure, immobilized microorganisms on biochar, and biochar-based biofilters are illustrated. The developed biochar-based materials and devices afford new solutions to challenging environmental problems.

The full understanding of biochar’s structure and reac-tivity, and functionalization of biochar and its applications are still wanted. Until now, no undisputed molecular struc-tural model has been put forward for biochar despite some dedicated efforts (Xiao and Chen 2017). This hinders the in-depth understanding of the reactivity of biochar and the functionalization of biochar for environmental applica-tion. Many scientific and technological challenges remain and attract considerable research attention. Figure 10

Table 2 Comparison of biochar and other substrate or amendment in biofilters

Property and function comparison Soil Gravel Compost Activated carbon Biochar

Source and availability ★★★ ★★★ ★★ ★★

Low price ★★★ ★★★ ★★ ★★

Energy requirement ★★★ ★★★ ★★★ ★★

Greenhouse gas emission ★★★ ★★★ ★★ ★★

Specific surface area and porosity ★★★ ★★★

Hydraulic conduction ★★ ★★★ ★★ ★★

Controllable synthesis ★★ ★★★

Adsorption of organic pollutants ★★ ★★★ ★★★

Adsorption of inorganic pollutants ★★★ ★★ ★★★

Seed germination and plant growth ★★★ ★★★

Microbial growth ★★ ★★★ ★★ ★★★

Fig. 9 a Schematic diagram of the enhanced trace BPA and other contaminants removal in stormwater by biochar-amended biofilters (Lu and Chen 2018).

b Comprehensive mechanisms of biochar to enhance contami-nants removal in biofilters is highly related to their physi-cal, chemiphysi-cal, and biological structure and properties, which could be tuned in the synthesis process

24 Biochar (2020) 2:1–31

summarizes some of the critical research areas involved to make further progress in the comprehensive knowledge of the relationship of the structure–reactivity–functionali-zation–application and the development of biochar-based materials and devices for environmental application.

1. More efforts should be made to elucidate the multiple and multilevel structure of biochar; there are two direc-tions to forward. One is the mechanisms of biochar for-mation that underlie the pyrolysis of complex biomass, and the other one is applying and combining advanced techniques to characterize the structure of biochar. Thus, advanced instruments and proper combined techniques should be used to understand the physical and chemi-cal composition of biochar from both macroscopic and microscopic directions.

2. The sorption and catalytic performance, and their mech-anism of biochar towards a wider range of organic com-pounds and metal ions should be well studied. Mean-while, the redox property and its effect on direct reaction with contaminants and indirect reaction with contami-nants through biochar–microbe interactions, for exam-ple, electron transfer between biochar (shuttle), contami-nants, and microbes should be systematically elucidated.

Since reactivity is closely correlated with the structural properties of biochar, the reactivity of biochar affected by aging process should also be taken into consideration.

3. The concept of biochar by design was proposed for years (Abiven et al. 2014) and its large-scale produc-tion should be improved with the goal of environmental

protection. Eco-friendly and cost-effective approaches to modify and functionalize biochar for a specific purpose are important. Furthermore, integrating functionalized biochar within water treatment plants and soil pollution remediation should be given priority in future research.

4. It should be noted that most of the studies regarding bio-char-based materials or systems are still in the lab scale;

thus, more works in field should be paid to. Researches about biochar should change from material or environ-mental science to environenviron-mental engineering. Further scrutiny considering underlying mechanisms and long-term application performance and economic analyses of mature cases are still necessary.

In summary, more attention should be paid to the struc-ture–reactivity–functionalization–application relationship of biochar. In-depth structure elucidation, a better understand-ing of the reactivity of biochar, precise functionunderstand-ing and long-term field application evaluation are needed. We anticipate the biochar-based materials with intelligent functionalization and device achieve the greatest agricultural and environmen-tal benefits possible.

Acknowledgements This project was supported by the National Natural Science Foundations of China (21621005, and 21537005, 21425730), and the National Key Technology Research and Develop-ment Program of China (2018YFC1800705).

Compliance with ethical standards

Conflict of interest The authors declare no conflict of interest.

Fig. 10 Future research and per-spectives for the structure–reac- tivity–functionalization–appli-cation relationship of biochar

References

Abdullah H, Wu HW (2009) Biochar as a fuel: 1. Properties and grind-ability of biochars produced from the pyrolysis of mallee wood under slow-heating conditions. Energy Fuel 23(8):4174–4181 Abisado RG, Benomar S, Klaus JR, Dandekar AA, Chandler JR (2018)

Bacterial quorum sensing and microbial community interactions.

MBio. https ://doi.org/10.1128/mBio.02331 -17

Abit SM, Bolster CH, Cai P, Walker SL (2012) Influence of feedstock and pyrolysis temperature of biochar amendments on transport of Escherichia coli in saturated and unsaturated soil. Environ Sci Technol 46(15):8097–8105

Abiven S, Schmidt MWI, Lehmann J (2014) Biochar by design. Nat Geosci 7(5):326–327

Alam MS, Gorman-Lewis D, Chen N, Flynn SL, Ok YS, Konhauser KO, Alessi DS (2018a) Thermodynamic analysis of Nickel(II) and Zinc(II) adsorption to biochar. Environ Sci Technol 52(11):6246–6255

Alam MS, Gorman-Lewis D, Chen N, Safari S, Baek K, Konhauser KO, Alessi DS (2018b) Mechanisms of the removal of U(VI) from aqueous solution using biochar: a combined spectroscopic and modeling approach. Environ Sci Technol 52(22):13057–13067 Albuquerque P, Casadevall A (2012) Quorum sensing in fungi—a

review. Med Mycol 50(4):337–345

Aller MF (2016) Biochar properties: transport, fate, and impact. Crit Rev Environ Sci Technol 46(14–15):1183–1296

Ashoori N, Teixido M, Spahr S, LeFevre GH, Sedlak DL, Luthy RG (2019) Evaluation of pilot-scale biochar-amended woodchip bio-reactors to remove nitrate, metals, and trace organic contaminants from urban stormwater runoff. Water Res 154:1–11

Becker L, Bada JL, Winans RE, Hunt JE, Bunch TE, French BM (1994) Fullerenes in the 185-billion-year-old sudbury impact structure.

Science 265(5172):642–645

Bi H, Yin Z, Cao X, Xie X, Tan C, Huang X, Chen B, Chen F, Yang Q, Bu X, Lu X, Sun L, Zhang H (2013) Carbon fiber aerogel made from raw cotton: a novel, efficient and recyclable sorbent for oils and organic solvents. Adv Mater 25(41):5916–5921

Brewer CE, Schmidt-Rohr K, Satrio JA, Brown RC (2009) Characteri-zation of biochar from fast pyrolysis and gasification systems.

Environ Prog Sustain Energy 28(3):386–396

Byers JT, Lucas C, Salmond GPC, Welch M (2002) Nonenzymatic turnover of an Erwinia carotovora quorum-sensing signaling molecule. J Bacteriol 184(4):1163–1171

Cai W, Wei J, Li Z, Liu Y, Zhou J, Han B (2019) Preparation of amino-functionalized magnetic biochar with excellent adsorption per-formance for Cr(VI) by a mild one-step hydrothermal method from peanut hull. Colloid Surface A 563:102–111

Cantrell KB, Hunt PG, Uchimiya M, Novak JM, Ro KS (2012) Impact of pyrolysis temperature and manure source on physicochemi-cal characteristics of biochar. Bioresour Technol 107:419–428 Cao XD, Ma LN, Gao B, Harris W (2009) Dairy-manure derived

bio-char effectively sorbs lead and atrazine. Environ Sci Technol 43(9):3285–3291

Cao XD, Ma LN, Liang Y, Gao B, Harris W (2011) Simultaneous immobilization of lead and atrazine in contaminated soils using dairy-manure biochar. Environ Sci Technol 45(11):4884–4889 Cheah S, Malone SC, Feik CJ (2014) Speciation of sulfur in biochar

produced from pyrolysis and gasification of oak and corn stover.

Environ Sci Technol 48(15):8474–8480

Chen B, Ding J (2012) Biosorption and biodegradation of phenanthrene and pyrene in sterilized and unsterilized soil slurry systems stimulated by Phanerochaete chrysosporium. J Hazard Mater 229–230:159–169

Chen B, Zhou D, Zhu L (2008) Transitional adsorption and partition of nonpolar and polar aromatic contaminants by biochars of

pine needles with different pyrolytic temperatures. Environ Sci Technol 42(14):5137–5143

Chen B, Wang Y, Hu D (2010) Biosorption and biodegrada-tion of polycyclic aromatic hydrocarbons in aqueous solu-tions by a consortium of white-rot fungi. J Hazard Mater 179(1–3):845–851

Chen B, Chen Z, Lv S (2011) A novel magnetic biochar efficiently sorbs organic pollutants and phosphate. Bioresour Technol 102(2):716–723

Chen B, Yuan M, Qian L (2012a) Enhanced bioremediation of PAH-contaminated soil by immobilized bacteria with plant residue and biochar as carriers. J Soil Sediment 12(9):1350–1359 Chen Z, Chen B, Chiou CT (2012b) Fast and slow rates of

naphtha-lene sorption to biochars produced at different temperatures.

Environ Sci Technol 46(20):11104–11111

Chen Z, Chen B, Zhou D, Chen W (2012c) Bisolute sorption and thermodynamic behavior of organic pollutants to biomass-derived biochars at two pyrolytic temperatures. Environ Sci Technol 46(22):12476–12483

Chen Z, Xiao X, Chen B, Zhu L (2015) Quantification of chemical states, dissociation constants and contents of oxygen-contain-ing groups on the surface of biochars produced at different temperatures. Environ Sci Technol 49(1):309–317

Chen DD, Chen CW, Hung CM (2017a) Synthesis of magnetic biochar from bamboo biomass to activate persulfate for the removal of polycyclic aromatic hydrocarbons in marine sedi-ments. Bioresour Technol 245:188–195

Chen M, Wang D, Yang F, Xu X, Xu N, Cao X (2017b) Transport and retention of biochar nanoparticles in a paddy soil under environmentally-relevant solution chemistry conditions. Envi-ron Pollut 230:540–549

Chen Q, Zheng J, Yang Q, Dang Z, Zhang L (2019a) Insights into the glyphosate adsorption behavior and mechanism by a MnFe2O4@cellulose-activated carbon magnetic hybrid. ACS Appl Mater Interfaces 11(17):15478–15488

Chen T, Zhang J, Li M, Ge H, Li Y, Duan T, Zhu W (2019b) Bio-mass-derived composite aerogels with novel structure for removal/recovery of uranium from simulated radioactive wastewater. Nanotechnology 30(45):455602

Chen W, Meng J, Han X, Lan Y, Zhang W (2019c) Past, present, and future of biochar. Biochar 1(1):75–87

Chen Z, Xiao X, Xing B, Chen B (2019d) pH-dependent sorption of sulfonamide antibiotics onto biochars: sorption mechanisms and modeling. Environ Pollut 248:48–56

Cheng S, Liu F, Shen C, Zhu C, Li A (2019) A green and energy-sav-ing microwave-based method to prepare magnetic carbon beads for catalytic wet peroxide oxidation. J Clean Prod 215:232–244 Chiou CT, Cheng J, Hung WN, Chen B, Lin TF (2015) Resolution of adsorption and partition components of organic compounds on black carbons. Environ Sci Technol 49(15):9116–9123 Chu G, Zhao J, Chen FY, Dong XD, Zhou DD, Liang N, Wu M,

Pan B, Steinberg CEW (2017) Physi-chemical and sorp-tion properties of biochars prepared from peanut shell using thermal pyrolysis and microwave irradiation. Environ Pollut 227:372–379

Chuaphasuk C, Prapagdee B (2019) Effects of biochar-immobilized bacteria on phytoremediation of cadmium-polluted soil. Environ Sci Pollut Res 26(23):23679–23688

Cornelissen G, Rutherford DW, Arp HPH, Dörsch P, Kelly CN, Rostad CE (2013) Sorption of pure N2O to biochars and other organic and inorganic materials under anhydrous conditions. Environ Sci Technol 47(14):7704–7712

Covarrubias SA, de-Bashan LE, Moreno M, Bashan Y (2012) Alginate beads provide a beneficial physical barrier against native micro-organisms in wastewater treated with immobilized bacteria and microalgae. Appl Microbiol Biotechnol 93(6):2669–2680

26 Biochar (2020) 2:1–31

Creamer AE, Gao B (2016) Carbon-based adsorbents for postcom-bustion CO2 capture: a critical review. Environ Sci Technol 50(14):7276–7289

Ding K, Xu W (2016) Black carbon facilitated dechlorination of DDT and its metabolites by sulfide. Environ Sci Technol 50(23):12976–12983

Ding B, Huang S, Pang K, Duan Y, Zhang J (2017a) Nitrogen-enriched carbon nanofiber aerogels derived from marine chitin for energy storage and environmental remediation. ACS Sustain Chem Eng 6(1):177–185

Ding Y, Liu YG, Liu SB, Huang XX, Li ZW, Tan XF, Zeng GM, Zhou L (2017b) Potential benefits of biochar in agricultural soils: a review. Pedosphere 27(4):645–661

Epstein E (1972) Mineral nutrition of plants: principles and perspec-tives. Bull Torrey Bot Club 36(4):viii

Fang G, Gao J, Liu C, Dionysiou DD, Wang Y, Zhou D (2014a) Key role of persistent free radicals in hydrogen peroxide activation by biochar: implications to organic contaminant degradation.

Environ Sci Technol 48(3):1902–1910

Fang Q, Chen B, Lin Y, Guan Y (2014b) Aromatic and hydrophobic surfaces of wood-derived biochar enhance perchlorate adsorp-tion via hydrogen bonding to oxygen-containing organic groups.

Environ Sci Technol 48(1):279–288

Fang G, Liu C, Gao J, Dionysiou DD, Zhou D (2015) Manipulation of persistent free radicals in biochar to activate persulfate for contaminant degradation. Environ Sci Technol 49(9):5645–5653 Fernandes MB, Brooks P (2003) Characterization of carbonaceous

combustion residues: II. Nonpolar organic compounds. Chem-osphere 53(5):447–458

Frohlich AC, Foletto EL, Dotto GL (2019) Preparation and characteri-zation of NiFe2O4/activated carbon composite as potential mag-netic adsorbent for removal of ibuprofen and ketoprofen phar-maceuticals from aqueous solutions. J Clean Prod 229:828–837 Fu H, Liu H, Mao J, Chu W, Li Q, Alvarez PJ, Qu X, Zhu D (2016)

Photochemistry of dissolved black carbon released from biochar:

reactive oxygen species generation and phototransformation.

Environ Sci Technol 50(3):1218–1226

Fu D, Singh RP, Yang X, Ojha CSP, Surampalli RY, Kumar AJ (2018) Sediment in situ bioremediation by immobilized microbial acti-vated beads: pilot-scale study. J Environ Manag 226:62–69 Fu H, Ma S, Zhao P, Xu S, Zhan S (2019) Activation of

peroxymono-sulfate by graphitized hierarchical porous biochar and MnFe2O4 magnetic nanoarchitecture for organic pollutants degradation:

structure dependence and mechanism. Chem Eng J 360:157–170 Gao X, Wu H (2014) Aerodynamic properties of biochar particles:

effect of grinding and implications. Environ Sci Technol Lett 1(1):60–64

Gao X, Cheng HY, Del Valle I, Liu S, Masiello CA, Silberg JJ (2016) Charcoal disrupts soil microbial communication through a combination of signal sorption and hydrolysis. ACS Omega 1(2):226–233

Garcia-Delgado C, Eymar E, Camacho-Arevalo R, Petruccioli M, Crognale S, D’Annibale A (2018) Degradation of tetracyclines and sulfonamides by stevensite- and biochar-immobilized lac-case systems and impact on residual antibiotic activity. J Chem Technol Biotechnol 93(12):3394–3409

Ghaffar A, Zhu X, Chen B (2018) Biochar composite membrane for high performance pollutant management: fabrication, structural characteristics and synergistic mechanisms. Environ Pollut 233:1013–1023

Ghaffar A, Zhang L, Zhu X, Chen B (2019) Scalable graphene oxide membranes with tunable water channels and stability for ion rejection. Environ Sci Nano 6(3):904–915

Grandclement C, Tannieres M, Morera S, Dessaux Y, Faure D (2016) Quorum quenching: role in nature and applied developments.

FEMS Microbiol Rev 40(1):86–116

Grebel JE, Mohanty SK, Torkelson AA, Boehm AB, Higgins CP, Maxwell RM, Nelson KL, Sedlak DL (2013) Engineered infil-tration systems for urban stormwater reclamation. Environ Eng Sci 30(8):437–454

Guo J, Chen B (2014) Insights on the molecular mechanism for the recalcitrance of biochars: interactive effects of carbon and silicon components. Environ Sci Technol 48(16):9103–9112 Haham H, Grinblat J, Sougrati MT, Stievano L, Margel S (2015)

Engineering of iron-based magnetic activated carbon fabrics for environmental remediation. Materials 8(7):4593–4607 Hale SE, Lehmann J, Rutherford D, Zimmerman AR, Bachmann RT,

Shitumbanuma V, O’Toole A, Sundqvist KL, Arp HP, Cor-nelissen G (2012) Quantifying the total and bioavailable poly-cyclic aromatic hydrocarbons and dioxins in biochars. Environ Sci Technol 46(5):2830–2838

Han L, Chen B (2017) Generation mechanism and fate behav-iors of environmental persistent free radicals. Prog Chem 29(9):1008–1020

Han Z, Sani B, Mrozik W, Obst M, Beckingham B, Karapanagioti HK, Werner D (2015) Magnetite impregnation effects on the sorbent properties of activated carbons and biochars. Water Res 70:394–403

Harvey OR, Herbert BE, Rhue RD, Kuo LJ (2011) Metal interactions at the biochar-water interface: energetics and structure-sorption relationships elucidated by flow adsorption microcalorimetry.

Environ Sci Technol 45(13):5550–5556

He J, Song Y, Chen JP (2017) Development of a novel biochar/PSF mixed matrix membrane and study of key parameters in treat-ment of copper and lead contaminated water. Chemosphere 186:1033–1045

Hu SJ, Zhang DN, Yang Y, Ran Y, Mao JD, Chu WY, Cao XY (2019) Effects of the chemical structure, surface, and micropore properties of activated and oxidized black carbon on the sorp-tion and desorpsorp-tion of phenanthrene. Environ Sci Technol 53(13):7683–7693

Huang Q, Song S, Chen Z, Hu B, Chen J, Wang X (2019) Biochar-based materials and their applications in removal of organic contaminants from wastewater: state-of-the-art review. Biochar 1(1):45–73

Idrees M, Jeelani S, Rangari V (2018) Three-dimensional-printed sustainable biochar-recycled PET composites. ACS Sustain Chem Eng 6(11):13940–13948

Inchagcova KS, Duskaev GK, Deryabin DG (2019) Quorum sensing inhibition in Chromobacterium violaceum by amikacin combi-nation with activated charcoal or small plant-derived molecules (pyrogallol and coumarin). Microbiology 88(1):63–71 Inyang MI, Gao B, Yao Y, Xue Y, Zimmerman A, Mosa A,

Pullam-manappallil P, Ok YS, Cao X (2015) A review of biochar as a low-cost adsorbent for aqueous heavy metal removal. Crit Rev Environ Sci Technol 46(4):406–433

Jarvis JM, Page-Dumroese DS, Anderson NM, Corilo Y, Rodgers RP (2014) Characterization of fast pyrolysis products gener-ated from several western USA woody species. Energy Fuels 28(10):6438–6446

Jiang X, Xiang X, Hu H, Meng X, Hou L (2019) Facile fabrication of biochar/Al2O3 adsorbent and its application for fluoride removal from aqueous solution. J Chem Eng Data 64(1):83–89 Jin J, Sun K, Yang Y, Wang Z, Han L, Wang X, Wu F, Xing B (2018)

Comparison between soil- and biochar-derived humic acids:

composition, conformation, and phenanthrene sorption. Envi-ron Sci Technol 52(4):1880–1888

Johannes L, Stephen J (2009) Biochar for environmental manage-ment: science and technology. Earthscan, London

Jung KW, Lee S, Lee YJ (2017) Synthesis of novel magnesium fer-rite (MgFe2O4)/biochar magnetic composites and its adsorption

behavior for phosphate in aqueous solutions. Bioresour Tech-nol 245:751–759

Kang JK, Yi IG, Park JA, Kim SB, Kim H, Han Y, Kim PJ, Eom IC, Jo E (2015) Transport of carboxyl-functionalized carbon black nanoparticles in saturated porous media: column experiments and model analyses. J Contam Hydrol 177–178:194–205 Katam K, Bhattacharyya D (2019) Simultaneous treatment of domestic

wastewater and bio-lipid synthesis using immobilized and sus-pended cultures of microalgae and activated sludge. J Ind Eng Chem 69:295–303

Keiluweit M, Nico PS, Johnson MG, Kleber M (2010) Dynamic molec-ular structure of plant biomass-derived black carbon (biochar).

Environ Sci Technol 44(4):1247–1253

Khan S, Chao C, Waqas M, Arp HP, Zhu YG (2013) Sewage sludge biochar influence upon rice (Oryza sativa L) yield, metal bioac-cumulation and greenhouse gas emissions from acidic paddy soil.

Environ Sci Technol 47(15):8624–8632

Kim KH, Kim JY, Cho TS, Choi JW (2012) Influence of pyrolysis temperature on physicochemical properties of biochar obtained from the fast pyrolysis of pitch pine (Pinus rigida). Bioresour Technol 118:158–162

Klüpfel L, Keiluweit M, Kleber M, Sander M (2014) Redox properties of plant biomass-derived black carbon (biochar). Environ Sci Technol 48(10):5601–5611

Kong XK, Chen CL, Chen QW (2014) Doped graphene for metal-free catalysis. Chem Soc Rev 43(8):2841–2857

Lan Y, Yan N, Wang W (2016) Application of PDMS pervaporation membranes filled with tree bark biochar for ethanol/water separa-tion. RSC Adv 6(53):47637–47645

Lan Y, Yan N, Wang W (2018) Optimization of the PDMS/biochar nanocomposite membranes using the response surface methodol-ogy. Sci Eng Compos Mater 25(5):947–956

Lau AY, Tsang DC, Graham NJ, Ok YS, Yang X, Li XD (2017) Sur-face-modified biochar in a bioretention system for Escherichia coli removal from stormwater. Chemosphere 169:89–98 Le Brech Y, Raya J, Delmotte L, Brosse N, Gadiou R, Dufour A (2016)

Characterization of biomass char formation investigated by advanced solid state NMR. Carbon 108:165–177

Lee JW, Kidder M, Evans BR, Paik S, Buchanan AC, Garten CT, Brown RC (2010) Characterization of biochars produced from cornstovers for soil amendment. Environ Sci Technol 44(20):7970–7974

Lehmann J (2007) A handful of carbon. Nature 447(7141):143–144 Lehmann J, Rillig MC, Thies J, Masiello CA, Hockaday WC, Crowley

D (2011) Biochar effects on soil biota—a review. Soil Biol Bio-chem 43(9):1812–1836

Lewis J, Miller M, Crumb J, Al-Sayaghi M, Buelke C, Tesser A, Alshami A (2019) Biochar as a filler in mixed matrix materials:

synthesis, characterization, and applications. J Appl Polym Sci 136(41):48027

Li F, Lu L, Zheng X, Ngo HH, Liang S, Guo W, Zhang X (2014) Enhanced nitrogen removal in constructed wetlands: effects of dissolved oxygen and step-feeding. Bioresour Technol 169:395–402

Li H, Mahyoub SAA, Liao W, Xia S, Zhao H, Guo M, Ma P (2017) Effect of pyrolysis temperature on characteristics and aromatic contaminants adsorption behavior of magnetic biochar derived from pyrolysis oil distillation residue. Bioresour Technol 223:20–26

Li J, Fan J, Liu D, Hu Z, Zhang J (2019) Enhanced nitrogen removal in biochar-added surface flow constructed wetlands: dealing with seasonal variation in the north China. Environ Sci Pollut Res 26(4):3675–3684

Li XP, Wang CB, Zhang JG, Liu JP, Liu B, Chen GY (2020) Prepara-tion and applicaPrepara-tion of magnetic biochar in water treatment: a critical review. Sci Total Environ 711:134847

Lian F, Xing B (2017) Black carbon (biochar) in water/soil environ-ments: molecular structure, sorption, stability, and potential risk. Environ Sci Technol 51(23):13517–13532

Lieke T, Zhang X, Steinberg CEW, Pan B (2018) Overlooked risks of biochars: persistent free radicals trigger neurotoxicity in Cae-norhabditis elegans. Environ Sci Technol 52(14):7981–7987

Lieke T, Zhang X, Steinberg CEW, Pan B (2018) Overlooked risks of biochars: persistent free radicals trigger neurotoxicity in Cae-norhabditis elegans. Environ Sci Technol 52(14):7981–7987

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