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Important formulations: Punarnav¡Àtaka

In document API-Pt-I, Vol-9 (Page 103-107)

kv¡tha c£r¸a, Punarnav¡di ma¸·£ra, Punarnav¡sava, Sukum¡ra gh¤ta

Therapeutic uses:

Dh¡tu kÀaya (tissue

wasting), P¡¸·u (anaemeia), áotha (inflammation)

Rf

1.0

0.5

0.0 Punarnav¡ Hydro-alcoholic Extract is a dried and

powdered extract prepared from Punarnav¡ (appropriately powdered). The extract contains not less than 0.025 per cent of boeravinone B when assayed.

Method of preparation:

Take Punarnav¡ suitably sized (powder or pieces) in an extractor. Add 50 per cent aqueous alcohol, about 3 times the quantity of raw material and heat under a reflux at a temperature between 80- 850 for 3-4 hours. Filter the extract through a filter

(preferably 10 m pore size) to a suitable sized vessel. The marc is extracted three times more, filtering the extract each time into the same vessel. Concentrate the combined filtrate to a syrupy consistency and dry under vacuum (between 400-600 mm of Hg) at a temperature not exceeding 800 till the moisture is below 5 per

cent. Mill the mass and sieve the powder through 500 m mesh to obtain the extract and pack. The yield obtained is about 10 per cent.

Identity, Purity and Strength:

Thin-layer chromatography:

Carry out thin-layer chromatography on a precoated silica gel 60F254 plate (Appendix 3.5)

using boeravinone Bas a reference standard. Test

solution: Extract 2 g of substance by refluxing

with 50 ml of methanol for a period of 15 min. Filter and concentrate the extract to 25 ml.

Standard solution: Dissolve 2 mg of boeravinone B RS in 10 ml of methanol. Procedure: Apply 10

l each of the test and standard solutions as bands at a height of 10 mm from the base of a 10 x 5 cm TLC plate and develop up to 8 cm from the base of the plate using the mobile phase: toluene : ethyl

acetate : formic acid (4.0 : 5.0 : 1.0). Dry the plate

in air and examine under UV 254 nm. The chromatographic profile of the test solution shows a band corresponding to that of the standard solution (Fig. 1).

254 nm

 

RS T

Fig. 1: Thin-Layer Chromatogram of Punarnav¡ water extract

RS: Boeravinone B, T: Test solution

Quantitative parameters:

Loss on drying: not more than 7.0 per cent

(Appendix 2.1.4); Total ash: not more than 12.0 per cent (Appendix 2.1.5); Acid-insoluble ash: not more than 2.0 per cent (Appendix 2.1.7); pH: 6.0- 8.0 (Appendix 2.1.10); Total soluble solids: not less than 90.0 per cent (Appendix 2.1.11) (Method-I)

Other requirements:

Heavy metals:  Complies with the prescribed

limits, (Appendix 3.1); Microbial contamination: Complies with the prescribed limits, (Appendix 3.2); Pesticide residues: Complies with the prescribed limits, (Appendix 3.3); Residual

solvent: Complies with the prescribed limits,

(Appendix 3.8); Aflatoxins: Complies with the prescribed limits, (Appendix 3.4)

Assay:

Carry out the assay by liquid chromatography (Appendix 3.6). Test solution: Take about 5 g, accurately weighed, of the substance being examined and reflux with methanol (25 ml x 3)

on water bath for 15 min each, cool and filter. Combine all the filtrates and transfer to a 100-ml volumetric flask and make up the volume. Filter through 0.42 m membrane. Standard solution: Take about 2.5 mg, accurately weighed,

boeravinone B RS in a 100-ml volumetric flask

and dissolve in about 50 ml of methanol and make up the volume with methanol. Filter through 0.42

m membrane. Chromatographic system: High performance liquid chromatography. Column and

stationary phase: C18 (250 mm x 4.6 mm, 5 m).

Mobile phase: Filtered and degassed gradient

mixture of water and acetonitrile in the following proportions:-

Time

(min) (per cent) Water Acetonitrile (per cent) 0.01 80 20 5 55 45 15 20 80 20 20 80 23 55 45 25 80 20 30 80 20

Injection volume: 20 l. Flow rate: 1.5 ml per min. Detection: UV 280 nm. Procedure: Inject 20

l of the standard solution and record the chromatogram. Inject 20 l of the test solution, record the chromatogram and measure the response for the analyte peak. Calculate the content of boeravinone B in the substance being examined from the peak response of analyte. The test is not valid unless the relative standard deviation for replicate injections is not more than 2.0 per cent.

Fig. 2: HPLC chromatogram of Punarnav¡ hydro-alcoholic extract with

Boeravinone B as RS

Additional requirements:

Storage: Store in well closed container protected

from heat, light, moisture and against attack by insects and rodents.

Labelling: The label states the official name,

followed by the Latin binominal name and the part of the plant contained in the article.

API reference standard:

API Boeravinone B RS

Rf

1.0

0.5

0.0 Punarnav¡ Water Extract is a dried and powdered

extract prepared from Punarnav¡. The extract contains not less than 0.0025 per cent of

boeravinone B when assayed.

Method of preparation:

Take Punarnav¡ suitably sized (powder or pieces) in an extractor. Add water, about 3 times the quantity of raw material and heat at a temperature between 80–850 for 3-4 hours. Filter the extract

through a filter (preferably10 m pore size) to a suitable sized vessel. The marc is extracted three times more, filtering the extract each time into the same vessel. Concentrate the combined filtrate to a syrupy consistency and dry under vacuum (between 400-600 mm of Hg) at a temperature not exceeding 800 till the moisture is below 5 per cent.

Mill the mass and sieve the powder through 500

m mesh and pack. The yield obtained is about 8 per cent.

Identity, Purity and Strength:

Thin-layer chromatography:

Carry out thin-layer chromatography on a precoated silica gel 60F254 plate (Appendix 3.5)

using boeravinone Bas a reference standard. Test

solution: Extract 2 g of substance by refluxing

with 50 ml of methanol for a period of 15 min. Filter and concentrate the extract to 25 ml.

Standard solution: Dissolve 2 mg of boeravinone B RS in 10 ml of methanol. Procedure: Apply 10

l each of the test and standard solutions as bands at a height of 10 mm from the base of a 10 x 5 cm TLC plate and develop up to 8 cm from the base of the plate using the mobile phase : toluene :

ethyl acetate : formic acid (4.0 : 5.0 : 1.0). Dry the

plate in air and examine under UV 254 nm. The chromatographic profile of the test solution shows a band corresponding to that of the standard solution (Fig. 1).

254 nm

 

RS T

Fig. 1: Thin-Layer Chromatogram of Punarnav¡ water extract

RS: Boeravinone B, T: Test solution

Quantitative parameters:

Loss on drying: not more than 7.0 per cent

(Appendix 2.1.4); Total ash: not more than 12.0 per cent (Appendix 2.1.5); Acid-insoluble ash: not more than 2.0 per cent (Appendix 2.1.7); pH: 6.0-8.0 (Appendix 2.1.10); Total soluble solids: not less than 90.0 per cent (Appendix 2.1.11) (Method-II)

Other requirements:

Heavy metals: Complies with the prescribed limits,

(Appendix 3.1); Microbial contamination: Complies with the prescribed limits, (Appendix 3.2); Pesticide residues: Complies with the prescribed limits, (Appendix 3.3); Aflatoxins: Complies with the prescribed limits, (Appendix 3.4)

Assay:

Carry out the assay by liquid chromatography (Appendix 3.6). Test solution: Take about 5 g, accurately weighed, of the substance being examined and reflux with methanol (25 ml x 3) on water bath for 15 min each, cool and filter. Combine all the filtrates and transfer to a 100-ml

volumetric flask and make up the volume. Filter through 0.42 m membrane. Standard solution: Take about 2.5 mg, accurately weighed,

boeravinone B RS in a 100 ml volumetric flask

and dissolve in about 50 ml of methanol and make up the volume with methanol. Filter through 0.42 m membrane. Chromatographic system: High performance liquid chromatography.

Column and stationary phase: C18 (250 mm x 4.6

mm, 5 m). Mobile phase: Filtered and degassed gradient mixture of water and acetonitrile in the following proportions:

Time

(min) (per cent) Water Acetonitrile (per cent) 0.01 80 20 5 55 45 15 20 80 20 20 80 23 55 45 25 80 20 30 80 20

Injection volume: 20 l. Flow rate: 1.5 ml per min. Detection: UV, 280 nm. Procedure: Inject 20 l of the standard solution and record the chromatogram. Inject 20 l of the test solution, record the chromatogram and measure the response for the analyte peak. Calculate the content of boeravinone B in the substance being examined from the peak response of analyte. The test is not valid unless the relative standard deviation for replicate injections is not more than 2.0 per cent.

Fig. 2: HPLC chromatogram of Punarnav¡ water extract with Boeravinone B as RS 

Additional requirements:

Storage: Store in well closed container protected

from heat, light, moisture and against attack by insects and rodents.

Labelling: The label states the official name,

followed by the Latin binominal name and the part of the plant contained in the article.

API reference standard:

In document API-Pt-I, Vol-9 (Page 103-107)