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Physics Procedia 25 ( 2012 ) 355 – 362

1875-3892 © 2012 Published by Elsevier B.V. Selection and/or peer-review under responsibility of Garry Lee doi: 10.1016/j.phpro.2012.03.096

2012 International Conference on Solid State Devices and Materials Science

Surface Integrity of Titanium Alloy Ti-6Al-4V in Ball end

Milling

M-B. Mhamdi

a,b,*

, M. Boujelbene

a,c

, E. Bayraktar

a

, A. Zghal

b a LISMMA /Supmeca -Paris, 3 rue Fernand Hainaut - 93407 Saint-Ouen Cedex, France

bURMSSDT/ESSTT, 5 Avenue Taha Houssien-1008 Bab Mnara Tunis, Tunisia cUR-ME-ENIT BP.37, 1002 Tunis le Belvédère, Tunisia

Abstract

With the evolution of machine tools and the emergence of new cutting tools such as cermet, CBN; and in framework of the production of parts with complex geometry, the manufacturers were able to realize more and more parts of complex shape. The multi-axis machining is the main technique for achieving the free form; in fact the multi-axis milling with ball end tools attracts the interest of the aerospace industry and the mussel industry which continues to seek ways to improve the surface quality of finished parts. The titanium alloy is widely used in aerospace industry is the subject of this studyin fact, the integrity of the surfaces of parts produced by multi-axis millingis an issue more relevant than ever for the aerospace industry. This paper aims to study the influence of the tool position and the parameters cutting precisely the speed feed Vf, the engagement of the toolon the roughness 3 D, micro-hardness and

microstructure alteration created in sub-surface during the milling of concave surface oftitanium alloytype Ti-6Al-4V.

© 2011 Published by Elsevier Ltd. Selection and/or peer-review under responsibility of [name organizer]

Keys words: Surface integrity, multi-axis milling, titanium alloy Ti-6Al-4V, roughness, micro-hardness, microstructure alteration;

1. Introduction

The titanium alloy Ti-6Al-4V is a material widely used in aerospace, biomedical, and chemical industries thanks to its good mechanical and thermal properties because of their good strength-to-weight ratio, corrosion resistance, possibility of use in harsh environments such as high temperature. For example, in the aerospace industry in general the mechanical parts are extracted by the milling process because of

*Corresponding author. Tel.: +33 (0) 1 49 45 29 54; fax: +33 (0)1 49 45 29 59.

E-mail address: [email protected].

© 2012 Published by Elsevier B.V. Selection and/or peer-review under responsibility of Garry Lee

Open access under CC BY-NC-ND license.

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the different forms of parts as the complex forms. However, titanium alloys have a poor machinability due to its low thermal conductivity, which causes a high chemical reactivity caused by the elevation of temperature in the field cutting [1], indeed, the quality of a machined surface, is becoming more and more important to satisfy the increasing demands of sophisticated component performance. However, the surface integrity is one of the most relevant parameters used for evaluating the quality of machined surface.Indeed,the quality and performance of a product is directly related to surface integrity achieved by final machining. However, the surface integrity is influenced by a set of parameter as we include for example the orientation of the tool axis relative to the surface the direction of feedrate in sense scans. Various studies on the characterization of the influence of the hemispherical tool orientation were conducted. Some have a more experimental [2-3] and are more attached to observe the tool wear as the final surface finish. Other studies [4] analyze the trace left by a tool for different inclination angle and propose a model to predict the surface, but the criteria used to the surface state, are only linear and non-surfacic. The presence of vibration in the system machine-tool-piece has a bearing on the quality of finished surface [5]. Other researchers have analyzed the influence of cutting parameters on surface state such Daymi et al. and Amin et al. [6-7]. However, the surface integrity including several criteria such as roughness, microstructural changes, residual stresses, micro-hardness and plastic deformation at the surface. These criteria are influenced by the same factors mentioned earlier, but the variation of each parameter has a different influence (in the sense all criteria can be good or bad at a time) on each criterion. However, researchers have studied these criteria a case by case several researchers found that surface roughness values became larger at high cutting speeds in turning Ti–6Al–4V [8] and in end milling Ti– 6Al–4V using WC-Co and PCD insert [7]. The tool wear has a positive effect on the workpiece indeed, with increasing the tool wear the surface will be smoother [9], in addition the hardness to the surface layer in turning titanium alloy Ti-6Al-4V is increased about 30% the hardness of metal located in the heart, this layer is assumed in the order of 100 —m. The same way [10] estimated the same value 30%. The microstructure at the surface layer can be changed as a result of chemical changes caused by the tool, enlargements and elongations of the grains for the turning Ti-6Al-4V are observed by Hughes et al. [11]. Moreover, the residual stresses were studied in terms of cutting parameters for the Ti-6Al-4V by several researchers such as Ulutan [12]. Similar work on the surface integrity generated by the milling tool hemispherical was carried by His-Yung et al. and Boujelbene et al. [13, 14].

The subject of this paper is to study the topography of a surface machined by the tool hemispherical in 3-axis milling of Ti-6Al-4V with cutting conditions of finishing, we mainly analyze the roughness 3 D, the micro-hardness and micro-structural alterations caused by the effect of tool.

2. Experimental work and conditions

2.1. Workpiece material

Materials studied here is titanium alloy Ti-6Al-4V, is widely used in aerospace, biomedical, chemical and petroleum industries because of their good mechanical and thermal properties. Few properties are listed in Table 1.

The micro-structure of Ti-6Al-4V is an alpha-beta alloy (Į + ȕ), the alpha phase proportion usually varies from 60 to 90%. The alpha phase in pure titanium is characterized by a hexagonal close-packed crystalline structure that remains stable from room temperature; beta phase in pure titanium has a body-centered cubic structure, and is stable from room temperature to the melting point. The addition of aluminum alloy can stabilize the alpha phase; that is they raise the temperature at which the alloy will be transformed completely to the beta phase. Adding alloying elements to titanium provides a wide range of physical and mechanical properties. Alloying additions such as chromium, copper, iron, manganese,

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molybdenum, and vanadium stabilize the beta phase by lowering the temperature of transformation from alpha to beta. The chemical composition is given in table 2.

2.2. Machining tests

Three axis milling with a hemispherical tool were carried in dry machining out at various cutting conditions on the Ti–6Al–4V alloy. The machined shape are concave surfaces (see Fig 1), the cutting tests are carried out on a three-axis high speed milling centre in a ball-end mill with a diameter of 16 mm, The tool used is a hemispherical tool with removable insert to two teeth, the tool is brand Sandvik its substrate neat grained, associated with a PVD coating of TiAlN: Designation of insert: R216F-16 40 E-L P20A.

Table 1. Mechanical and thermal properties of Ti–6Al–4V. Density (g /cm3) Hardness (HB) Modulus E (GPa) Tensile Strength (MPa) Thermal conductivity (W /m°K) Melting point (°C) 4.42 345 113.8 995 7.3 1670

Table 2. Chemical composition (%) of Ti–6Al–4V Alloy.

Element Al V Fe C N H O Ti

% 6 4 0.3 0.08 0.05 0.01 0.2 Balance

Table 3.Machining conditions. Spindle speed N

(rpm) Feed speed V(mm/min) f

Axial depth of cut ap

(mm)

Pick or step over, ae

(mm)

Type of milling

3000 300 -600 - 900 0.5 0.5 one direction, one way

The cutting style for ball end milling of concave surface used and the cutting conditions are listed in the table 3.

However, for measuring results we are used Scanning Electron Microscope (SEM) to control the surface topography, Micro-hardness tester to measure the micro-hardness and tester-roughness to measure the surface roughness.

(a) (b) Fig.1. (a) Photo of milling of concave surface; (b) Tool position for milling of concave surface

Workpiece

șd șup

Vf

Vc-eff-mini Downward

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3. Results and discussion

3.1. Surface topography and roughness

In order to generate the topography of surfaces in ball-end milling, the study of the surfaces is requested. However, there are many parameters used in the literature related to surface roughness. Otherwise, for the 2D surface roughness parameters, the most popular of these parameters is average roughness. It is quoted as Ra symbol. Mathematically, Ra is the arithmetic value of the profile from centerline; for the 3D surface roughness parameters, the most used parameters are, Sa and Sq, respectively, the arithmetical mean of the surface and the root mean square roughness. In this investigation, representative parameters of 3D surface were studied.

The arithmetical mean of the surface Sa and the root mean square roughness Sq are given respectively by equations (1) and (2). ܵܽ ൌ ͳ ݊݉෍  ௡ିଵ ௫ୀ଴ ෍ȁܼሺݔǡ ݕሻȁ ௡ିଵ ௬ୀ଴ ሺͳሻ “ ൌ ͳ ෍  ୬ିଵ ୶ୀ଴ ෍ȁଶሺšǡ ›ሻȁ ୬ିଵ ୷ୀ଴ ሺʹሻ

The Sa and Sq variation of the concave surface machined were studied according to the tool position and the speed feed Vf. The study has shown that the tool position influences significantly the values of Sa

and Sq. Indeed, when the tool removes the material with a low effective cutting speed Vc-eff-minimale at the

top of the concave surface, ș = 0°, (see Fig. 1b), we recorded high values of Sa and Sq (Sq = 4.6 —m and Sa = 2.8 —m) compared to downward milling and upward milling (see Fig.5a). Also, the surface topography and SEM observation in this zone shows traces disturbed of the cutting tool and non-regular scallop (Fig.3a, 3b) which shows the change of the cutting direction at the top of the concave surface. However, the phenomena of vibrations were heard during machining in this area that has been machined with a very low effective cutting speed (even zero). By cons, when the tool removes materials with effective cutting speeds relatively important (downward milling and upward milling) we recorded a best topography and regular scallop (see Fig. 1b, 2, 4). Nevertheless the surface state in upward milling șup =

60°, has a slight advantage compared to downward milling șd = 60°. This is probably due to the

difference of the effective cutting speed and cutting phenomenon (how entered the edge of tool in the material) in the same zone.

The result of the study of state surface 3 D Sa and Sq at the top of the concave form depending on the speed feed Vf is show in Fig. 5b. This study shows that Sa and Sq increase significantly depending on the

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(a) (b) Fig.2. State of surfaces in upward milling șd = 60° at N = 3000 rpm, Vf= 900 mm/min, ae = 0.5 mm, ap = 0.5 mm: (a) Topography 3 D

measured by roughness-tester, (b) SEM observation of a milled surface.

(a) (b) Fig.3. State of surfaces in the top of concave surface ș = 0° at N = 3000 rpm, Vf= 900 mm/min, ae = 0.5 mm, ap = 0.5 mm: (a)

Topography 3 D measured by roughness-tester, (b) SEM observation of a milled surface.

(a) (b) Fig.4. State of surfaces in downward milling șd = 60° at N = 3000 rpm, Vf= 900 mm/min, ae = 0.5 mm, ap = 0.5 mm: (a)Topography 3

D measured by roughness-tester, (b) SEM observation of a milled surface. 2 mm 2 mm 2mm 2mm 2mm 2mm Vf Vf Vf

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(a) (b) Fig.5. The variation of Sa and Sq: (a) according to the tool position at N = 3000 rpm, Vf = 900 mm/min, ae = 0.5 mm, ap = 0.5 mm; (b) according

to feed speed Vf at N = 3000 rpm, ae = 0.5mm, ap = 0.5 mm.

3.2. Micro-hardness and micro-structure alteration

During the machining operations by the hemispherical tool, the workpiece material is exposed to thermal, mechanical and chemical energy that can change the properties of superficial layer (about 100 - 200 —m) of the surface machined. In the case of the hardness measurement, the hardness profile has been evaluated on the surface as a function of the distance from the machined surface (Fig. 6a). That can give an idea on surface proprieties, the level of the work hardening of the deformed layer produced at the local surface. However, the hardness measurements were made according to the tool position; for a depth 120 —m from the machined surface and each 20 —m we measured the hardness two times then we plotted the average of the two measures for each depth (see Fig. 6a). First when we approaching to the core of workpiece, the hardness is decreases for the different positions of tool, the increase in hardness is more important in the top of concave surface, the value of the hardness is about 375 to 20 —m then we approaching at core the hardness can be same as the bulk material (see Fig. 6a), this is due to the very low value of the effective cutting speed (Vc-eff-mini even zero in the centre of the cutter) in the top of concave

surface that will cause crushing of the material, in addition the vibration phenomenon increasing when the tool cut with a low effective diameter (Deff low), which is unfavorable for obtaining good state of surface.

Finally, we observe that hardness in superficial layer is increased at about 8% than the bulk material. However, machining by the hemispherical tool can be creates the variation of near surface microstructure, that is caused by the combined effects of mechanical and thermal loads in milling. Then as in the milling by the hemispherical tool cutting temperatures are too low to induce any phase transformations such as a white layer on the machined surfaces. It implies that no thermal damage occurred at the milling conditions, but the mechanical and thermal loads can creates a very thin layer of hardened material and plastic deformations on top of the machined concave surface. Surface deformation induced strain hardening was the main factor for the measured surface hardness in previous section. First, we note that layer alteration of machined surface is according of cutting condition and tool position in end ball milling. Us, we have interested by the tool position in the machined surface, it was found that when machining under dry conditions a thin layer of disturbed or plastically deformed layer was formed immediately beneath the machined surface.

Fig. 6b, shows a layer that has been disrupted as a result of milling in the top of concave surface at ș = 0 °. This disturbance in general present a plastic deformation in compression of the surface layer that seems to change the orientation of grain and grain boundary, under a result of elongation or / and

0 1 2 3 4 5

Upward milling at ș = 60° Zone of the top of concave surface Downward milling at ș = 60° Values ( — m) Sq (—m) Sa (—m) 0 1 2 3 4 5 200 400 600 800 1000 — m

Speed feed Vf(mm/min)

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racourssicement of the grains. However, it is note that milling in the top of concave surface disturbs the surface much more than the downward milling when upward milling, This is probably due to the cutting phenomenon in this area that is more complicated other the two positions of the tool, because in this area the cutting speed is very low that is can generated a exceptional mechanical and thermal loading that will influence the microstructure in sub-surface machined. By cons, After the examination of the top surface of all machined workpieces shows the occurrence of neither heat affected zone (HAZ) nor white interface layer (WIL).

(a) (b)

Fig.5. (a) Micro-hardness profile of the distance from the machined surface, (b) Microstructure alteration of the top machined concave surface.

4. Conclusions

The surface integrity in end milling titanium Ti–6Al–4V in dry machining of concave surface is the subject of this present work. A series of end milling titanium experiments were conducted to comprehensively characterize surface integrity in various milling conditions, surface integrity includes several criteria. The following are the specific conclusions reached in this paper for few criteria to surface integrity:

x Tool position influences the surface roughness, indeed when hemispherical tool at upward and downward milling provided the best finish surface compared to machining in the top of concave surface.

x The 3D roughness Sa and Sq have influenced by the speed feed Vf, indeed the values of roughness

are increased according to increasing the speed feed.

x The milling by the hemispherical tool produced a thin layer of disturbed or plastically deformed layer formed immediately beneath the machined surface, and it should be noted that the surface not heat affected indeed, neither heat affected zone (HAZ) nor white interface layer (WIL). x The tool positions obviously influence the microhardness of the machined surface.

References

[1]J. Sun, Y.B. Guo, A comprehensive experimental study on surface integrity by end milling Ti–6Al–4V; Journal of Materials

Processing Technology, 2009; 209:4036–4042.

[2]T. J. Ko, H. S. Kim, S. S. Lee, Selection of the machining inclination angle in high-speed ball end milling, International

Journal of Advanced Manufacturing Technology, 2001; 17:163-170.

300 320 340 360 380 0 20 40 60 80 100 120 140 Hardenes Hv 0.2

Depth beneath the machined surface (—m) Milling at the top of concave surface base metal

Downward millig at ș = 60 °

Upward millig at ș = 60° Alteration of machined surface

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[3]M. C. Kang, K. K. Kim, D. W. Lee, J. S. Kim, N. K. Kim, Characteristics of inclined Planes According to the Variations of the cutting direction in high-speed ball-end milling, International Journal of Advanced Manufacturing Technology, 2001; 17:323-329.

[4]K.-D. Bouzakis, P. Aichouh, K. Efstahiou, Determination of the chip geometry, cutting force and roughness in free form surfaces finishing milling, with ball end tools, International Journal of Machine Tools & Manufacture, 2003; 43:499-514.

[5]D. Biermann, P. Kersting, T. Surmann, A general approach to simulating workpiece vibrations during five-axis milling of turbine blades, CIRP Annals - Manufacturing Technology, 2010; 59:125–128.

[6]A. Daymi, M. Boujelbene, A. Ben Amara, E. Bayraktar and D. Katundi, Surface integrity in high speed end milling of titanium alloy Ti–6Al–4V; Materials Science and Technology, 2011; 27:387-393.

[7]N.A.K.M. Amin, A.F. Ismail, N.M.K. Khairusshima, Effectiveness of uncoated WC–Co and PCD inserts in end milling of titanium alloy—Ti–6Al–4V. Journal of Materials Processing Technology, 2007; 192/193:147–158.

[8]M.V. Ribeiro, M.R.V. Moreira, J.R.. Ferreira, Optimization of titanium alloy (Ti–6Al–4V) machining. Journal of Materials

Processing Technology, 2003; 143/144:458–463.

[9]C.H. Che-Haron, A. Jawaid, The effect of machining on surface integrity of titanium alloy Ti–6%Al–4%V. Journal of

Materials Processing Technology, 2005; 166:188–192.

[10]J.L. Canteroa, M.M. Tardiob, J.A. Cantelia, M. Marcosc, M.H. Miguelez, Dry drilling of alloy Ti–6Al–4V. International

Journal of Advanced Manufacturing Technology, 2005; 45:1246–1255.

[11]J.I. Hughes, A.R.C. Sharman, K. Ridgway, The effect of tool edge preparation on tool life and workpiece surface integrity.

Proc. Inst. Mech. Eng., Part B: J. Eng. Manuf. 2004; 218:1113–1123.

[12]Ulutan, T. Ozel, Machining induced surface integrity in titanium and nickel alloys: A review, International Journal of

Machine Tools & Manufacture, 2011; 51:250–280.

[13]Hsi-Yung Feng, Ning Su, Integrated tool path and feed rate optimization for the finishing machining of 3D plane surfaces,

International Journal of Machine Tools & Manufacture, 2000; 40:1557–1572.

[14]M. Boujelbene, A. Moisan, W. Bouzid, S. Torbaty: Variation cutting speed on the five axis milling. Journal of

References

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