1.3 to 1.5 eV
3 Ethylsulfinyl 2 (3 fluorophenyl) 5 phenyl 1 benzofuran
... 3-Chloroperoxybenzoic acid (77%, 202 mg, 0.9 mmol) was added in small portions to a stirred solution of 3-ethyl- sulfanyl-2-(3-fluorophenyl)-5-phenyl-1-benzofuran (278 mg, 0.8 mmol) in ...
9
5 (4 Methoxyphenyl) 1 phenylpyrazolidin 3 one
... To a solution of sodium (40 mmol) in anhydrous methanol (9 mol) were added ethanolamine (4 ml) and n-butanol (20 ml). The methanol was then removed by distillation and 3-(4-methylphenyl)- acrylic acid was added. ...
7
1 (3 Chlorobenzyl) 5 iodoindoline 2,3 dione
... A mixture of 5-iodoisatin (1.8 g, 10 mmol) and 3-chlorobenzyl chloride (1.6 g, 10 mmol) was refluxed in DMF (50 ml) in the precense of potassium carbonate for 6 h. DMF was removed from the reaction mixture ...
6
5 (4 Chlorophenyl) 1 phenylpyrazolidin 3 one
... Ethanolamine (4 ml) and n-butanol (20 ml) were added to a solution of sodium (40 mmol) in anhydrous methanol (9 mol). The methanol was removed by distillation and ethyl 3-(4-chlorophenyl)acrylate (30 mmol) was ...
10
1 Benzoyl 3 (5 quinolyl)thiourea
... mmol), 5-aminoquinoline (1300 mg, 9 mmol) and dichloromethane (50 ml) in the presence of PEG-400 (1200 mg, 3 mmol) as phase transfer catalyst at room temperature for 8h with ...
7
5 Cyclopentyl 2 methyl 3 (3 methylphenylsulfonyl) 1 benzofuran
... 3-Chloroperoxybenzoic acid (77%, 448 mg, 2.0 mmol) was added in small portions to a stirred solution of 5-cyclo- pentyl-2-methyl-3-(3-methylphenylsulfanyl)-1-benzofuran (290 mg, 0.9 ...
8
3,3,4,4,5,5 Hexafluoro 1 [5 (3 fluorophenyl) 2 methyl 3 thienyl] 2 (2 methyl 5 phenyl 3 thienyl)cyclopent 1 ene
... thienyl)perfluorocyclopent- 1-ene, (5) (Peters et al. , 2003) (2.6 g, 7.1 mmol), was added and the mixture was stirred for 2 h at this temperature. The reaction mixture was extracted with ether and ...
16
5 (4 Chlorophenyl) 1 methyl 3 oxocyclohexanecarbonitrile
... A mixture of 5–4′-chlorophenyl-3-methylcyclohex-2-enone (6.40 g, 0.02 mol), potassium cyanide (2.60 g, 0.04 mol), ammonium chloride (1.59 g, 0.03 mol), dimethyl formamide (50 ml) and water (2 ml) was heated ...
7
() 5 (3,4 Dimethoxyphenyl) 1 phenylpyrazolidin 3 one
... To a solution of sodium (40 mmol) in anhydrous methanol (9 ml) was added ethanolamine (4 ml) and n-butanol (20 ml). The methanol was removed by distillation and ethyl 3-(3,4-dimethoxyphenyl)acrylate was added. The ...
8
5 Chloro 2,7 dimethyl 3 (3 methylphenylsulfonyl) 1 benzofuran
... 3-Chloroperoxybenzoic acid (77%, 448 mg, 2.0 mmol) was added in small portions to a stirred solution of 5-chloro-2,7- dimethyl-3-(3-methylphenylsulfanyl)-1-benzofuran (272 mg, 0.9 mmol) ...
8
1 (Carbamoylmethyl) 5 oxopyrrolidin 3 yl acetate
... An anhydrous pyridine solution of 2-(4-hydroxy-2-oxopyrrolidin-1- yl)acetamide (1.58 g, 10 mmol) was added to acetic anhydride (1.02 g, 10 mmol). The mixture was stirred at 298 K for 25 h under nitrogen, and a ...
6
5 Cyclohexyl 3 (3 fluorophenylsulfonyl) 2 methyl 1 benzofuran
... For the biological activity of benzofuran compounds, see: Aslam et al. (2009); Galal et al. (2009); Khan et al. (2005). For natural products with benzofuran rings, see: Akgul & Anil (2003); Soekamto et al. (2003). ...
9
5 (3 Fluorophenyl) 1 phenylpyrazolidin 3 one
... conformation. An intramolecular C—H N hydrogen bond results in the formation of a five-membered ring adopting an envelope conformation. In the crystal structure, inter- molecular N—H O and C—H O hydrogen bonds link the ...
7
5 Ethyl 3 (3 fluorophenylsulfonyl) 2 methyl 1 benzofuran
... For the biological activity of benzofuran compounds, see: Aslam et al. (2009); Galal et al. (2009); Khan et al. (2005). For natural products with benzofuran rings, see: Akgul & Anil (2003); Soekamto et al. (2003). ...
9
5 Chloro 3 ethylsulfinyl 2 (3 fluorophenyl) 1 benzofuran
... methyl H atoms. The positions of methyl hydrogens were optimized rotationally. The F1 and F2 atoms of the 3-fluoro- phenyl rings are disordered over two positions with site occupancy factors, from refinement of ...
10
5 Cyclohexyl 3 ethylsulfinyl 2 (3 fluorophenyl) 1 benzofuran
... 3-Chloroperoxybenzoic acid (77%, 202 mg, 0.9 mmol) was added in small portions to a stirred solution of 5-cyclo- hexyl-3-ethylsulfanyl-2-(3-fluorophenyl)-1-benzofuran (283 mg, 0.8 mmol) ...
8
5 (2 Furyl) 3 hydroxy 1 phenylpenta 2,4 dien 1 one
... Finally, the arrangement of molecules III and IV relative to the central molecule indicate CÐH interactions between atoms H7 and H9 and the furanyl rings III and IV, respectively (Fig. 3; symmetry codes as in Fig. ...
7
2,3 Dibromo 1 (2,4 dichloro 5 fluorophenyl) 3 phenylpropan 1 one
... of 1-(2,4-dichloro-5-fluorophenyl)-3-phenylprop-2-en-1-one) (1 mmol) in chloroform (25 ml), bromine (1 mmol) was added slowly with ...
8
1 (Carbamoylmethyl) 5 oxopyrrolidin 3 yl propionate
... O4 0.0923 (15) 0.0511 (11) 0.0727 (15) −0.0092 (9) 0.0119 (11) −0.0055 (9) N1 0.0607 (14) 0.0437 (11) 0.0596 (16) 0.0047 (10) 0.0081 (11) 0.0029 (10) N2 0.0620 (17) 0.0610 (16) 0.102 (2) 0.0072 (14) 0.0002 (15) 0.0173 ...
6
5 Bromo 2 methyl 3 (3 methylphenylsulfinyl) 1 benzofuran
... Br1 0.03812 (10) 0.03427 (10) 0.02629 (9) 0.01357 (7) 0.00008 (6) 0.01480 (7) S1 0.02985 (19) 0.02419 (19) 0.0310 (2) 0.01154 (15) 0.00610 (15) 0.01633 (16) O1 0.0335 (6) 0.0250 (6) 0.0242 (6) 0.0104 (5) 0.0017 ...
8