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Powder XRD

Gel Growth, Powder XRD and FTIR Study of Magnesium Levo-Tartrate Crystals

Gel Growth, Powder XRD and FTIR Study of Magnesium Levo-Tartrate Crystals

... of powder XRD study, it is found that the powdered sample is crystalline in nature and confirms the unit cell parameters and d-values having orthorhombic ...

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Complex of Tris(Phenanthroline)Cobalt(II)Trifluoroacetate: Characterisation and Powder XRD Analysis

Complex of Tris(Phenanthroline)Cobalt(II)Trifluoroacetate: Characterisation and Powder XRD Analysis

... The powder complex of tris(phenanthroline)cobalt(II) trifluoroacetate (TFA) has been prepared by interaction of cobalt(II) nitrate, phenanthroline (phen) in aqueous solution with drops of ethanol, and an excess of ...

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Synthesis, Spectroscopic Characterization and Powder XRD Study of 4-(5-(Ethylthio)-1,3,4-Oxadiazole-2-yl) Aniline

Synthesis, Spectroscopic Characterization and Powder XRD Study of 4-(5-(Ethylthio)-1,3,4-Oxadiazole-2-yl) Aniline

... oriented powder samples enables us to obtain much important information on orientational and positional order of the molecular arrangements of liquid crystalline, which is essential for understanding their packing ...

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Growth, Characterization and Antibacterial Study of Sulfanilamide Doped by 4 Aminobenzoic Acid

Growth, Characterization and Antibacterial Study of Sulfanilamide Doped by 4 Aminobenzoic Acid

... To enhance the antibacterial activity of toxic drug compound sulfanilamide, it is doped by non-toxic compound 4- aminobenzoic acid by slow evaporation method. The powder XRD analysis shows that the doped ...

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Studies on the Synthesis, Spectral, Optical and Thermal properties of Zinc chloride doped L-Valine cadmium chloride crystals

Studies on the Synthesis, Spectral, Optical and Thermal properties of Zinc chloride doped L-Valine cadmium chloride crystals

... The title compound L-Valine Cadmium Chloride (LVCC) crystal doped with zinc chloride has been grown by the conventional slow evaporation technique. The sharp peaks from the observed powder XRD pattern of ...

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Synthesis and crystal structure of a neodymium borosilicate, Nd3BSi2O10

Synthesis and crystal structure of a neodymium borosilicate, Nd3BSi2O10

... the major phases within the residual glass matrix in some formulations of the glass-ceramic waste form for treatment of raffinate high-level waste (Crum et al., 2012, 2014, 2016). Studies on the crystal chemistry and ...

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Synthesis of Pure Nano semiconductor Oxide ZnO with Different AgNO3 Concentrations

Assist. Prof. Dr. Ali S. Al-Taie | Hiba S. Abd Alwahab

Synthesis of Pure Nano semiconductor Oxide ZnO with Different AgNO3 Concentrations Assist. Prof. Dr. Ali S. Al-Taie | Hiba S. Abd Alwahab

... 1. X-ray Diffraction (XRD) Studies The powder XRD for the synthesized compound (calcined at 500 °C for 3 hr) obtained from direct precipitation method of 3.0 g Urea and 4.7 g zinc nitrate is shown in ...

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Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation

Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation

... The powder XRD pattern of the bulk sample of ( 4 ) shows fair agreement with the pattern simulated from the single crystal structure (ESI † ), although the elemental analy- sis shows excess nitrogen ...

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Synthesis and Characterization of L Alanine Sodium Bromide: A New Semi Organic Nonlinear Optical Material

Synthesis and Characterization of L Alanine Sodium Bromide: A New Semi Organic Nonlinear Optical Material

... out to study the structural, optical and mechanical properties of the grown crystals. Single crystal X- ray diffraction analysis shows that the grown crystal belongs to the monoclinic system. The crystalline nature and ...

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Growth and Characterization of L-Proline Doped Adp Crystals for Optoelectronic Applications

Growth and Characterization of L-Proline Doped Adp Crystals for Optoelectronic Applications

... and powder XRD, FTIR, UV–vis NIR, SEM, EDAX Vicker’s microhardness and NLO studies to reveal their structures, spectral properties, optical transmittance, microstructural morphology, elemental composition, ...

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A solid state NMR method for solution of zeolite crystal structures

A solid state NMR method for solution of zeolite crystal structures

... Structure completion and refinements of the zeolite crystal structures against the powder XRD data were carried out using the atomic coordinates for the silicon atoms solved by solid-state NMR as the ...

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SINGLE DIFFUSION GEL GROWTH, SPECTRAL AND ANTIMICROBIAL ACTIVITY STUDIES ON 4-CARBOXYANILINE CRYSTAL

SINGLE DIFFUSION GEL GROWTH, SPECTRAL AND ANTIMICROBIAL ACTIVITY STUDIES ON 4-CARBOXYANILINE CRYSTAL

... the folic acid [1]. Even though, it is not fully recognized as vitamin because most people have colon bacteria that generate PABA from chorismate by the combined action of the enzymes [2]. It is naturally found in foods ...

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Synthesis of nano crystalline spatulae of lead zirconate titanate (PbZr0 52Ti0 48O3)

Synthesis of nano crystalline spatulae of lead zirconate titanate (PbZr0 52Ti0 48O3)

... Powder XRD pattern of as-ignited PZT powder (Figure 4a) shows broad and an ordered arrangement of peaks, indicating the formation of nano-crystalline lead zircon- ate titanate, presumably resulting ...

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Synthesis and characterization of SnO2 nano particles for carbon absorbing applications

Synthesis and characterization of SnO2 nano particles for carbon absorbing applications

... The SnO 2 nanoparticles was synthesized by Microwave assisted technique.From the powder XRD the particle size was calculated using Scherrer formula, it from 57 nm.The absorption spectrum was recorded from ...

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Elemental Compositions of Some Eye Shadow Products Marketed in Saudi Arabia

Elemental Compositions of Some Eye Shadow Products Marketed in Saudi Arabia

... a Powder XRD diffractometer (Model Equinox1000 – INEL (France) with Co K α ( λ = ...shadow powder sample was preparation, fixed into sample holders and located into the ...ICDD Powder Dif- ...

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Mechanical Analysis of the Effects of Different Mechanical Alloying Periods on Ni3Al Intermetallic Compound Fabrication Quality

Mechanical Analysis of the Effects of Different Mechanical Alloying Periods on Ni3Al Intermetallic Compound Fabrication Quality

... Simultaneous thermal analysis (STA), consisting of Simultaneous Differential Thermal Analysis (SDTA) and Thermogravimetric Analysis (TGA), was conducted on milled powder using TGA/SDTA 851 Mettler Toledo under ...

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Reactively Sputtered InVO4 Thin Films: Effect of Non Stoichiometric Composition on Photocatalytic Activity

Reactively Sputtered InVO4 Thin Films: Effect of Non Stoichiometric Composition on Photocatalytic Activity

... The crystallinity of the films was investigated by a Bruker D8 Advance X-ray diffractometer (XRD) operating with Cu K radiation at 40 kV and 100mA. Raman spectra for the films are recorded on RENISHAW 1000B ...

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Feasibility of the quantification of respirable
crystalline silica by mass on aerosol sampling
filters using Raman microscopy

Feasibility of the quantification of respirable crystalline silica by mass on aerosol sampling filters using Raman microscopy

... Variation of the Raman signal intensity of the silicon external standard measurement at the same position was < 2% when collected sequentially. Repeatability in different positions within a few minutes was ...

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FABRICATION OF FINE GRAINED DENSE HAP THROUGH SLIP CASTING ROUTE

FABRICATION OF FINE GRAINED DENSE HAP THROUGH SLIP CASTING ROUTE

... Hydroxyapatite (HAp), a major inorganic component of bone and teeth, has been used extensively for biomedical implant applications and bone regeneration due to its excellent bioactivity, biocompatibility and ...

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Preparation and Characterization of SnO2 Nanofibers via Electrospinning

Preparation and Characterization of SnO2 Nanofibers via Electrospinning

... for 4 h. Both spun and heat treated nanofibers are characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), Fourier transform infra red spectroscopy (FTIR) etc. XRD analysis of ...

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