[PDF] Top 20 Methyl 5 iodo 2 methoxybenzoate
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Methyl 5 iodo 2 methoxybenzoate
... planar [maximum deviation from benzene ring plane = 0.229 (5) A ˚ for the methyl carboxylate C atom] with the methyl groups oriented away from each other. In the crystal, molecules form stacked ... See full document
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Methyl 2 benzyloxy 6 (2 methyl 1,3 dioxolan 2 yl)benzoate monohydrate
... C3 0.0379 (9) 0.0354 (8) 0.0582 (10) −0.0099 (7) 0.0129 (8) −0.0018 (7) C4 0.0409 (9) 0.0350 (8) 0.0440 (9) −0.0027 (6) 0.0109 (7) −0.0063 (7) C5 0.0309 (8) 0.0301 (7) 0.0343 (7) 0.0035 (5) 0.0082 (6) 0.0018 (6) ... See full document
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(2R,3S,4S,5R) 4 Hydroxy 3 iodo 5 methyltetrahydro 2 furylmethyl benzoate
... The resulting solution was stirred at 263 K in the dark under argon (flask wrapped in aluminium foil). After 16 h, TLC analysis indicated that all of the starting material had been consummed (eluent; ether: petrol, 1:1). ... See full document
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Methyl 2,4 dihydroxy 5 (4 nitrobenzamido)benzoate
... O1 0.0365 (11) 0.0729 (14) 0.0296 (10) 0.0091 (10) 0.0093 (9) 0.0050 (10) O2 0.0332 (12) 0.0922 (17) 0.0453 (12) 0.0137 (11) 0.0146 (10) 0.0050 (11) O3 0.0351 (12) 0.0936 (17) 0.0440 (12) 0.0141 (12) 0.0216 (10) 0.0101 ... See full document
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Methyl 2 [4 (trifluoromethyl)phenylsulfanyl]benzoate
... reactant 2-(4-Trifluoromethylphenylsulfanyl)benzoic acid (I) was obtained as a gift sample from ...Na 2 CO 3 solution was added and the mixture stirred for 5 ... See full document
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{[2 Methyl 2 (phenoxymethyl)propane 1,3 diyl]bis(oxy)}dibenzene
... in THF (30 ml) at 273K. Phenol (4.23 g, 45 mmol) was added in portions to the stirred suspension over 1 h. The trifluoro- methanesulfonate solution was then slowly added to the sodium phenoxide solution at 273K to give a ... See full document
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Methyl 2 (4 methoxypyrimidin 2 ylcarbamoylsulfamoyl)benzoate
... The title compound was synthesized by condensation of 2-methoxy- carbonylbenzenesulfonyl isocyanate and 2-amino-4-methoxy- pyrimidine (Li et al., 1993). Single crystals suitable for crystallographic ... See full document
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Methyl 4 (5 methoxy 1H indol 3 yl)benzoate
... O1 0.0261 (4) 0.0340 (5) 0.0151 (4) −0.0048 (3) 0.0069 (3) 0.0006 (3) O2 0.0269 (4) 0.0248 (4) 0.0210 (4) 0.0003 (3) 0.0017 (3) 0.0020 (3) O3 0.0247 (4) 0.0209 (4) 0.0202 (4) −0.0035 (3) 0.0056 (3) −0.0013 (3) N1 ... See full document
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Methyl 2 (N methoxycarbonylmethyl N methylsulfamoyl)benzoate
... of methyl 2-(4-methoxypyrimidin-2-ylcarbamoylsulfamoyl)benzoate, (II) (Ma et ...planar methyl ester moiety (O1/O2/C7/C8) and SO 2 group at dihedral angles of ... See full document
8
Methyl 5 methoxy 2 nitro 4 [3 (piperidin 1 yl)propoxy]benzoate
... A solution of methyl 4-(3-chloropropoxy)-5-methoxy-2-nitrobenzoate (0.013 mol), potassium carbonate (0.052mol), sodium iodide (0.026mol) in acetonitrile (33 mL) was stirred for 5-10 min at ... See full document
7
Disorder in methyl 4 (3,5 dimethoxy 2 methylphenoxy) 2,6 dihydroxy 3 iodo 5 methylbenzoate
... of methyl 4-(2-carboxy-3,5-dimethoxy-6-methylphenoxy)-2,6-di- hydroxy-3-methylbenzoate with excess of methyl lithium (freshly prepared from methyl iodide and lithium), instead of the expected ... See full document
11
Methyl 2,6 bis(4,6 dimethoxypyrimidin 2 yloxy)benzoate
... intermolecular C—H O hydrogen bond (Table 2 and Fig. 2) and a – stacking interaction between the benzene rings [C7–C12 and C7 ii –C12 ii ; symmetry code: (ii) x, 2 y, z] (Fig. 3). The ... See full document
9
Methyl 2 {[3 (4,6 dimethoxypyrimidin 2 yl)ureido]sulfonylmethyl}benzoate
... O5 0.0351 (12) 0.0769 (18) 0.0383 (13) 0.0013 (12) 0.0046 (10) 0.0061 (12) C5 0.0336 (17) 0.062 (2) 0.0423 (18) −0.0094 (16) 0.0041 (14) −0.0014 (17) O6 0.0460 (14) 0.0707 (17) 0.0428 (13) 0.0023 (12) 0.0117 (11) ... See full document
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Methyl 3,5 bis[(3 chloropyrazin 2 yl)oxy]benzoate
... The bond distances and angles in the title compound (Fig. 1) agree very well with the corresponding bond distances and angles reported in a closely related compound (Nasir et al., 2010). In the title compound, the ... See full document
7
{rac 5 [Meth oxy(phen yl)meth yl] 10,20 diphenyl porphyrinato}nickel(II)
... Grignard reaction of the respective formylporphyrin to yield {5-[hydroxy(phenyl)methyl]-10,20-diphenylporphyrinato}- nickel(II), followed by crystallization from methylene chloride/methanol. The molecule ... See full document
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Crystal stucture of methyl 2 ({[2 (methoxycarbonyl)phenyl]carbamoyl}amino)benzoate
... Data collection: APEX2 Bruker, 2009; cell refinement: SAINT Bruker, 2009; data reduction: SAINT; programs used to solve structure: SHELXS97 Sheldrick, 2008; programs used to refine struc[r] ... See full document
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Methyl 2,4 dihydroxy 5 (2 methylpropanamido)benzoate
... H O hydrogen bonds generate S(5) and S(6) rings, respectively. In the crystal, molecules are linked by O— H O hydrogen bonds, generating C(7) chains propagating in [001]. Weak aromatic – stacking ... See full document
7
Methyl 2 (methoxyacetylamino)benzoate
... Methyl 2-(methoxyacetylamino)benzoate, (I), is an important intermediate in the chemical industry (Aavid et al., 1949) and is used extensively in medicine and pesticides (Stephen et al., 2002). For ... See full document
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Crystal structure of methyl 2 hydroxy 5 [(4 oxo 4,5 dihydro 1,3 thiazol 2 yl)amino]benzoate
... C8 0.0461 (11) 0.0347 (9) 0.0216 (9) 0.0007 (8) 0.0059 (8) −0.0030 (7) C9 0.0301 (9) 0.0228 (7) 0.0175 (7) 0.0012 (6) −0.0018 (6) −0.0013 (6) C10 0.0413 (10) 0.0240 (8) 0.0253 (9) 0.0047 (7) −0.0066 (7) −0.0003 (7) C11 ... See full document
11
Crystal structure of 5 iodo 2 methyl 3 [(4 methylphenyl)sulfonyl] 1 benzofuran
... iodo-2-methyl-3-(4-methylphenylsulfanyl)-1-benzofuran (342 mg, 0.9 mmol) in dichloromethane (30 ml) at 273 K. After being stirred at room temperature for 10h, the mixture was washed with saturated ... See full document
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