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Document ID Number
30809
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~ ~’~" Golder Associates Inc,
~
1751 West Count~ Rood B, Suite 105 Rosevllle, MN USA 55113-4037 Telephone (6511 697-9737 Fox (651) 697-9735July 22, 2009 Project No.:023-6105.009
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Metropolitan Council Environmental Services Industrial Waste Division
390 Robert St. N.
St. Paul, MN 55101
Attention: Mr. Berhane Worku
RE: 2009 SECOND QUARTER SPECIAL DISCHARGE REPORT INDUSTRIAL DISCHARGE PERMIT NUMBER 2289
SOUTHEAST PUMP AND TREAT SYSTEM CANADIAN PACIFIC SHOREHAM FACILITY
Dear Mr. Worku:
On behalf of Canadian Pacific, enclosed is the 2009 Second Quarter Special Discharge
Report for the site located at 28th & Central Avenue NE, Minneapolis MN. In accordance with Metropolitan Council Environmental Services (MCES) Industrial Discharge Permit Number #2289 dated October 1, 2007 (MCES permit), this submittal documents the volume of treated water discharged from the pump and treat system owned by Canadian Pacific.
The total quantity of water discharged into the sanitary sewer system during this reporting quarter was approximately 3,007,100 gallons. The average dally discharge for the system was 33,045 gallons.
The required information for the discharge is provided as follows:
* Attachment A- Special Discharge Report.
e Attachment B - analytical data from Pace Analytical Inc. for the April 2009 monthly sampling event.
o Attachment C - analytical data from Pace Analytical Inc. for the May 2009 month!y sampling event for pH only.
e Attachment D - analytical data from Pace Analytical Inc. for the June 2009 sampling event.
The analytical results from these sampling events showed that the treated discharges water was in compliance with the MCES permit discharge limitations during this reporting period.
OFFICES ACROSS ASIA, AUSTRALASIA, EUROPE, NORTH AMERICA, ~OUTH AMERICA
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MCES July 22, 2009
Mr. Berhano Wod~u -2- 023-6105
If you have any questions or comments, please do not hesitate to contact Barbara Johnson at (651) 697-9737. Thank you for your assistance in this matter.
Very truly yours,
GOLDER ASSOCIATES INC.
Ms. Barbara Johnson, PE Senior Project Engineer
Mr. Michael Morris, PG
Associate and Senior Consultant
Ms. LeeAnn Thomas, CP Mr. Chris Munson, Goldcr
Golder Associates
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Attachment A
SPECIAL DISCHARGE REPORT
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Metropolitan Council Environmental Services Industrial Waste & Pollution Prevention Section 390 Robert Stoat North
St. Paul, Minnesota 55101-1805
For MCES Use Only Permit!Approval No:
Staff:
Received: O L 45 E
Special Discharge ReDor
0~008
1. Permittee*: Canadian Pacific Railway - Permit 2289
*The co~poratinn, proprietorship, government unit or individual that was issued the MCES Permit or Approval Letter.
2. Site Address: 28t~ and Central Avenue NE, Minneapolis, MN
Billing Address or Mailing Address Changed? [] Yes [] No lfYas, attach the change(s).
3. Reporting PeHod:
A. [] Jan-Mar, 20__ [] Apr-Jun, 2009 [] JuI-Sep, 20__ [] Oct-Dec, 20__
B. [] Jan-Dec, 20__
C. [] Short-Term Discharge Start Date: End Date:
Discharge Information:
Indicate whether the wastewater was discharged on-site and/or hauled during this reporting perind, and complete the associated questions. If an wasteweter was disposed to MCES during this reporting period, indicate no discharge.
[] No Discharge to MCES during this reporting period If no discharge was selected, proceed directly to Item #10.
[] On-Site Discharge
A. Total volume discharged during this reporting period (gallons):
B. Total days of discharge during this reporting period (days):
C. Average volume discharged per day (galloas/day):
D. Method of volume determination for this period:
[] Hauled Discharge
A. Total number of loads hauled during this reporting period:
B. Total volume hauled during this reporting period (gallons):
C. Total days of discharge during this reporting period (days):
D. Average volume per discharge day (gallons/day):
E. Method of volume determination for this period:
3~007,100 91
33,045
Effluent flowmater
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Sampling Information:
A. Number of sampling events during this reporting period: 4
B. Sample(s) collected by: [] Permittee [] Other, name Golder Associates Inc.
C. Describe method of sample collection:
Grab samples were collected at pre-inntalled sample ports. Effluent is denoted as "SE P&T Effluent" or "SP01 Effluent"
D. Sample(s) analyzed by: [] Permittee [] Other, name Pace Analytical Services
E, Were all samples collected acenrding to MCES requirements?[]Yes [] No If NO, attach an explanation.
This form is available in electronic format at:
h~.metrocouncil.org/environmenfflndustrialWasle/fom~s.hlm_ Page I o1"2
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6. Sample Results: In the table below (or an MCES-approved alternative), entar the values for eanh sampling event during the reporting period. If there is more than one sampling point, attach a separate table to provide the information. In addition to completing the information in the table below, list the parameters and results for analytical values that are > 0.100 mg/L.
Sampling Point Sample Date pH
TSS COD
Results Averages ~-¢ ] Unit~
SP: OI De~dption: Effluent
4116/2009 5112/2009
NS NS
NS N5
6/I 1/2009
7.2 7.2 Units
<0.17 <0.17 mgJL
NS 58.9 58.9
mg/L
VOC ~sults are in Atiaehra©nts B, C~ D
Parameters (Other)
Thc~ arc no paramctm’~ that ~gceed 0.100 mg/L (100 jig/L), mg/Lmg~L mg/L
mg~L mg~L mg/L NA - Not Available. Parameter was not analyzed.
NS - Not Sampled. Analyte is required on a quarterly basis; not monthly.
7. Data Sheets: Are laboratory data sheets fi’om all wastewater sampling events included with this report?
[] Yes [] No If No, attach an explanation.
9.
10.
Representative Discharge: Are the analytical results, for Item #6 above, representative of the wastewater discharged during this reporting period? [] Yes [] No If No, attach an explanation.
Compliance Status: All values reported during the reporting period are: [] In compliance [] Not in corapliance with MCES Discharge Liraitations.
Process Changes:
a. Have there been any significant process problems/changes during this reporting period?
[] Yes [] No IfYas, attach an explanation.
b. Are there any planned or expected future changes that will impact discharge volume or quality?
[] Yes [] No If Yes, attach an explanation.
11. Certification Statement*:
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gather and evaluate the information submitted. Ba~ed on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. [ am aware that there are significant penaltie~ under law for submitting false information, including the possibility of fine and imprisonment for knowing violations.
Authorized Representative
Name (print): Barbara Johnson~ PE Title: Canadian Pacific
Email: [email protected] Phone: 651-336-9885
fur
*This report must be signed by the authorized representative or designated representative.
Page 2 of 2
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Attachment B
ANALYTICAL RESULTS FOR TREATED GROUNDWATER
April 2009
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. ,~ace Analytical"
A~ 23,
Psce Analytical ~e~lce=, Inc.
1241 Bellevue Street - Suite 9 Green Bay, W~ 54302 (~20)46~2436
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Patricia Landes
Golder Associates, tnc.
200 Century Parkway Suite C
Mount Laurel, NJ 08054
RE: Project: East Side P&T WO 901 Pace Project No.: 4016184 Dear Patricia Landes:
Enclosed are the analytical results for sample(s) received by the laboratory on April 17, 2009. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laurie Woelfel
[email protected] Project Manager
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REPORT OF LABORATORY ANALYSIS
Thie report shell not be reproduced, except In full, without the w~lten consent of pace Analy~cal Servicas, Inc..
Page I of 25
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Project: East Side P&T ~ 901 Paco Project No.: 4016184
CERTIFICATIONS
Green Bay Certification ID~
Wisconsin DATCP Cartlficaaon #: 105-444 V,~laconsln DATCP Certification #: 105-444 Wisconsin Certification #: 405132750 Wisconsin Certification #: 405132750 South CamJ~na CertJ~catJon #: 83006001 South Carolina Codification #: 830~6001 North Dakota Certification #: R-200 North Dakota Certification #: R-150 North Carolina Certification #: 503 North Carolina Certification #: 503 New York Certification #: 11887
New York Ce~flca0on #: 11888 Minnesota Certlflcatton #: 055-999-334 Minnesota Certlflca0on #; 055-999-334 Louisiana Certification #: 04189 Louisiana Ced~t~t/on #: 04188 Kentucky Certification #: 83 Kentucky Certification #: 82 Illinois Certification #: 200051 Illinois Certification #: 200050 Flodda/NELAP Certification #: E87851 Flodda/NELAP Certification #: E87848
Pmc¢ AnllytJcal 8ervlcu, Inc.
1241 Bellevue Street - Suite O Green Bay, ’~M 54302 (920)469-2438
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REPORT OF LABORATORY ANALYSIS
This mpori sbel~ not be reproduced, except in full, w~lhout the wdtten consent of P~.~ AnalytlcaJ SaUces, Inc..
Page 2 of 25
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~ceAnalytical °
Project:
Pace Project No.:
LablD 4016184001 4018184002 4018184003 4016184004 4016184005 4018184006 4016184007 4019184008
East S~e P&T WO901 4016184
Sample ID RW07-39-SP RWOT-40-SP RW08.29-1 RW07-38.1 RWO6.27.BR 8E P&T BETWEEN SE P&T EFFLUENT TRIP BLANK
SAMPLE SUMMARY
Matrix Date Collected Date Received Water 04/16/09 13:49 04/17/09 08:30 Water 04/16109 13:53 04/17109 08:30 V~ter 04/16/09 13;59 04117109 08:30 Water 04116109 14:01 04117109 08:30 Water 04116/09 14:05 04117109 08:30 Water 04/16/09 14:09 04117/09 08:30 Water 04116109 14:16 04117109 08:30 Water 04116/09 00:00 04117/09 08:30
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, ex~pt In full, without the w~aen (~onsent of Pace Analy~lcaJ Se~,~ces, Inc..
Page 3 of 25
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Project: East Side P&T WO 001 Pace Project No.: 4018184
Lab IO Z]emple ID
4018184001 RW07-39-Sp 4016184002 I~NO7-40-SP 4016184003 RIN08-28-1 4016184004 RW07-~8-I 4016184008 R~KIS-27-BR 4018184006 8E P&T BETWEEN 4018184007 SE P&T EFFLUENT 4016184008 TRIP BLANK
8AMPLE ANALYTE COUNT
Method Ane~et$
EPA8260 JJB
EPA8260 JJB
EPA8260 JJB
EPA8260 JJB
EPA 8280 JJB
EPA8260 JJB
EPA8260 JJB
EPA8260 JJB
71 PASr-G
71 PASI-G
71 PASI-G
71 PASI-G
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REPORT OF LABORATORY ANALYSIS
Page 4 of 25aceAnalytica/"
/
1241 Bellevue Street - Suite 9 Groan Bay, ~1 54302 (920)ze~.2438
ANALYTICAL RESULTS Project: r:ast Side P&T we 80!
Pace Project No,: 4018184
Sample: RW97-39-Sp Lab tO: 4016184001 Collected: 04116/09 13:49 Received: 04117/0008:30 Mstdx: Water
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Parameters Results Unite PQL MDL DF Prepared Analyzed CAS No, Qusl
8260 MSV Ana~lJcal Method: EPA 8280
Acetone <25.0 uglL 100 25.0 5 04/21/09 11;16 67-64-1
Allyl chlodde <10.0 ug/L 25.0 10.0 5 04/21109 11:18 107-05-1
Benzene <2.0 ug/L 5.0 2.0 5 04/21/09 11:16 71-43-2
Bromobenzene <4,1 uglL 5,0 4.1 5 04/21/09 11:16 108-88-1
Bromochloromethane <4,8 ug/L 5.0 4,8 5 04/21/00 11:16 74-97-5
Bromodlchlommethsne <2.8 ug/L 5,0 2,8 5 04/21/09 11:16 75-274
Bromoform <4,7 uglL 5,0 4,7 5 04/21/09 11:16 75-25-2
Bmmomethsne <4.6 ug/L 5,0 4,6 5 04/21/00 11:16 74-83-9
2-Butenone (Mr:K) <21.6 uglL 100 21,5 5 04/21/09 11:16 78-93-3
n-Butylbenzene <4,6 ug/L 5,0 4,6 5 04/21/09 11:18 104-51-8
sec-Butylbenzene <4.4 uglL 25.0 4,4 5 04/21/00 11:16 135-98-8
tert-Butylbenzene <4.8 ug/L 5,0 4.8 5 04/21/09 11:16 95-08-6
Carbontetrschlor~de <2.4 uglL 5,0 2.4 5 04/21/09 11:16 55-23-5
Chlorobenzerle <2.0 ug/L 5.0 2.0 5 04/21/00 11:16 108-00.7
Chloroethane <4.8 uglL 5,0 4.8 5 04/21/09 11:16 75-00-3
Chloroform <6.5 uglL 25,0 6.5 5 04/21/09 11:16 6766-3
Chloromethane <1.2 uglL 5,0 1,2 5 04121109 11:18 74-87-3
2-Chlorotoluene <4.2 ug/L 5,0 4,2 5 04/21100 11:16 95-49-8
4-Chlomtoluene <5.7 uglL 5,0 3.7 5 04/21/09 11:16 108-43-4
Dlbromochlommethane <4,0 uglL 5,0 4,0 5 04/21/00 11:16 124-48-1
1,2-DIbromoethane (EDB) <2,8 uglL 5.0 2,8 5 04/2110011:16 106-03-4
Dibromomethene <3,0 uglL 5.0 3,0 5 04/21/09 11:16 74-95-3
1,2-Dichlombenzene <4.2 uglL 5,0 4,2 5 04/21/09 11:16 95.50-1
1,3-Dichlorobenzene <4.4 ug/L 5,0 4,4 5 04121109 11:16 541-73-1
1,4-DIchlorobenzene <4,8 ug/L 5.0 4.8 5 04/21/09 11:18 106-46-7
Dlchlorodifluommethsne <5,0 ug/L 5,0 5,0 5 04121/08 11:16 75-71-8
1,1-DIchloroethene 63.0 ug/L 5,0 3,8 5 04121/09 11:16 75-34-3
1,2-DIchloroethane <1.8 ug/L 5,0 1,8 5 04/21109 11:16 107-06-2
1,l-Dlchloroethene 38.7 ug/L 5.0 2.8 5 04121/00 11:10 75-35-4
cls-l,2-Dichloroethene 42,4 ug/L 5.0 4.2 5 04121/09 11:16 156-59-2
trans-l,2-DIchloroethene <4,4 ug/L 5.0 4.4 5 04121/0911:16 158-60.5
Dichlorofluommethane <4.4 ug/L 5.0 4,4 5 04/21/09 11:16 75-43-4
1,2*DIchloropropane <2,4 ug/L 5,0 2.4 5 04121109 11:16 78-87-5
1,3-DIchloropropsne <3.0 ug/L 5,0 3.0 5 04/21/09 11:16 142-28-0
2,2-Dlchloropropene <3.1 ug/L 5,0 3.1 5 04/21109 11:16 594-20-7
1,1-Dichloropropene <3.8 ug/L 5.0 3,8 5 04121109 11:16 563-58-6
cls-l,3-DIchlompropene <1.0 ug/L 5,0 1,0 5 04/21/09 11:16 10081-0%5
trans-l,3-Dlchloropropene <0.08 ug/L 5.0 0.95 5 04121109 11:16 10061-02-6
Dlethyl et~er ~Ethy~ ether) <4.9 ug/L 5,0 4.9 5 04/21/09 11:16 60-20-7
Ethylbenzene <2,7 uglL 5,0 2.7 5 04/2110911:1fl 100-41-4
Hexachloro-l,3-butedlene <3,4 ug/L 25.0 3.4 5 04/21/09 11:16 87-60-3
Isopmpylbenzene (Cumene) <3,0 ug/L 5,0 3,0 5 04/21/09 11:16 98-82*8
p-lsopropyltoluene <3.4 ugiL 5.0 3.4 5 04/21100 11:16 99-87-6
Methylene Chloride 2.6J ug/L 5,0 2,2 5 04/21/09 11;16 75-08-2
4-Methyl-2-pentanone(MIBK) <6.0 ugiL 25.0 6.0 5 04/21/0911:16 108-10.1
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This report sh=dl not he reproduced, exc~p~ in full,
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ANALYTICAL RESULTS
Project: East Side P&T ~NO 801 Pace Project No,: 4016184
8ample: RINOT-39-SP Lab ID: 4016184001 Collected: 04119/09 13:49 Received: 04117/09 08;30 Metrlx: Water
Parameters Results Units PQL MDL DF Prepared Analyzed C.AS No. Qual
8260 Mev Analytical Method: EPA 8260
3.0 4.4 Methyl-ted-butyl ether <$.0 ugiL 5.0 5
Naphthalene <4.4 uglL 25.0 5
n-Propylbenzene <4.0 uglL 5.0 4.0 5
Styrene <4.3 uglL 5.0 4.3 5
1.1.1,2-Tetrachloroethane <4.6 uglL 5,0 4.8 5
1,1.2,2-Tetrachloroethane <1.0 uglL 5.0 1.0 5
Tetrachlomethene t0,10 uglL 5.0 2.2 5
Tetrahydrofuran <8.8 uglL 25.0 8.5 5
Toluene <6.4 uglL 5.0 3.4 5
1,2,3-Tdchlorobanzene <3.7 uglL 5.0 3.7 5
1,2,4-TrichloroherBene <4.6 uglL 5.0 4.8 5
1,1,1 -Trlchloroethane 271 uo/L 53 43 5
1,1,2-Trichloroethane <2.1 ug/L 5.0 2.1 5
Tdd~loroethene ~ 38.6 uglL_ 5.0 2.4 5
Tdc~loro~luoromethane <4.0 uglL 5.0 4.0 5
1,2,3-Tdchloropropane <5.0 ug/L 5.0 5.0 5
l,l,2-Trichlomtdfluomethana <6.4 ug/L 25.0 6.4 5
1,2.4-Trimethy}benzena <4.8 ug/L 8.0 4.8 5
1,3,5-Trlmethylbenzena <4.2 ug/L 5.0 4,2 5
m&p-Xyfene <6.0 ug/L 10.0 9.0 5
o-Xylena <4.2 ugiL 5.0 4.2 5
4-Bromofiuorobenzene (S) 88 % 70-130 5
Dibromofluoromethane (S) 117 % 70-130 5
Toluene-d8 (S) 97 % 70-130 5
04/21109 11:16 04/21/09 11:16 04/21109 11:16 04/21/09 11:16 04121/09 11:16 04121109 11:16 04121109 11:18 04121/09 11:16 04/21/09 11:16 04/21/09 11:16 04/21/09 11:16 04/21/09 11:16 04/21/09 11:18 04121/09 11:16 04121109 11:16 04121/09 11:16 04/21/09 11:16 04/21/09 11:16 04/21/09 11:16 84/21/09 11:16 04/21/09 11:16 04/21/09 11:18 04/21/09 11:16 04/21109 11:16 04/21/09 11:16
1634.04-4 91-20-3
630-20-6 79-34-5
127-18-4 109-99-9 108-88-3 87-61-6
120-82-1 71-55-6 79-00-5 75-69-4 98-18-4 95.63-6 105-67-8 76-01-4 1330-20-7 95-47-9 460-00-4 1868-53-7 2037-26-5
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Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
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../ cace Analytical "
ANALYTICAL RESULTS
Pace Analytical Services, Inc, 1241 Bellevue Street - Suite 9
Green Bay, "W1 54302 (920)4892436
Proiact: East Side P&T we 901 Pace Project No.: 4016184
8erupts: RWO7-40-eP Lab ID: 4016184002 Collected: 04116/09 13:53 Received: 04/17/09 08:30 Matdx: Water
Parameters Reeulte Units PQL MDL OF Prepared Analyzed CAS No. Qual
0280 MeV AnelyiIcal Mefhod: EPA 8260
Acetone <26.0 ug/L 100 25.0 5 04121/09 17:13 67-64-1
Allyl chlodde <10.0 ug/L 25.0 10.0 5 04121/09 17:13 107.65-1
Benzene <2.0 ug/L 5.0 2.0 5 04/21/09 17:13 71-43-2
Bromobenzene <4.1 ug/L 5.0 4.1 5 04121/09 17:13 108.68-1
Bromochloromethane <4.0 ug/L 5.0 4.8 5 04121/09 17:13 74-07-5
Bromodichloromelhane <2.8 ug/L 5.0 2.8 5 04121/09 17:13 75-27-4
Bromoform <4.7 uglL 5.0 4.7 5 04121/09 17:13 75-25-2
Bromomethene <4.8 uglL 5.0 4.6 5 04121/09 17:13 74-83-9
2-Butanone (MEK) <21.8 uglL 100 21.5 5 04/21/09 17:13 78-93-3
n-Butylbenzene <4.0 ug/L 5.0 4.6 5 04121/09 17:13 104-51-8
sec-Butylbenzene <4A ug/L 25.0 4.4 5 04/21/09 17:13 135.98-8
tart-Butylbenzene <4.8 ug/L 5.0 4.8 5 04121/09 17:13 08.68-6
Carbontetrachlorlde <2.4 ug/L 5.0 2.4 5 04/21/09 17:13 56-23-5 L1
Chlorobenzene <2.0 ug/L 5.0 2.0 5 04/21/09 17:13 108-90-7
Chloroethane <4.8 ug/L 5.0 4.8 5 04/21/09 17:13 75-00-3
Chloroform <6.0 uglL 25.0 6.5 5 04/21/09 17:13 67.66-3
Chlommethene <1.2 uglL 5.0 1.2 5 04/21/09 17:13 74-87-3
2-Chlorotoluene <4,2 uglL 5.0 4.2 5 04/21100 17:13 95-40-8
4.Chlorotoluene <3.7 ug/L 5,0 3.7 5 04/21/00 17:13 106-43-4
1.2.Dlbrome-3-ch!oropmpane <8.4 ug/L 25.0 8.4 5 04/21/09 17:13 013-12.6
Dibromochlaromethene <4.0 ug/L 5.0 4.0 5 04/21109 17:13 124-48-1
1.2-Olbromoethane (EDB) <2.0 ugA. 5.0 2.8 5 04/21109 17:13 108-03-4
Dlbromometha,e <3.0 ug/t. 5.0 3.0 5 04/21/09 17:13 74-95-3
1.2-Dlchlorobenzene <4.2 ug/L 5.0 4.2 5 04/21109 17:13 98-50-1
1.3-Dichlorobenzene <4.4 ug/L 5.0 4.4 5 04/21109 17:13 541-73.1
1.4-Dichlorobenzene <4.8 uglL 5.0 4.8 5 04/21100 17:13 106-46-7
DIchlorodifluoromethane <5.0 uglL 5.0 5.0 5 04/21/09 17:13 75-71.6
1,1-D[chlomathane 8.3 ug/L 5.0 3.8 5 04/21/00 17:13 75°34-3
1,l-Dlchloroethene 8.3 uglL 5.0 2.8 5 04/21109 17:13 75-35-4
cis-l,2-Dlchloroethene 7.6 uglL 5.0 4.2 5 04/21109 17:13 156-50-2
trana*l,2-Dichloroethene <4.4 uglL 5.0 4.4 5 04/21109 17:13 150-60-5
Dichlorofluommethane <4.4 uglL 5,0 4.4 5 04/21109 17:13 75-43-4
1,2-DIchlompropane <2.4 uglL 5.0 2,4 5 04/21/09 17:13 78-87-5
1,3-Dichloropropane <3,0 uglL 5.0 3.0 5 04/21109 17:13 142-28-0
2,2-Dlchloropropane <3.1 ugiL 5,0 3.1 5 04/21100 17:13 594-20-7
1,1-Dlchloropropene <3.8 uglL 5.0 3,8 5 04/2tl09 17:13 563-58-6
cLe-l,3-Dichloropropene <1.0 uglL 5.0 1.0 5 04/21100 17:13 10061-01-5
trans-l,3-Dlchlompropene <0.06 uglL 5.0 0.95 5 04/21/09 17:13 10061-02-6
Dlethylether (Ethylethe~) <4.0 ug/L 5,0 4.9 5 04121/0917:13 60-20-7
Ethylbenzene <2.7 ug/L 5.0 2.7 5 04/21/09 17:13 100-41-4
Hexachlomol,3-butadlene <3.4 uglL 25.0 3.4 5 04121/09 17:13 87-60-3
Isopropylbenzene (Cumene) <3.0 ug/L 5.0 3.0 5 04/21109 17:13 98.62.6
p-lsopropyltoluene <3.4 ug/L 5.0 3.4 5 04/21109 17:13 99-87-6
Methylene Chloride 2.6J ug/L 5.0 2.2 5 04/21/09 17:13 75.69-2 Z3
4-Methyl-2-pentenone (MiBK) <8.0 ug/L 25.0 6.0 5 04/21/09 17:13 108-10-1
REPORT OF LABORATORY ANALYSIS
Thi= report eha~l not be reproduced, except in full, without the wflben coneent of pace An~Jytlcal Services, Inc..
Date: 0412312009 08:53 AM Page 7 of 25
Pace Analytical Barrio=e, Inc, 1241 Bellevue Street - Suite 9 Green Bay, W1 54302 (~20)48B-2436
I I I I I I I I I I
ANALYTICAL RESULTS
Project: East Side P&T WO 901 Pace Project No.: 4016184
Sample: RWO7-40-SP Lab ID: 4016184002 Collected: 04116/99 13:53 Received: 04/17/09 08:30 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Analytical Method: EPA 8260
Methyl-tedobutylether <3.0 uo/L 5.0 3.0 5 04/21/0817:13 1634-04-4
Naphthalene <4.4 uglL 25.0 4.4 5 04/21/09 17:13 91-20-3
n-Propylbenzane <4.0 uo/L 5.0 4.0 5 04/21/09 17:13 103-65-1
Styrene <4.3 uglL 5.0 4.3 5 04/21/09 17:13 100-42-5
l,l,!,2-Tetrechloroethace <4.0 uglL 5.0 4.6 5 04/21/09 17:13 830-20-6
1,1,2,2-Tetrachforoethane <t.0 uglL 5,0 1.0 5 04/21/09 17:13 79-34-5
Tetrachlorcethene 200 ug/L 5,0 2.2 5 04/21/09 17:13 127-18~4
TatrehydrofiJran <8.0 ug/L 25.0 8.5 5 04/21/08 17:13 100-98-9
Toluene <3.4 uglL 5.0 3.4 5 04/21/09 17:13 108-08-3
1,2,3oTdchlombenzece <3.7 uglL 5.0 3.7 5 04/21/09 17:13 87-81-6
1,2,4-Tdchlorobenzena <4,8 ug/L 5.0 4.8 5 04/21/09 17:13 120-02-1
1,1,1°Tdch~omethane 71.2 ug/L 5.0 4.5 5 04/21/00 17:13 71-55-0
1,1,2oTrlchloroethene <2.1 ug/L 5.0 2.1 5 04/21/00 17:13 78,60-5
Trichloroethene 24.2 ug/L 5.0 2.4 5 04/21/00 17:13 79-01-6
Tdchlom/]uommethane <4.0 uglL 5.0 4.0 5 04/21/08 17:13 75-69-4
1,2,3-Trichlorepropana <8,0 ug/L 5.0 5.0 5 04/21/00 17:13 96-18-4
1,1,2-Trichlorotdfluoreethane <8.4 uglL 25.0 6.4 5 04121/00 17:13 76-13-1
1,2,4-Tdmethylbenzena <4.8 ug/L 5.0 4.8 5 04/21/09 17:13 95,60-6
1,3,5-Trlmethy[benzena <4.2 ug/L 5.0 4.2 5 04/21/08 17:13 108-67-8
Vinyl ch~odde <0.90 ug/L 5.0 O.8O 5 04/21/99 17:13 75-01-4
m&poXylena <9.0 ug/L 10.0 9.0 5 04/21/99 17:13 1330-20-7
o-Xylane <4.2 uglL 5.0 4.2 5 04/21100 17:13 90-47-0
4-Bromofluorobenzene (S) 87 % 70-130 5 04/21109 17:13 400-00-4
Dibromofluoromethene (S) 121% 70-130 5 04/21189 17:13 1860-53-7
Toluene-d8 (S) 97 % 70-130 5 04/21/09 17:13 2037-26-5
I I I
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This reporl ihell not be reproduced, except in full,
Page 8 of 25
. aceAnalj/tical"
PaceAnelytlcalSe~lces, foc, 1241BellevueStre~ - Suite 9Green Ss~WI54302 (920)469-2430
ANALYTICAL RESULTS Project: East Side P&T ~NO 901
Pace Project No,: 4016184
Sample: RW08-28.1 Lab ID: 4018184003 Collected: 04116/09 13:59 Received: 04/17/09 08:30 Metdx: Water
I I I I I I I I I I I I I I I
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No, Qual
8280 MSV Analytical Meth(~d: EPA 8260
Acetone <8.0 ug/L 20.0 5,0
Allyl chlodde <2,0 ug/L 5.0 2.0
Benzene <0.41 ug/L 1.0 0,41
Bromobenzene <0,82 ug/L 1,0 0.82
Bromochloromathane <0.97 ug/L 1.0 0.97
Bromodlct~lommethane <o.r~ ug/L 1.0 0.56
Bmmoform <0,84 uglL 1.0 0.94
Bromomethane <0.91 ug/L 1,0 0.91
2-Butsnone (MEK) <4.3 uglL 20.0 4,3
n-Butylbenzene <0.03 ug/L 1,0 0.93
sec-Butylbenzene <0.89 ug/L 5.0 0.89
tert-Butylbenzene <0.87 ugiL 1.0 0.97
Carbon tetrac~loride <0.40 aglL 1,0 0,49
Chlorobenzene <0AI ug/L 1.0 0,41
Chloroethane <0.97 uglL 1,0 0,97
Chloroform <1.3 uglL 5.0 t.3
Chloromethsne <0.24 uglL 1.0 0,24
2-Chlerotoluene <0.86 ug/L 1,0 0,85
4-Chlorotoluene <0.74 ug/L 1,0 0.74
1,2-Dlbromo-3-chlompmpane <1.? ug,q. 5.0 1.7
Dfbromochloromethana <0.8t uglL 1,0 0.81
1,2-Dibromoethane (EDB) <0.50 uglL 1,0 0,56
Dibromomethane <0,80 uglL 1,0 0.60
1,2-Dichlorobanzene <0,8~ ug/L 1,0 0,83
1,3-Dichlorebenzene <0.87 uglL 1,0 0.87
1,4-Dichlorobenzene <0.86 ug/L 1.0 0,95
Dichlorodifluoromathane <0.99 uglL 1,0 0.99
1,1-Dtchloroethene 9.4 ug/L 1,0 0,75
1,2-Dlchlorcathane <0.36 uglL 1,0 0.36
l,l-Dichlomathena 8.3 uglL 1,0 0,57
cis-l,2-Dlchloroathene 4,4 uglL 1,0 0,83
trans-1,2-Dic~loroathane <0.80 ug/L 1.0 0.89
DIchlorofluoromethane <0.88 uglL 1,0 0,88
1,2-DIchloropropane <0.40 uglL 1.0 0.49
1,3-Dlchloropropane <0.01 uglL 1,0 0,61
2,2-Dichloropropana <0.82 uglL 1,0 0,62
1,1-DIchloropropene <0.70 uglL 1,0 0.75
cis-l,3-Dichlompropene <0,20 uglL 1,0 0.20
trans-l,3-D]chloropmpsne <0,10 uglL 1.0 0.19
Dlethyl ether (Ethyl ether) <0.98 ug/t. 1,0 0.98
Ethylbenzane <0.M ug/L 1.0 0.54
Haxachloro-l,3-butsdlene <0.67 ug/L 5.0 0,87
Isopropylbenzene (Cumene) <0.90 uglL 1.0 0.59
p-lsopropyltoluane <0.67 ug/L 1.0 0,67
Methylene Chloride <0.43 ug/L 1,0 0A3
4-Methyl-2-pentsnone (MIBK) <t.2 uglL 5,0 1.2
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This repo~ shall not be reproduced, ~xc~ pt in full, w~hout the written consent of Pace Analytical Serials. Inc,.
04/21109 12:51 67-64-1 04/21/0012:51 107-05-1 04/21/09 12:51 71-43-2 04121109 12:51 108-88-1 04121100 12:51 74-97-5 04/21/09 12:51 78-27-4 04121109 12:51 75-25-2 04/21/09 12:51 74-83-9 04/21/09 12:51 78-93-3 04/21/09 12:51 104-51-8 04/21/09 12:51 135-98-8 04/21/09 12:51 98-00-6 04/21109 12:51 56-23-5 04/21/09 12:51 108-90-7 04121/09 12:51 75-00-3 04/21109 12:51 57-66-3 04/21/09 12:51 74487-3 04121/09 12:51 95-49-8 04121109 12:51 106-43-4 04/21/09 12:51 90-12-6 04121/09 12:51 124-48-1 04/21/09 12:51 106-93-4 04/21109 12:51 74-95-3 04121/09 12:51 95-50-1 04/21109 12:51 541-73-1 04/21/09 12:51 108-46-7 04/21/09 12:51 75-71-8 04121/09 12:51 75-34-3 04/21109 12:51 107-06o2 04/21/09 12:51 75-35-4 54/21/09 12:51 156-59-2 (}4/21/09 12:51 156-60-5 04/21109 12:51 75-43-4 04/21109 12:51 78-87-5 04/21109 12:51 142-28-9 04/21109 12:51 594-20-7 04/21100 12:51 563-58-6 04/21/09 12:51 10081-01-5 04121/09 12:51 10061-02-6 04/21/09 12;51 80-29-7 04/21/0912:51 100-41-4 04/21/09 12:51 87-68-3 04/21/0912:51 98-82-8 04/21/0912:51 99-87-6 04/21/09 12:51 75-09-2 04/21/0912:51 108-10-1
L1
Page 9 of 25
(S20)4SS-2438
I I I I I I I I I I
ANALYTICAL RESULTS
Project: East Side P&T We 901 Pace Project No.: 4016184
Sample: RW06-28-1 Lab ID: 4016184003 Collected: 041!6/09 13:59 Received: 04/17/09 08:30 Matdx: ~h~zter
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Analytical Method: EPA 8260
Methyl-te~-butylether <0.81 ug/L 1.0 0.61 1 04/21109 12:51 1634-04-4
Naphthalene <0.89 uglL 5.0 0.89 1 04/21/09 12:51 91-20-3
n-Propylbenzene <0.0t uglL 1.0 0,8t 1 04/21109 12:51 103-65-1
Styrene <0.86 uglL 1.0 0,86 1 04121109 12:51 100-42-5
1,1.1,2-Tetrechloroethane <0.92 uglL 1,0 0,92 1 04121/09 12:51 630-20-0
1 ,l,2,2-Tetrechioroethana <0,20 uglL 1.0 0,20 1 04121109 12:51 79-34-5
Tetrechlomethene 100 uglL 1.0 0.45 1 04121/09 12:51 127-18-4
Tetrehydrofumn <1.7 uglL 5,0 1.7 1 04/21/09 12:51 109-99-9
Toluene <0.87 uglL 1.0 0.67 1 04/21/09 12:51 t08-88-3
1,2,3-Trichlorobenzene <0.74 ug/L 1.0 0,74 1 04121109 12:51 87-61-6
1,2,4-Trichlombenzane <0.97 uglL 1.0 0.97 1 04/21109 12:51 120-82-1
1,1,1-Trichloreethane 38.0 uglL 1.0 0,g0 1 04/21/09 12:51 71..55-6
1,1,2-Trlchloroethane <0.42 uO/L 1,0 0,42 1 04/21109 12:51 79-00-5
Tdchloroathene 10.4 uglL 1.0 0,48 1 04121/09 12:51 79-01-6
TdchloreEuoromethane <0.70 uglL 1,0 0,79 1 04121/09 12:51 75-6g-4
1,2,3-Tdchloropmpane <0.99 uglL 1.0 0.99 1 04/21109 12:51 96-18-4
1,1,2-Tdchlemtdfluoroethene <1.$ ug/L 5,0 1.3 1 04/21/09 12:51 76-13-1
1,2,4-Tdmethylbenzene <0.07 uglL 1,0 0.97 1 04/21/09 12:51 95-63-6
1,3,5-Tdmethylbenzene <0.05 ug/L 1,0 0.83 1 04/21109 !2:51 108-67-6
Vinylchloride <0.t8 uglL 1,0 0.18 1 04/21/0912:51 75-01-4
m&p-Xytene <t.8 uglL 2,0 1.8 1 04/21100 12:51 1330.20-7
o-Xylene <0.83 uglL 1.0 0.83 1 04/21/08 12:51 95-47-6
4-Bromofluorobenzene(S) 84 % 70-130 1 04/21/0912:51 460-00-4
Dibromofluoromethane(S) 125 % 70-130 1 04/2110912:51 1868-63-7
Toluene-d8(S) 95 % 70-130 1 04/21/0912:51 2037-26-5
I I I I
Date: 04/23/2009 08;53 AM
REPORT OF LABORATORY ANALYSIS
Th]! report Ihall not be repmduc~l, except in full, without the wdtten consent of Pac~ Anelytical $tlvicel, Inc,.
Page 10 of 25
Pace Analytical Services, Inc.
1241 Bnllevue Stm~t - Suite 9 Green Bay. W~ 54302 (020)469-2436
ANALYTICAL RESULTS Project; East Slde P&T we 901
Pace Project No.: 4016184
Sample: RW07-38.1 Lab lD: 4018184004 Collected: O4/16/09 14:01 Received: 04/17/0908:30 Matdx:~Nater
I I I I I I I I I I I I I I I
Parsmeters Results Units PQL MDL DF prepared Analyzed CAS No. Qual
8260 MSV Anelyticel Method: EPA 8260
Acetone <12.6 ug/L 80.0 12.5 2,5
Allyl chlodde <8.0 ug/L 12.5 5.0 2.5
Benzene <1.0 uglL 2.5 1,0 2.5
Bromobenzene <2.0 uglL 2,5 2,0 2.5
Bromochloremethene <2,4 uglL 2,5 2.4 2,5
Bromodlchlommethane <1.4 ug/L 2.5 1.4 2,5
Bromoform <2.4 ug/L 2.5 2.4 2,5
Bromomethene <2.8 uglL 2,5 2,3 2.5
2-Butanone (MEK) <t0.8 ug/L 50.0 10,8 2,5
n-Butylbenzene <2.3 ug/L 2.5 2.3 2,5
sec-Butylbenzena <2.2 uglL 12,5 2,2 2.5
tert-Butylbenzene <2.4 ug/L 2.5 2.4 2.5
Carbon tetrachledde <1.2 ug/L 2,5 1,2 2.5
Chlorobenzene <1.0 uglL 2.5 1,0 2.5
Chloroethane <2.4 ug/L 2,5 2.4 2.5
Chloroform <8.2 ug/L 12,5 3.2 2.5
Chfommethane <0.60 ug/L 2,5 0,80 2,5
2-Chlorotoluene <2.1 ug/L 2.5 2,1 2,5
4-Chlorotoluene <1.6 ug/L 2,5 1.8 2,8
1.2-Dibromo-3~ch~ompmpane <4.2 ug/L 12.8 4.2 2.5
Dibromochlommethane <2.0 ug/L 2.5 2.0 2,5
1,2-Dibmmoethane (EDB) <t.4 ug/L 2.5 1,4 2.5
Dlbromomethane <1.6 ug/L 2.5 1,5 2,5
1,2-Dlchlorobenzene <2.1 ug/L 2,5 2,1 2,5
1,3-Dlchlorobenzene <2.2 ug/L 2,5 2,2 2,5
1,4-Dlchlombenzene <2.4 ug/L 2,5 2,4 2.5
DichlorodiSuorometha ne <2.6 uglL 2,5 2,5 2,5
1,l-Dlchloroethane 48.9 uglL 2,5 1,9 2,5
1,2-Dlchloroethane <0.80 uglL 2,5 0.90 2,5
1,1 -Dlchlorcethene 33.7 uglL 2,5 1,4 2,5
cis-l,2-Dfchloroethene 43.9 uglL 2,5 2,1 2,5
trane-1,2-DIchloroe~hene <2.2 ug/L 2.5 2,2 2,5
DIchlorofluoromethane <2,2 ug/L 2,5 2.2 2,5
1,2-DIchloropmpane <1.2 uglL 2.5 1.2 2.5
1,3-D[chloropropane <1,6 ug/L 2.5 1.8 2.5
2,2-DIchloropropane <1.8 ug/L 2.5 1,6 2.5
1,1-Dichloropropene <t.9 ug/L 2.5 1,6 2.5
cls-l,3-Dichloropropene <0.80 ug/L 2,5 0.50 2,5
tra ne-l,3-Dlchloropmpene <0,46 ug/L 2,5 0,48 2.5
Dlethyl ether (Ethyl ether) <2.4 uglL 2.5 2,4 2.5
Ethylbenzene <1.4 uglL 2,5 1,4 2,5
Hexechloro-l,3-butedlena <1.7 ug/L 12,5 1.7 2,5
Isopropylbenzene (Cumene) <1.8 ug/L 2,5 1,5 2,5
p-lsopropyltoluene <1.7 uglL 2.5 1,7 2.5
Methylene Chloride <1.1 uglL 2.5 1,1 2,5
4-Methyl-2-pentenone (MIBK) <8,0 uglL 12.5 3,0 2,5
Date: 04/23/2000 08:53 AM
REPORT OF LABORATORY ANALYSIS
This report ~hsil not be reproduced, except In full,
04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/08 18:24 04/21/08 18:24 04/21100 18:24 04/21/08 18:24 04/21/09 18:24 04121109 18:24 04121109 18:24 04121/08 18:24 04121109 18:24 04/21109 18:24 04121/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/08 18:24 04/21/09 18:24 04/21/09 18:24 04121109 18:24 04/21/09 18:24 04121/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21109 18:24 04/21/09 18:24 04/21/08 18:24 04/21/08 18:24 04/21/09 18:24 04/21/09 18:24 04/21109 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24 04/21/09 18:24
67-64-1 107-65-1 71-49-2
108-88-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104.51-8 98-65-6 56-23-5 108-90-7 75.00-3 67-65-3 74-87-3 95-49-8 100-43-4 98-12-8 124-48-1
105-93-4 74-95-3 95-59-1 541-73-1 106-46-7 75-71-8 75-34-3 107-08-2 75-38-4 156-59-2 155-60-5 75-434 78-87-5 142-28-0 594-20-7 563-58-6 10061-0!-5
10061-02-6 60-29-7 100-41-4 87-68-3 08-62-6 99-87-6 75-09-2
LI
Page 11 ef25
I I
I I I I I I I I I I
Pace Analytical Barvlcms, Inc.
1241 Baflevua Street - Suite 9 Gromn Bay, V~ 54302 {920)459-2438
ANALYTICAL RESULTS
Project: East Side P&T we 901 Pace Project No.: 4016184
8ample: RW07-38.1 Lab ID: 4016184004 Collected: 04116/09 14:01 received: 04/17/09 08:30 Matdx: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Quel
8280 MaV Analytical Method: EPA 8260
Methyl-te~-butylether <1.8 ug/L 2.5 1.5 2.5 04/21/0918:24 1634-04-4
Naphthalene <2.2 uglL 12.5 2.2 2.5 04/21/09 18:24 91-20-3
n-Pmpy~benzene <2.0 ug/L 2.5 2.0 ¯ 2~5 04/21/09 18:24 103-85-1
Styrene <2.2 uglL 2.5 2.2 2.5 04/21/09 18:24 100-42-5
1,1,1,2-Tetrachloroethene <2.2 ug/L 2.5 2.3 2.5 04/21/09 18:24 630-20-6
l,l,2,2-Tetrachloroethane <0.60 uglL 2.6 0.50 2.5 04121109 18:24 79-34-5
Tetrachloroethene 802 uglL 2.5 1.1 2.5 04/21109 18:24 127-18-4
Tetrahydrofuren <4.2 ug/L 12,5 4.2 2.5 04121109 18:24 109-99-9
Toluene <1.7 uglL 2.5 1.7 2.5 04/21109 18:24 108-88-3
1,2,3-Trlchiorobenzene <1.8 uglL 2,5 1.8 2,5 04/21109 18:24 87-61-6
1,1,l-Tdchloroethane 184 ug/L 2.5 2.2 2.5 04121/09 18:24 71-55-6
1,1,2-Tdchloroethene <1.0 ug/L 2.5 1,0 2.5 04/21/09 18;24 79-00-5
Tdchlomelhene 28.0 ug/L 2.5 1.2 2.5 04/21/08 18:24 79-01-6
Tdchlomfluoromethane <2.0 ug/L 2.5 2.0 2.5 04/21/09 18:24 75-09-4
1,2,3-Tdchloropropane <2.1~ ug/L 2.5 2.5 2.5 04/21/09 18:24 99-18.-4
1,1,2-Tdchlorotdfluomethane <8.2 uglL 12.5 3.2 2.5 04/21/09 18:24 78-13-1
1.2,4-Tdmethylbenzene <2.4 uglL 2.5 2.4 2.5 04/21/09 18:24 95-63-6
1,3.5-Tdmethylbenzene <2.1 uglL 2.5 2.1 2.5 04/21/09 18:24 108-67-8
m&p-Xylene <4.8 uglL 5.0 4.5 2,5 04/21/09 18:24 1330-20-7
o-Xylene <2,1 uglL 2.5 2.1 2.5 04121109 18:24 95-47-6
4-Bromofluorobenzene (S) 88 % 70-130 2.5 04121/00 18:24 460-00-4
Oibromofluoromethane (S) 111% 70-130 2.5 04121100 18:24 1868-53-7
Toluene-de(S) 98 % 70-130 2.5 04/21/09 18:24 2037-28-5
I I I
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This raped shall not be reproduced, except in full, without the written c~nsent of Pace Analy~ca~ Sen/ices, Inc..
Page 12 of 25
I I I I I I I I I I I I I I I I I I I
e2eAnalyticaI.
ANALYTICAL RESULTS
Project: East Side P&T W~ 901 Pace Project No.: 4016184
Sample: RW06-27-BR Lab lD: 4018184005 Collected: 04/16/09 14:05 Received: 0411710908:30 Matdx: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No, Qua1
8280 MSV AnelyScel Method: EPA 8260
Acetone <t0 ug/L 40.0 10 2 04/21/09 18:48 67-64-1
Allyl chlodda <4.0 uglL 10.0 4.0 2 04/21/09 18:48 107-05-1
8~nzene <0,82 ugiL 2,0 0,82 2 ~4/21/09 18:48 71-43-2
Bromobenzene <1.~ ug/L 2.0 1.6 2 04/21/09 18:48 108-86-1
Bromochloromethane <1.6 ugiL 2.0 1.8 2 04/21/09 18:48 74°97-5
Bromodlchloromethane <1.1 ug/L 2.0 1.1 2 04/21/09 18:48 75-27-4
Bmmoform <t.$ ug/L 2.0 1,9 2 04/2110918:48 75.25-2
Bromomethane <1,~ ug/L 2.0 1,8 2 04/21109 18:48 74-83-9
2-Butanone(MEK) <8.6 ug/L 40,0 8.6 2 04/21/0918:48 76-93-3
n-Butylbenzene <1.9 ug/L 2,0 1.9 2 04/21/09 18:48 104.51-8
sec-Butylbenzene <1.8 ug/L 10.0 1.8 2 04/21/09 18:48 135-96-8
tert-Butylbonzene <1.8 ug~ 2,0 1.9 2 04/21/09 18:48 95-05-5
Carbon tet~achlorlde <0,96 uglL 2,0 0.98 2 04/21/09 18:48 56-23-5 LI
Chlorebonzene <0.52 uglL 2,0 0.82 2 04/21109 18:48 108-90-7
Chloroothane <1.6 uglL 2,0 1,0 2 04/21/09 18:48 75-00-3
Chloroform <2.6 uglL 10.0 2,6 2 04/21/09 18:48 67-66-3
Chlommethane <0.46 ug/L 2,0 0,48 2 04/21109 18:48 74-87-3
2-Chlorotoluene <1.7 ug/L 2,0 1.7 2 04/21/09 18:48 95-49-6
4-Chlorotoluene <t,8 ug/L 2.0 1.5 2 04/21/09 18:48 108-43-4
1,2-DIbromo-3-ch/oropropane <3.4 ~ 10.0 3.4 2 04/21/09 18:48 98-12-8
Dibromochloromethane <1.8 ug/L 2,0 ¯ 1,5 2 04/21/09 18:48 124-48-1
1,2-DIbromoothono (EDB) <1.1 ug/L 2,0 1,1 2 04/2!/09 18:48 100-83-4
Dibromomothane <1.2 uglL 2.0 1,2 2 04/21/09 18:48 74-65-3
1,2-Dichlorobenzene <1.7 ug/L 2.0 1.7 2 04/21/09 18:48 95-50-1
1,3*Dichlorobenzene <1.7 ug/L 2.0 1.7 2 04121/09 18:48 541-73-1
1,4-Dlchlorobenzene <1.9 uglL 2.0 1.9 2 04/21/09 18:48 106-46-7
Dlchlorodifluoromethane <2,0 ug/L 2,0 2,0 2 04/21/09 18:48 75-71-8
1,1-Dlchloroothone 42,2 ug/L 2.0 1.5 2 04/21/09 18:48 75-34-3
1,2-Dfchloroethene <0.72 uglL 2,0 0.72 2 04/21/09 18:48 107-06-2
1,1-Dlchloroethene 34.8 uglL 2.0 1.1 2 04/21/09 18:48 75-35-4
cls-l,2-DIchloroethene 28.7 ug/L 2,0 1.7 2 04/21/09 18:48 150-59-2
trans-l,2-Dichlomethene <1.8 ug/L 2,0 1,8 2 04/21/09 18:48 156-80-5
DlchJorofluoromethano <1.8 ug/L 2,0 1.8 2 04/21/09 18:48 75-43-4
1,2-Dichloropropene <0.98 ug/L 2.0 0.98 2 04/21109 18:48 78-87-5
1,3-Dichloropropane <1.2 uoiL 2.0 1,2 2 04/21109 18:48 142-28-9
2,2-D]chloropropano <t.2 uglL 2,0 1.2 2 O4/21109 18:48 594-20-7
1,1-D]chloropropene <1.8 uglL 2,0 1.5 2 04/21109 18:48 563-58-6
cls-l,3-Dichioropropene <0.40 uglL 2,0 0.40 2 04/21/09 18:48 10061-01-5
trans-l,3-Dichloropropene <0.68 ug/L 2.0 0.38 2 04/21/09 18:48 10061-02-6
Dlothyl elhor (Elhy~ ether) <2.0 uglL 2.0 2.0 2 04/21/09 18:48 66-29-7
Ethylbenzene <1.1 ug/L 2,0 1.1 2 O4/21/08 18:48 100-41-4
Hexachloro-l,3-butediene <1.0 uglL 10,0 1,3 2 04/21/09 18:48 87-68-3
IsopmwIbenzene(Cumene) <1.2 ug/L 2,0 1,2 2 04/2!10918:48 96-82-8
p-lsopropyltoluene <1.$ uglL 2.0 1,3 2 04/21/09 18;48 99-87=8
Methylene Chloride <0.86 ug/L 2.0 0,86 2 04/21/09 18:48 75-09-2
4-Methylo2-pentanone (MISK) <2.4 ug/L 10,0 2,4 2 04/21/09 18:48 108-16-1
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This tepee ahell not be rep~oduc~d, except in full, without the written consent of Pace Analytical Services, Inc..
Page 13 of 25
I I
I I I I I I I I I I
Green Bey, wi 54302 (920)469-2438
ANALYTICAL RESULTS
Project: East Side P&T we 901 Pace Project NO.: 4016184
Sample: RW08.27-BR LeblD: 4016184008 Collected: 04/18/0914:05 Received: 04/17/0908:30 Matrix:Water
Parameters Result~ Units PQL MDL DF Prepared Analyzed CAS No, Qua1
8260 MSV Analytical Method: EPA 8260
Methyl-tert-butylether <t.2 uglL 2.0 1.2 2 04/21/0918:48 1834-04-4
Naphthalene <1.8 uglL 10.0 1.8 2 04/21/09 18:48 91-20-3
n-Propylbenzene <1.8 uglL 2,0 1.8 2 04/21/09 18:48 103-65-1
Styrene <1.7 ug/L 2,0 1.7 2 04/21/09 18:48 100-42-5
1,1,1,2-Totrachloroethene <1.8 ug/L 2.0 1,8 2 04/21109 18:48 630-20-6
1,1,2,2-Tetrachloroethene <0A0 ug/L 2.0 0,40 2 04/21/09 18:48 78-34-5
Tetrachloroethene 267 ug/L 2.0 0.60 2 04/21/09 18:48 127-18-4
"~trahydrofuran <3A ug/L 10.0 3.4 2 04/21/09 18:48 109-99-9
Toluene <1.3 uglL 2.0 1.3 2 04/21/09 18:48 108-88-3
1,2,3-Trichlorobenzene <1.6 ug/L 2,0 1.5 2 04/21/09 18:48 87-61-6
1,2,4-Tdchlorobencene <1.8 ug/L 2.0 1.9 2 04/21/09 18:48 120-82-1
1,1,1-Trichloroethane 114 ug/L 2.0 1.8 2 04/21/08 18:48 71-85-6
1,1,2-Tdchloroethene <0,84 ug/L 2.0 0,84 2 04/21/09 18:48 79-00-5
Trlchloroethene 18.8 uglL 2.0 0.98 2 04/21/09 18:48 79-01-6
Trichloroftuoromethane <1.8 ug/L 2.0 1.8 2 04/21/09 18:48 75-89-4
1,2,3-Trlchlompmpane <2,0 uglL 2,0 2.0 2 04/21/09 18:48 96-18-4
1,1,2-Trlchlomtdt~uomethano <2.8 uglL 10.0 2.6 2 04/21/09 18:48 76-13-1
1,2,4-Tdmethylbenzene <1.8 uglL 2.0 1.9 2 04/21/09 18:48 95-63-6
1,3,5-Trimathylbenzene <1.7 uglL 2,0 1,7 2 04/21/09 18:48 108-67-8
~nyl ch~odde <8.38 ug/L 2.0 0.38 2 04/21/09 18:48 75-61-4
m&p-Xylene <8.8 ug/L 4.0 3.6 2 04/21/09 18:48 1330-20-7
o-Xylene <1,7 ugJL 2.0 1.7 2 04/21/09 18:48 65-47-6
4-Bromofluorobenzene (S) 83 % 70-130 2 04/21/0918:48 480-00-4
Dibromofluoromethane (S) 118 % 70-130 2 04/21/09 18:48 1868-53-7
Toluene-d8 (S) 88 % 70-130 2 04/21/09 18:48 2037-26-5
I I I
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
Thil report shall not b~ reproduced, except in full without the w~t~en consent of Pace An=dytlcal
Page 14 of 25
.. ace Analytical "
Pace AnalytlcalServlces, lnc, 1241 Bellevue Street-Suite 8GreenBay, WI54302 (920)469-2436
I I I i I I I I I I I I I I I I I
ANALYTICAL RESULTS
Project: t=ast Side P&T we 901 Pace Project No.: 4016184
Sample: St= P&T BETWEEN Lab ID: 4016184008 Collected: 04/16/09 14:09 Received: 04/17/09 08:30 Matdx: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No, Qual
8280 MSV Analytical Method: EPA 8260
Acetone <8.0 ug/L 20,0 5.0
Allyl chlodde <2.0 ugiL 5.0 2.0
Benzene <0,41 ug/1. 1.0 0,41
Bromobenzene <0.82 ug/L 1.0 0.82
Bromochloromethane <0,07 ug/L 1.0 0,97
Bromodichloromethane <0.88 uglL 1.0 0.58
Bromoform <0.84 ug/L 1.0 0.~4
Bremom~.thene <0.91 uglL 1.0 0,91
2-Butanone (MEK) <4.8 ug/L 20.0 4.3
n-Butylbenzena <0.88 uglL 1.0 0.93
sec-Butylbenzene <0.89 uglL 5.0 0.89
tert-Butylbenzene <0.97 ug/L 1.0 0.97
Carbon tetmchlodde <0.49 ug/L 1.0 0.49
Chlombenzena. <0.41 ug/1. 1,0 0,41
Chlomethane <0.87 ug/L 1,0 0,97
Chloroform <1.8 ug/L 5,0 1.3
Chloromethane <0.24 ug/L 1.0 0,24
2-Chlomtoluene <0,88 ug/L 1,0 0,85
4-Chlorotoluene <0.74 ug/L 1,0 0,74
1,2-Dibromo-3-chlompmpane <1.7 U~[L 5.0 1.7
DIbmmochlommethane <0.81 ug/L 1.0 0,81
1,2-Dibromoethane (EDB) <0.~ ug/L 1,0 0.56
DIbromomethane <0.80 ug/L 1.0 0.60
1,2-Dichlorobenzene <0,88 ug/L 1,0 0,83
1,3-Dichlorobanzene <0.8? ug/L 1,0 0.87
1,4-Dlchlorobanzene <0.88 ug/L 1,0 0,95
Dlchlomdifluoromatha ne <0.99 ug/~ 1.0 0.99
1.1-Dlchloroethana 68.8 ug/L 1.0 0.75
1,2~Dlchloroethane 0.44J ug/L 1.0 0.36
1.1-Dlchloroethane 20.4 uglL 1.0 0,57
cls-l.2-Dic~lomethane 14.2 ug/L 1.0 0.83
irons- 1.2-Dlchloroat hens <0.88 ug/L 1.0 0.89
Dichlorofluoromethane <0.88 ug/L 1.0 0.88
1,2.Dich~oroptopane <0.49 uglL 1.0 0.49
1,3-Dichloropropane <0.61 ug/L 1.0 0,61
2,2-Dichleropropane <0.82 ug/L 1.0 0.62
1,1-Dichloropmpene <0.78 uglL 1.0 0.75
cia-l.3-Dlchloropropene <0.20 ug/L 1.0 0.20
tra ns-l.3-Dlchloropmpena <0.t8 uglL 1.0 0.19
Diethyl ether (Ethyl ether) <0.98 uglL 1,0 0.98
Ethylbenzene <0.64 ug/L 1.0 0.54
Hexachlom-1,3-butadiene <0.87 ug/L 5.0 0.67
Isopmpylbenzane (Cumane) <0.88 ug/L 1,0 0.59
p-lsopmpyltoluene <0.87 ug/L 1.0 0.67
Methylene Chlodda <0.4~ uglL 1.0 0.43
4-Methyl-2-pentanone (MIBK) <1.2 ug/L 5,0 1.2
04/2110913:15 67.64-1 04/21/09 13:15 107-05-1 04121109 13:15 71-43-2 04/21/09 13:15 108-86-1 04/21/09 13:15 74-97-5 04121109 13:15 75-27-4 04/21/09 13:15 75-25-2 04/21/09 13:15 74-83-9 04/21/09 13:15 78-93-3 04121109 !3:15 104-51.6 04/21/0913:15 135-95-8 04/21/0913:15 98-08-6 04/21/0913:15 56-23-5 04/21/09 13:15 108-90-7 04/21/09 13:15 75-00-3 04/21/0913;15 67-66-3 04/21108 13:15 74-87-3 04121109 13:15 95-49-8 04121/09 13:15 106-43-4 04/21/09 13:15 98-12-B 04121109 13:15 124-45-1 04/21/0913:18 106-93-4 04/21/09 13:15 74-95-3 04/21/09 13:15 95-50-1 04/21/09 13:15 541-73-1 04/21/09 13:15 106-45-7 04121109 13:15 75-71-8 04/21106 13:15 75-34-3 04/21109 13:15 107-08-2 04121/09 13:15 75-35-4 04121/0013:15 156.69-2 04/21/0913:15 156-60.5 04/21/0913:15 75-43-4 04/21/09 13:15 78.67-5 04/21/0913:15 142o25-9 04121109 13:15 563.68-6 04121109 13:15 10061-01-5 04/21/09 13:15 10061÷02-6 04/21/09 13:15 60o2~-7 04/21/09 13:15 100-41-4 04/21/09 13:15 87-68-3 04121108 13:15 95-82-8 04121109 13:15 99-87-6 04121109 13:15 75-09-2
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
Page 15 of 25ceAnalytical"
(920)489-2436
ANALYTICAL RESULTS Project: Eaet Side P&T we 801
Pace Project NO,: 4016184
Semple; 8E P&T BETINEEN Lab ID: 4016184006 Collected: 04118/09 14:09 Received: 04117/09 08:30 Matdx: VVater
I I I I I I I I
Parameters Results Units PQL MDL OF Prepared Analyzed CAS No. Qual
8280 MSV Analytlca~ Method: EPA 8200
Methyl-tertobutyl ether <0.81 uglL 1.0 0.61 1 04121/09 13:15 1634-04-4
Naphthalene <0.80 ug/L 5.0 0.89 1 ~4/21/09 13:15 91-20-3
n-Propylbenzene <0.81 uglL 1.0 0.81 1 04121/09 13:15 103.65-1
Styrene <0.00 ug/L 1.0 0,86 1 04/21/09 13:15 100-42-5
1,1,1,2-Tetrachloroothano <0,92 uo/L 1.0 0.92 1 04/21/09 13:15 030-20-6
1,1,2,2-Tetrachloroethane <0.20 ug/L 1.0 0.20 1 04/21109 13:15 79-34-5
Tetrachloroethene 1.1 ug/L 1.0 0.45 1 04/21/09 13:15 127-18-4
Tetrohydrofuran <1.7 uglL 5.0 1.7 1 04/21/09 13:15 100-99-g
Toluene <0.87 uglL 1.0 0.87 1 04/21/09 13:15 105-88-3
1,2,3-Tr~chlorobenzene <0.74 ug/L 1.0 0.74 I 04121/09 13:~5 87-61-6
1,2,4-Trlchlorobonzene <0.07 ug/L 1.0 0,87 1 04/21/00 13:15 120-82-1
1,1,1-Tdchloroethene 108 ug/L 1,0 0.fl0 1 04/21109 13:15 71-55-6
1,1,2-Trichlo¢oethsne <0.42 uglL 1.0 0.42 1 04/21/09 13:15 79-00-5
Trlchloroethene <0.48 ug/L 1.0 0.48 1 04/21/09 13;16 79-01.6
Tdchlorofluoromethane <039 ug/L 1.0 0.79 1 04121/09 13:15 75-69-4
1,2,3-Trichloropropene <0.99 uglL 1.0 0.99 1 04/21/00 13:15 98-18-4
1,1,2-Trichlorotdfluoroethone <t.3 uglL 5.0 1.3 1 04/21/09 13:15 75-13-1
1,2,4-Trimothylbenzene <0.97 uglL 1.0 0.97 1 04/21/09 13:15 95-63-6
1,3,5*Tdmethylbenzene <0.83 uglL 1.0 0.83 1 04/21/09 13:15 108-67.6
Vinyl chtorlde <0.10 ug~L 1.9 0.18 1 0M21/09 13:15 75-01-4
m&p-Xylene <1.0 ug/L 2.0 1.8 1 04121/09 13:15 1330-20-7
o*Xylene <0.83 ug/L 1.0 0.83 1 04121/09 13:15 95-47-6
4-Bromofluombonzene (S) 80 % 70-130 1 04121/09 13;15 460-00-4
Dlbromolluoromethane (S) 121% 70-130 1 04/21/09 13:15 1868-63-7
Toluene-d8 (S) 85 % 70-130 1 04/21/09 13:15 2037-26-5
I I I
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This report shalJ not be reproduced, except In full.
Page 16 of 25
Analytical"
ANALYTICAL RESULTS Project: East Side P&T we 901
Pace Project No.: 4016184
Sample: BE P&T EFFLUENT Lab I0: 401018400"/’ Collected: 04116106 14:16 Received: 04117/09 08:30 Metflx: Water
I I I I I
I I I I I I I I I I
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Analytlca~ Method: EPA 8260
Acetone <8.0 ug/L 20.0 5.0 1
Allyl chlodde <2.0 ug/L 5.0 2.0 1
Benzene <0.41 ug/L 1,0 0.41 1
Eromobenzene <0,62 ug/L 1.0 0.82 1
Bromoc, hloromsthane <0.97 uglL 1,0 0.97 1
Bromodlchloromethane <0,86 uglL 1.0 0.58 1
Bromoform <0.94 uglL 1.0 0.94 1
Bromomethane <0.81 ug/L 1,0 0.91
2-Butsnone (MEK) <4,3 ug/L 20,0 4.3 1
n-Butylbenzeno <0.63 ug/L 1,0 0.03 1
aoc-Butylbenzene <0.86 uglL 5,0 0.89 1
tert-Eutylbonzene <0.67 uglL 1.0 0.97 1
Carbon tetrachlorlde <0.49 uglL 1,0 0.40 1
Chlerobenzene <0.41 ug/L 1.0 0.41 1
Chloreethane <0.07 ug/L 1,0 0.97 1
Chloroform <1,3 ug/L 5,0 1,3 1
Chlorornethane <0.24 ug/L 1.0 0,24 1
2-Chlorotoluece <0.86 uglL 1.0 0.85 1
4-Chlorotoluene <0,74 uglL 1.0 0.74 1
1,2.DIbromo-3-chJompmpene <1.7 ugJL 5.0 1.7 1
Dibromochlommethane <0.81 ug/L 1,0 0.81 1
1,2-Dibromoethane (EDB) <0.66 ug/L 1,0 0,56 1
Dibromomethans <0.60 uglL 1.0 0,60 1
1,2-Dichlorebsnzene <0.83 uglL 1,0 0,83 1
1,3-Dlchlorobenzene <0.87 uglL 1,0 0.87 1
1,4.Dtchtombenzene <0.86 ug/L 1.0 0.05 f
Dichlorodifluoromethane <0.90 ug/L 1.0 0.99 1
1,1-Dichloroethane 10.2 ug/L 1,0 0.75 1
1,2-Dich~oroathsne <0.36 ug/L 1,0 0,38 1
1,1-Dlchlometheno 1.0 uglL 1.0 0.57 1
cls-l,2-Dichlomothene <0.83 uglL 1.0 0.83 1
trano-1,2-Dichloroethene <0.86 uglL 1.0 0.89 1
Dichlorofluoromethane <0.88 uglL 1.0 0.88 1
1,2-Olchloroprepene <0.40 ug/L 1,0 0,49
1,3-Dlchloroprepene <0.81 ug/L 1.0 0.61 1
2,2.Dichloropropone <0,62 ug/L 1.0 0.62 1
1,1-Dichloropropeno <0.70 uglL 1,0 0,75 1
cio-l,3-Dichloropropene <0.20 ug/L 1,0 0.20
trana-l,3-Dichloropropene <0.16 uglL 1.0 0.19 1
Dlethyl ether (Ethyl ether) <0.68 uglL 1,0 0.98 1
Ethytbenzone <0.64 uglL 1.0 0.54 1
Hsxachloro-1,3-butsdlene <0.67 ug/L 5.0 0,67 1
laopmpylbenzene (Cumene) <0.69 ug/L 1.0 0.59 1
p-lsopropyltoluene <0.0T ug/L 1,0 0,67 1
Methylene Chlodde <0.43 uglL 1.0 0.43 1
4-Methyl-2-pentsnone (MIBK) <1.2 ug/L 5,0 1,2 1
Date: 04123/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
Thll report she, not be repmdu~d, e~c~pt in full, without the written consent of P~ Analytical Ser~c~=, In~.
04i21/09 16:49 04/21/09 16:49 04/21/09 18:48 04/21/09 18:49 04121/09 16:49 04/21109 16:49 04/21/09 16:49 04/21109 16:49 04/21109 16:49 04121109 16:49 04/21/09 16:49 04/21/09 16:49 04/21109 18:49 04/21109 18:49 04121109 16:49 04/21/09 16:49 04/21/09 16:49 04/21/09 18:49 04/21/09 18:49 04/21109 16:49 04121/09 16:49 04/21/09 16;49 04/21/09 16:49 04/21109 18:49 (}4/21/09 18:49 04/21/09 16:49 04/21109 16:49 04/21/09 16:49 04/21/09 16:49 04/21/09 16:49 04/21109 16:49 04/21109 18:49 04121/09 16:49 04/21/09 16:49 04/21109 16:49 04/21/09 18:49 04/21/09 18:49 04/21/09 16:49 04/21/09 16:49 04/21/09 16:49 04/21/09 16:49 04/21/09 16:49 04/21/09 18:49 04/21100 18:49 04/21109 16:49 04/21100 16:49
67-64-1 107-05-1 71.43-2 108-86-1 74-97-6 75-27-4 75-25-2 74-83-9 78-93-3 104-5%8 135-95-8 98-05-6 56-23-5
!00-90-7 75-00-3 67-65-3 74-87-3 95-49-8 106-43-4 96-12-8 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 75-71-8 75-34-3 107-00-2 75-35-4 156-60-2 156-60-5 75-43-4 78-67-5 594-20-7 563-58-6 10061-01-5 10061-62-6 60-20-7 100.41-4 87-65-3 98-82-8 99-87-6 75-09-2
Page 17 of 25
aceAnalytical °
(020)409.2438
I I I I I I I I I I
ANALYTICAL RESULTS
Prolect: East Side P&T WO 601 Pace Project No.: 4016184
8ample: EE P&T EFFLUENT Lab tD: 4016184007 Collected: 04/16/06 14:16 Received: 04/17/09 08:30 Matdx: W~ter
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Analytical Method: EPA 8260
Methyl.ted-butylether <0.61 uglL 1.0 0.61 1 04/21/09 16:49 1634-04~4
Naphthalene <0.88 uglL 5,0 0,88 1 04/21109 16:49 91-20-3
noPropylbenzane <0.81 uglL 1.0 0.81 1 04/21/08 16:40 103-65-1
Styrene <0.86 uglL 1.0 0.86 1 04/21109 16:49 100-42-5
1,1,1,2-TetracMoroethane <0.92 ug/L 1.0 0.92 1 04/21/09 16:49 630-20-6
1,1,2,2-Tetrachlorcethene <0.20 uo/L 1.0 0.20 1 04/21/09 16:40 70-34-5
Tatrachloroethene ’1.~1 ug/L 1.0 0.45 1 04/21/08 18:49 127-18-4
Tetrahydrofuran <1.7 ug/L 5,0 1,7 1 04/21/09 16:49 109-09-9
Toluene <0.67 uglL 1.0 0.67 1 04/21/08 16:49 108-88-3
1,2,3-Trich]orobenzene <0.74 uglL 1,0 0.74 1 04/21/00 16:49 87-61o6
1,2,4-Trlchlorobenzene <0.67 ug/L 1.0 0.97 1 04/21/09 16:49 120-82-1
l,l,l-Trichlorcethane 28.8 ug/L 1.0 0.90 1 04/21/00 16:49 71-55-8
l,l,2-Trichloroathane <0.42 uglL 1.0 0.42 1 04121/08 16:49 79-00-5
Trlchloroethene <0,46 uglL 1.0 0.48 1 04/21109 16:49 70-01-6
Tdchlorofluoromethane <0.79 uo/L 1.0 0.70 1 04/21109 16:49 75-69-4
1,2,3-Trlchloropropane <0.68 ug/L 1.0 0.99 ! 04121/09 !6:49 08-18-4
l,l,2-Trlchlorotdfluomethane <1.3 uglL 5.0 1.3 1 04/21/09 18:49 76-13-1
1,2,4-Tdmathylbenzane <0.67 ug/L 1.0 0,97 1 04121/09 18:49 05-63-6
1,3,5-Trimethylbenzene <0.83 ug/L 1.0 0,83 1 04/21/09 16:40 108-67-8
VJnyJ chloride <0.1B ug/L 1,0 0.18 1 04/21/09 18:40 75-01-4
m&p-Xylene <1.8 ug/L 2.0 1.8 1 04/21/09 16:49 1330-20-7
o-Xylene <0.83 uglL 1.0 0.83 1 04/21/09 16:49 95-47-6
4-Bromofluorobenzena (S) 85 % 70-130 1 04/21109 16;49 460-00-4
DIbromo/]uoromethane (S) 116 % 70-130 1 04121109 18:49 1868-60-7
Toluene-el8 (S) 98 % 70-130 1 04121/09 16:49 2037-26-5
I I I
Date: 04/23/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
Thi| report 8ha~l not be reproduced, except in full,
Page 18 of 25
Analytical"
I I I I I I I I I I I I I I I
ANALYTICAL RESULTS Project: East Side P&T we 801
Pace Project No,: 4016184
Sample: TRIP BLANK Lab ID: 4018184008 Collected: 04116/09 00:00 Received: 04/17/09 08:30 Matdx: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No, Qual
8260 MSV Anely~cal Method: EPA 8260
Acetone 8.8J ugit. 20,0 5.0 1 04/21/09 12:03 87-84-1
Aliylchlodde <2.0 uglL 5,0 2.0 1 04/21/0912:03 107-05-1
Benzene <0.41 uglL 1,0 0.41 1 04/21/09 12:03 71-43-2
Bromobenzene <0.82 uglL t,0 0,82 1 04/21/09 12:03 108-86-1
Bromochloromethane <0.87 uglL 1,0 0,97 1 04/21109 t2:03 74-97-5
Bmmodichloromethane <0.68 uglL 1.0 0,56 1 04/21109 12:03 75-27-4
Bromoform <0.94 uglL 1,0 0,94 1 04/21109 12:03 75-25-2
Bromomethane <0.01 uglL 1.0 0.91 1 04/21/09 12:03 74-83-9
2-Butanone(MEK) <4.8 ug/L 20,0 4,3 1 04/21/0912:03 78-93-3
n-Butylbenzane <0.82 uolL 1.0 0.93 1 04/21/09 12:03 104-51-8
sac-Butylbenzene <0.89 uglL 5,0 0.89 1 04/21109 12:03 135-98-8
terl-Butylbenzena <0.07 uglL 1,0 0.97 1 04/21106 12:03 98-09-6
Carbon tetrachlodde <0,49 uglL 1,0 0,49 1 04/21109 12:03 56-23-5 L1
Chlo~obenzene <0.41 uglL 1,0 0.41 1 04/21109 12:03 109-99-7
Chloroethene <0.87 uglL 1,0 0.97 1 04121109 12:03 75-00-3
Chloroform <1.3 uglL 5,0 1,3 1 04/21/09 12:03 87-65-3
Chloromethane <0.24 uglL 1.0 0,24 1 04/21/09 12:03 74-87-3
2-Chlorotoluane <0.88 uglL 1.0 0.85 1 04/21/09 12:03 95-40-8
4-Chlorotoluene <0.74 ug/L 1,0 0,74 1 04/21/09 12:03 106-43-4
DJbmmochloromathana <0.81 ug/L 1,0 0.81 1 04/21109 12:03 124-48-1
1,2-DIbromoethene(EDB) <0.86 uglL 1,0 0,56 1 04121/0912:03 106-93-4
Dibromomethane <0,60 ug/L 1,0 0,60 1 04/21/09 12:03 74-95-3
1,2-DIchlombenzene <0.83 uglL 1,0 0.83 1 04/21/09 12:03 95-50-1
1,3-Dichlorobenzene <0.87 ugiL 1.0 0,87 1 04/21/00 12:03 541-73.1
1,4-Dichlombenzene <0.08 uglL 1.0 0.95 1 C~/21/09 12:03 106-48-7
Dlchlomdlfluoromethene <0.88 uglL 1,0 0,99 1 04/21109 12:03 75-71-8
l,l-Dlchloroathane <0.78 ug/L 1,0 0.75 1 04/21109 12:03 75-34-3
1,2-Dlchloroethene <0,88 UgrL 1.0 0,36 1 04121109 12:03 107-06-2
1,1-Dichloroethene <0.87 uglL 1,0 0,57 1 04/21/09 12:03 75-35-4
cis+l,2-Dichloroethene <0.83 uglL 1,0 0.83 1 04/21/09 12:03 158-59-2
trans-l,2-Dichloroethene <0,88 uglL 1,0 0,89 1 04/21/09 12:03 156-60-5
Dichlorofluoromethane <0.88 uglL 1~0 0,88 1 04/21100 12:03 75-43-4
1,2-DIchloropropane <0.48 ug// 1,0 0.49 1 O4/21109 12:03 78-87-5
1,3-Dichloropmpane <0.81 ug/L 1,0 0,81 1 04/21109 12:03 142-28-9
2,2.Dichlorop¢opane <0,82 ug/L 1,0 0,62 1 04121109 12:03 594-20-7
l,l-DIchloropi’opene <0,76 uglL 1,0 0,75 1 04/21/09 12:03 563-58-6
cia-l,3-Dichlomprapene <0,20 uglL 1,0 0,20 1 04/21/09 12:03 10061-01-5
trane-l,3-Dichloropropene <0,19 ugJL 1.0 0.19 1 (}4/21/09 12:03 10061-02-6
DiethyL ether (Ethyl ether) <0.98 ug/L 1.0 0,98 1 04/21/0912:03 00-29-7
Ethylbenzene <0.84 UgrL 1,0 0,54 1 04/21109 12:03 100-41-4
Hexachlom-1,3-butadiene <0.87 ug/L 5,0 0.87 1 04121109 12:03 87-69-3
Isopmpylbenzena(Cumene) <0,68 ug/L 1,0 0.59 1 04/21/0912:03 98-82-8
p.lsopropyltoluene <0.87 uglL 1,0 0.87 1 04121/09 12:03 98-67-6
MethyleneChfodde <0,4~ uglL 1,0 0,43 1 04/21/0912:03 75-09-2
4-Methyl-2-pontsnone (MIBK) <1.2 uglL 5.0 1.2 1 04/21/00 12:03 108-19-1
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full, without the written conleot of Pace Analytical Services, Inc,,
Date: 04123/2009 08:53 AM Page 19 of 25
aceAnalyticalO
I I I I I I I I
ANALYTICAL RESULTS Project: East Side P&T WO 901
Pace Project No.: 4016184
Sample: TRIP BLANK Lab ID: 4010184008 Collected: 04/16108 00:00 Received: 04117/09 08:30 Matdx: ~Nater
Parameters Reaulta Units PQL MDL DF Prepared Analyzed CAS NO. Qual
8280 MgV Analytical Method: EPA 8260
Methyl-ted-butylether <0.61 ug/L 1.0 0.61 1 04121/09 12:03 1634-04-4
Naphthalene <0.88 uglL 5,0 0,89 1 04121109 12:03 91-20-3
n-Propylbenzene <0.81 uolL 1.0 0.81 1 04/21/09 12:03 103-65-1
Styrene <0.00 uglL 1.0 0.86 1 04/21/09 12:03 100-42-5
l,l,l,2-Tetrachloroethana <0,82 uglL 1.0 0.92 1 04/21/09 12:03 830-20-6
1,1,2,2-Tetrschloroathana <0.20 uglL 1.0 0.20 1 04/21108 12:03 79-.34-5
Tetrschloroethene <0.48 ug/L 1.0 0.45 1 04/21/09 12:03 127-18-4
Tetrahydrofu~an <1.7 uglL 5.0 1.7 1 04/21/00 12:03 109-89-9
Toluene <0.87 uglL 1,0 0.67 1 04/21/09 12:03 108-88-3
1,2,3-Tdchlorobenzena <0.74 ug/L 1,0 0.74 1 04/21/08 12:Q3 87-81-8
1,2,4-Tdchlorobenzene <0.07 ug/L 1.0 0,97 1 04/21/09 12:03 120-82-1
1,1,1-Tdchlomethane <0.80 ug/L 1.0 0.00 1 04/21/09 12:03 71-55-6
1,1,2-Trlchloroethane <0.42 ug/L 1.0 0.42 ! 04/21108 12:03 79-00-5
Trlchloroathane <0.48 ug/L 1.0 0.48 1 94/21/00 12:03 79-01-6
Trichlorofluoromethane <0.70 ug/L 1.0 0.79 1 04/21/09 12:03 75-69-4
1,2,3-Trlchlompropane <0,08 ug/L 1,0 0.99 1 04/21109 12:03 96-18-4
1,1,2-Trlchlomtdfluomethane <1.3 ug/L 5.0 1.3 1 04121109 12:03 76-13-1
1,2,4-Trimethylbenzene <0.97 ug/L 1.0 0.07 1 04121109 12:03 85-63-8
1,3,5-Tdmethylbenzene <0.83 uglL 1.0 0.83 1 04/21/09 12:03 108-67-8
V~nylchlodde <0.18 uglL 1.0 0.18 1 04/21/09 12:03 75-01-4
m&p-Xylene <1.8 uglL 2.0 1,8 1 04/21/00 12:03 1330-20-7
o-Xylene <0.83 ug/L 1.0 0.83 1 04/21109 12:03 85-47-8
4-Bromofluombenzene (S) 88 % 70-130 1 04/21/00 12:03 460-00-4
Dlbromofluommethane(S) 124 % 70-130 1 04121/0912:03 1888-53-7
Toluene-d8 (S) 98 % 70-130 1 04121/09 12:03 2037-26-5
I I I
Date: 04123/2009 08:53 AM
REPORT OF LABORATORY ANALYSIS
This r~port shall not be reproduced, except in full, without the w~tten conlent of Pa~ Analytical Se~cea, Inc..
Page 20 of 25
. aceAnalyticalO
I I I I I I I I I I I I I I I I I
QUALITY CONTROLDATA
Project: East Side P&T WO 901 Pace Project No.: 4016184
QC Batch: MSVI4228 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Descri0tJon: 8260 MSV
Associated Lab Samples: 4016184001,4016184002, 4016184003, 4016184004, 4016184005, 4010184008, 4016184007, 4010184008
METHOD BLANK; 147640 Matdx: Water
Associated Lab Samples: 4010184001,4018184002, 4016184003, 4016184004, 4016184005. 4018184006, 4016184007, 4010184008 Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane ug/L <0.02 1.0 04121/09 08:29
1,1,1-Tdchloroethane uglL <0.90 1.0 04121109 08:29
1,1,2,2-Tetrachloroethane uglL <0.20 1.0 04121/09 08:29
1,1,2-Trichloroethane ug/L <0.42 1.0 04/21/09 08:29
1,1,2-Trichlomtdfluomethane ug/L <1.3 5.0 04/21100 08:29
1,l-Dlchlomethana ug/L <0.75 1.0 04/21/00 08:29
l,l-Dlchloroethene ug/L <0,57 1.0 04/21/08 08:29
1,l-Dlchlompropene uglL <0.75 1.0 04/21/09 08:29
1,2,3oTrichlombenzene uglL <0.74 1.0 04/21/09 08:20
1,2,3-Tdchlompropane uglL <0.99 1.0 04/21/09 08:29
1,2,4-Tdchlombenzene ug/L <0.97 1.0 04/21/09 08:29
1,2,4.Tdmethylbenzene uglL <0.97 1.0 04/21/09 08:29
1,2-DIbromo-3-chloropmpana ug/L <1.7 5.0 04121109 08:29
1,2-Oibromoethane (EDB) uglL <0.56 1.0 04/21/09 08:29
1,2-Dichlorobenzene uglL <0.83 1.0 04/2110908:28
1,2-Dichloroethane uglL <0.36 1.0 04/21/09 08:29
1,2-Dichloropropane ug/L <0.49 1.0 04/21/00 08:29
1,3,5-Trimethylbenzene ug/L <0.83 1.0 04/21/09 08:29
1,3-Dlchlorobenzene uglL <0.87 1.0 04/21/0908:29
1,3-Dichloropropane uglL <0.61 1.0 04121/09 08:29
1,4-DIchlombenzene uglL <0.95 1.0 04121109 08:29
2,2.O]chlompmpane uglL <0.62 1.0 04121/09 08:29
2-Butsnone (MEK) ug/L <4.3 20.0 04/21/09 08:29
2-Chlorotoluene ug/L <0.85 1.0 04/21/09 08:29
4-Chlomtoluene uglL <0.74 1.0 (}4/21/00 08:29
4-Methyl-2opentanona (MIBK) ug/L <1,2 5.0 04/21109 08:29
Acetone ug/L <5.0 20.0 04121109 08:29
Allyl chlodde ug/L <2.0 5.0 04/21/09 08:29
Benzene ug/L <0.41 1,0 04/21/09 08:29
Bromobenzene uglL <0.82 1.0 04/21109 08:29
Bromochloromethane ug/L <0,97 1.0 04121109 08:29
Bromodlchloromethane ug/L <0,56 1.0 04/21109 08:29
Bromoform uglL <0.94 1.0 04/21/09 08:29
Bromomethane uglL <0.91 1.0 04/21/09 08:20
Carbon tetrachlodde ug/L <0.49 1.0 04/21109 08:29
Chlorobenzane uglL <0.41 1.0 04/21/09 08:29
Chforoethane ug/L <0.07 1.0 04,21/09 08:29
Chloroform ug/L <1.3 5.0 04/21/00 08:29
Chloromethane uglL <0.24 1.0 04/21109 08:29
cis-l,2-Dichlomethene ug/L <0.83 1.0 04/21/09 08:29
cis-l,3-Dlchlompropene ug/L <0.20 1.0 04/21/0908:29
Dibromochloromathane ug/L <0.81 1.0 04/21/09 08:29
Dlbromomethane uglL <0.60 1.0 04/21/00 08:29
Date: 04/2312009 08:53 AM
