Oil Analysis
Oil Analysis
About POLARIS
About POLARIS
Oil Analysis
Oil Analysis
Wear Debris Analysis
Wear Debris Analysis
Data Interpretation/Alarm Limits
Data Interpretation/Alarm Limits
Sampling Methods
Sampling Methods
Information Technology
Information Technology
Significant Accomplishments
Significant Accomplishments
Since start-up in 1999:
Since start-up in 1999:
•• Established customers in all 50
Established customers in all 50
states and over 15 countries
states and over 15 countries
•• Total customer base of over 40,000
Total customer base of over 40,000
•• Reports available in 3 languages
Reports available in 3 languages
•• 300% growth rate over past 2 years
300% growth rate over past 2 years
•• Among top 25 fastest-growing
Among top 25 fastest-growing
privately-held companies in
privately-held companies in
Indianapolis for past 3 years
Indianapolis for past 3 years
Industries Served
Industries Served
Power Generation
Power Generation
Transportation
Transportation
Oil & Gas
Oil & Gas
Industrial
Industrial
POLARIS
POLARIS
Laboratories
Laboratories
supports oil analysis
supports oil analysis
and reliability
and reliability
maintenance
maintenance
programming in a
programming in a
wide variety of
wide variety of
industry applications.
industry applications.
Const/Mining
Const/Mining
Facility Locations
Facility Locations
Houston
Houston
Salt Lake City
Salt Lake City
•
•Three locations
Three locations –
– 1
1
database
database
•
•Accessible within 48
Accessible within 48
hours by ground
hours by ground
•
•24-48 hour turnaround
24-48 hour turnaround
•
•Local technical sales
Local technical sales
support
support
Indianapolis
One Lab Three Locations
One Lab Three Locations
BIG Advantages
BIG Advantages
••
Ship your sample to the
Ship your sample to the closest lab
closest lab
reducing transit time and cost
reducing transit time and cost
••
One phone number to call for
One phone number to call for entire program
entire program
••
Centralized Customer Service ensures a thorough
Centralized Customer Service ensures a thorough knowledge of
knowledge of
your program
your program
••
Centralized Data Analysis ensures consistent commenting and
Centralized Data Analysis ensures consistent commenting and
recommendations on all data from each of our
recommendations on all data from each of our laboratories
laboratories
••
One database secures data history even when samples are sent to
One database secures data history even when samples are sent to
a different lab
a different lab
Fluids Tested
Fluids Tested
Oil
Oil
••
Test for wear metals and contamination
Test for wear metals and contamination
••
Monitor fluid properties and suitability for
Monitor fluid properties and suitability for
use
use
Fuel
Fuel
••
Troubleshoot filter problems
Troubleshoot filter problems
••
Determine compliance with s
Determine compliance with supplier
upplier
specifications
specifications
Coolant
Coolant
••
Detect corrosive chemicals
Detect corrosive chemicals
••
Monitor silicate levels
Monitor silicate levels
••
Determine compliance with OEM
Determine compliance with OEM
antifreeze concentration
antifreeze concentration
recommendations
recommendations
POLARIS specializes in testing oil,
POLARIS specializes in testing oil,
fuel, coolants and water-based fluids.
ISO 17025
ISO 17025
A2LA Accreditation
A2LA Accreditation
••
Takes quality standard of
Takes quality standard of
ISO 9000 to higher level
ISO 9000 to higher level
••
Ensures traceability back
Ensures traceability back
to standard
to standard
••
Determines uncertainties
Determines uncertainties
and repeatability
and repeatability
••
Is highest level of quality
Is highest level of quality
attainable by a laboratory
attainable by a laboratory
backed by the most
backed by the most
stringent accrediting
stringent accrediting
body in the industry
body in the industry
ISO 9000
ISO 9000
Guide 25
Guide 25
ISO 17025
ISO 17025
ISO ISO 17025 17025 A2LA A2LAAbout POLARIS
About POLARIS
Oil Analysis
Oil Analysis
Wear Debris Analysis
Wear Debris Analysis
Data Interpretation/Alarm Limits
Data Interpretation/Alarm Limits
Sampling Methods
Sampling Methods
Information Technology
Information Technology
OIL IS THE LIFEBLOOD
OIL IS THE LIFEBLOOD
OF MANY SYSTEMS
OF MANY SYSTEMS
•• Oil analysis is like a blood test
Oil analysis is like a blood test
–
– A sample is taken
A sample is taken
–
– Sample is documented
Sample is documented
–
– Sample is delivered to a lab
Sample is delivered to a lab
–
– Tests are performed
Tests are performed
–
– Results are interpreted
Results are interpreted
–
Oil Analysis Basics
Oil Analysis Basics
WHY DO OIL ANALYSIS?
WHY DO OIL ANALYSIS?
•• To monitor changes in lubricant properties
To monitor changes in lubricant properties
•• To identify contamination and its affect on
To identify contamination and its affect on
a lubricant properties
a lubricant properties
•• To determine type and severity of wear
To determine type and severity of wear
occurring
WHAT DOES OIL ANALYSIS TELL US?
WHAT DOES OIL ANALYSIS TELL US?
•• Determine condition of the oil
Determine condition of the oil
−
−
Monitoring changes in the lubricant to determine if the oil is
Monitoring changes in the lubricant to determine if the oil is
suitable for continued use
suitable for continued use
•• Determine condition of the unit
Determine condition of the unit
–
– Analysis provides clues that can identify problems
Analysis provides clues that can identify problems so they can
so they can
be corrected before permanent damage occurs
be corrected before permanent damage occurs
–
– Evaluates wear data
Evaluates wear data
•• Determine effectiveness of maintenance
Determine effectiveness of maintenance
strategy
strategy
–
– Run to failure
Run to failure
–
MAINTENANCE STRATEGIES
MAINTENANCE STRATEGIES
Unplanned Maintenance
Unplanned Maintenance
•• Run it to failure
Run it to failure
–
– Very high maintenance cost
Very high maintenance cost
–
– Short component life
Short component life
–
MAINTENANCE STRATEGIES
MAINTENANCE STRATEGIES
Preventive Maintenance
Preventive Maintenance
•• Interval-based Maintenance
Interval-based Maintenance
–
– Moderately high cost
Moderately high cost
–
– Short component life for unique equipment
Short component life for unique equipment
–
MAINTENANCE STRATEGIES
MAINTENANCE STRATEGIES
Predictive Maintenance
Predictive Maintenance
•• Condition-based and Planned
Condition-based and Planned
–
– Lowest overall cost
Lowest overall cost
–
– Considers unique component characteristics
Considers unique component characteristics
–
– Provides trending that can predict problems
Provides trending that can predict problems
and failures
and failures
–
– Increases component life
Increases component life
–
TESTING LUBRICANT PROPERTIES
TESTING LUBRICANT PROPERTIES
•• Viscosity
Viscosity
•• Viscosity Index
Viscosity Index
•• TAN
TAN
•• TBN
TBN
•• Oxidation
Oxidation
•• Nitration
Nitration
•• Demulsibility
Demulsibility
•• Foaming
Foaming
•• Rust
Rust
•• Copper Corrosion
Copper Corrosion
•• RPVOT
RPVOT
•• Pour Point
Pour Point
•• Flash Point
Flash Point
•• Aniline Point
Aniline Point
VISCOSITY
VISCOSITY
•• Shear force/shear rate
Shear force/shear rate
•• Factors that affect
Factors that affect viscosi
viscosity
ty
•• Temperature/relatio
Temperature/relationship by
nship by grade
grade
•• Pressure
Pressure
•• Measurement
Measurement
•• Comparative classifications
Comparative classifications
•• Viscosity Index
Viscosity Index
Viscosity is a
Viscosity is a
lubricant’s resistance to flow at a
lubricant’s resistance to flow at a
given temperature.
VISCOSITY
VISCOSITY
The force required to slide one object over another
The force required to slide one object over another
when the two surfaces are fully separated by a fluid is
when the two surfaces are fully separated by a fluid is
dependent on the fluid’s viscosity
dependent on the fluid’s viscosity
Stationary Surface
Stationary Surface
Moving Surface
Moving Surface
Sheared
Sheared
Liquid
Liquid
Shear Force (per area)
Shear Force (per area)
Viscosity =
Viscosity =
Shear Rate (flow)
Shear Rate (flow)
The higher a fluid’s
The higher a fluid’s
viscosity, the greater
viscosity, the greater
the force (energy)
the force (energy)
required to slide the
required to slide the
surfaces at a given
surfaces at a given
speed and gap
OPERATING
OPERATING
CONDITION
CONDITION
VISCOSITY
VISCOSITY
NEEDED
NEEDED
HIGHER LOAD
HIGHER LOAD
HIGHER
HIGHER
TEMPERATURE
TEMPERATURE
INCREASED
INCREASED
SPEED
SPEED
VISCOSITY SELECTION
VISCOSITY SELECTION
TOTAL ACID NUMBER
TOTAL ACID NUMBER
•• Measures amount of both organic and
Measures amount of both organic and
inorganic acid present
inorganic acid present
•• Indicates oxidation or contamination from
Indicates oxidation or contamination from
other corrosives
other corrosives
•• ASTM D-664M reported as mg/KOH per/g of
ASTM D-664M reported as mg/KOH per/g of
sample
sample
–
– Caution level >2X starting point of new oil
Caution level >2X starting point of new oil
–
TAN AND TBN BY TITRATION
TAN AND TBN BY TITRATION
OXIDATION
OXIDATION
•• Breakdown of a lubricant due to age and operating
Breakdown of a lubricant due to age and operating
conditions
conditions
•• Prevents additives from performing
Prevents additives from performing properly
properly
•• Causes the formation of acids and increases viscosity
Causes the formation of acids and increases viscosity
•• Testing done by Infrared Analysis (FTIR)
Testing done by Infrared Analysis (FTIR)
•• Rep
Report
orted a
ed as a
s au’s
u’s/cm
/cm (ab
(absor
sorpti
ption u
on uni
nits p
ts per c
er cent
entime
imeter
ter))
–
– 25 condemnation level by CAT & Waukesha
25 condemnation level by CAT & Waukesha
–
NITRATION
NITRATION
•• In
Indi
dica
cate
tes
s ex
exce
cess
ssiv
ive “
e “b
blo
low
w--by” from cylinder walls and/or
by” from cylinder walls and/or
compression rings
compression rings
•• Indicates presence of nitric acid, which speeds up oxidation
Indicates presence of nitric acid, which speeds up oxidation
•• Too much disparity between oxidation and
Too much disparity between oxidation and nitration points to
nitration points to
air-to-fuel ratio problems
air-to-fuel ratio problems
•• As oxidation/nitration increases, so d
As oxidation/nitration increases, so does TAN and viscosity,
oes TAN and viscosity,
while total base number will decrease
while total base number will decrease
•• Testing done by Infrared Analysis (FTIR)
Testing done by Infrared Analysis (FTIR)
•• Rep
Report
orted
ed as
as au’
au’s/cm
s/cm (Ab
(Absor
sorpti
ption
on uni
units
ts per
per cen
centim
timete
eter)
r)
–
– 25 condemnation level by CAT & Waukesha
25 condemnation level by CAT & Waukesha
–
FTIR - FUEL, SOOT,
FTIR - FUEL, SOOT,
OXIDATION, NITRATION
OXIDATION, NITRATION
REPORTING MEASUREMENTS
REPORTING MEASUREMENTS
Fu
Fue
el
l %
% So
Soot
ot %
% W
Wa
atte
er
r %
% Vi
Vis
s @
@ 4
40
0 Vi
Vis
s @
@ 1
10
00
0 A
AN
N BN
BN O
Ox
xi
i Ni
Nitt
Per Cent By
Per Cent By
Volume
Volume
Viscosity In
Viscosity In
Centistokes
Centistokes
–
–
cSt
cSt
at Specified
at Specified
Temperature
Temperature
Neutralization
Neutralization
Number Expressed
Number Expressed
In Mg/KOH/g
In Mg/KOH/g
FT-IR Results
FT-IR Results
Expressed In
Expressed In
Absorbance Units
Absorbance Units
Per Centimeter
Per Centimeter
CONTAMINANT LIMITS
CONTAMINANT LIMITS
Oil
Silico
Oil
Silico
n
n
Sodium Potassiu
Sodium Potassiu
m
m
Fue
Fue
l %
l %
Soot
Soot
%
%
Oxidatio
Oxidatio
n
n
Nitration
Nitration
Diesel
Diesel
Engine
Engine
20
20
70
70
20
20
2
2
2
2
20
20
20
20
160
160
250
250
250
250
6
6
6
6
30
30
30
30
Transmission
Transmission
20
20
50
50
20
20
N/A
N/A
N/A
N/A
25
25
N/A
N/A
160
160
90
90
150
150
N/A
N/A
N/A
N/A
40
40
N/A
N/A
Gear Box
Gear Box
20
20
75
75
80
80
N/A
N/A
N/A
N/A
30
30
N/A
N/A
256
256
307
307
180
180
N/A
N/A
N/A
N/A
50
50
N/A
N/A
Hydraulic
Hydraulic
15
15
25
25
10
10
N/A
N/A
N/A
N/A
20
20
N/A
N/A
65
METALS BY ELEMENTAL ANALYSIS
METALS BY ELEMENTAL ANALYSIS
Wear Metals
Wear Metals
Contaminants
Contaminants
Lubricant
Lubricant
Additives
Additives
F
Fee
C
Crr
N
Ni
i A
Al
l C
Cu
u P
Pb
b S
Sn
n C
Cd
d A
Ag
g
T
Tii
V
V
S
Si
i N
Naa
K
K
M
Mo
o S
Sb
b M
Mn
n
Lii
L
B
B M
Mg
g C
Ca
a B
Ba
a P
P Z
Zn
n
1
13 3 0 0 0 0 1 1 2 2 0 0 0 0 0 0 0 0 0 0 0 0 3 3 3 3 0 0 0 0 0 0 0 0 0 0 5 5 0 0 2244449 9 0 0 1122660 0 11114444
Reported in concentrations of parts per million - ppm
Reported in concentrations of parts per million - ppm
Multi - Source
ICP SPECTROMETER
ICP SPECTROMETER
FLAGGING POINTS & ALARM
FLAGGING POINTS & ALARM
LIMITS
LIMITS
••
sample information YOU provide
sample information YOU provide
the lab
the lab
••
OEM/equipment specifications
OEM/equipment specifications
••
lubricant specifications
lubricant specifications
••
laboratory database of samples
laboratory database of samples
with same criteria
with same criteria
••
s
stta
attiis
sttiic
ca
al a
l an
na
aly
lys
siis o
s of “
f “re
rea
al l
l liiffe
e””
laboratory data
laboratory data
Where do the numbers come from?
SETTING ALARM LIMITS
SETTING ALARM LIMITS
•• Statistics used to establish alarm limits for wear
Statistics used to establish alarm limits for wear
metal concentrations
metal concentrations
•• Mean (average, indicated by x) and standard
Mean (average, indicated by x) and standard
deviation (the distance the spread of numbers
deviation (the distance the spread of numbers
are from the mean, indicated by
are from the mean, indicated by σ
σ ) are
) are
determined for each population of elemental
determined for each population of elemental
concentrations
concentrations
•• How many standard deviations from the mean (-
How many standard deviations from the mean
(-3 to +(-3) alarm limits will be set is based on
3 to +3) alarm limits will be set is based on
frequency distribution
ALARM LIM
ALARM LIMIT SPECIF
IT SPECIFICS
ICS
•• Base alarm limits on specific information
Base alarm limits on specific information
–
– Unit Type
Unit Type
•• Diesel Engine
Diesel Engine
•• Turbine
Turbine
•• Compressor
Compressor
–
– Reciprocating, Rotary Screw, Centrifugal
Reciprocating, Rotary Screw, Centrifugal
•• Gear System
Gear System
–
– Helical, Double Helical, Hypoid, Worm
Helical, Double Helical, Hypoid, Worm
•• Hydraulic System
Hydraulic System
•• Bearing
Bearing
–
– Babbitt, Roller, Spherical Roller, Needle
Babbitt, Roller, Spherical Roller, Needle
•• Pump
Pump
–
– Piston, Gear, Vane
Piston, Gear, Vane
–
Information Pyramid
Information Pyramid
Transmission
Transmission
217
217
PPM
PPM
Iron
Iron
Flagging
Flagging
Point
Point
Information Pyramid
Information Pyramid
Transmission
Transmission
217
217
PPM
PPM
Iron
Iron
Flagging
Flagging
Point
Point
Automatic Tran
Automatic Transmission
smission
149
149
Information Pyramid
Information Pyramid
PPM
PPM
Iron
Iron
Flagging
Flagging
Point
Point
Transmission
Transmission
217
217
Automatic Tran
Automatic Transmission
smission
149
149
Allison
Allison
171
171
Information Pyramid
Information Pyramid
PPM
PPM
Iron
Iron
Flagging
Flagging
Point
Point
Automatic Tr
Automatic Transmission
ansmission
149
149
Transmission
Transmission
217
217
Allison
Allison
171
171
HT754CR
68
HT754CR
68
Transmission
Transmission
217
217
Automatic
Automatic Transm
Transmission
ission
149
149
Allison
Allison
171
171
HT754CR
HT754CR
68
68
10µm
10µm
Fltr
Fltr
60
60
Information Pyramid
Information Pyramid
PPM
PPM
Iron
Iron
Flagging
Flagging
Point
Point
217
217
10µm
10µm
Fltr
Fltr
52
52
Information Pyramid
Information Pyramid
Iron
Iron
PPM
PPM
Flagging
Flagging
Point
Point
Lack of
Lack of
information
information
allows 165
allows 165
ppm where
ppm where
failure may
failure may
occur!!!
occur!!!
WEAR METAL LIMITS
WEAR METAL LIMITS
Oil
Oil
Iron
Iron
Chrome
Chrome Nickel
Nickel
Aluminum
Aluminum
Coppe
Coppe
rr
Lea
Lea
d
d
Tin
Tin
Gas Turbines
Gas Turbines
7
7
1
1
1
1
4
4
6
6
4
4
3
3
35
35
5
5
7
7
20
20
24
24
28
28
30
30
Rotary Screw
Rotary Screw
Compressors
Compressors
62
1
62
1
2
2
5
5
15
15
5
5
7
7
217
217
7
7
6
6
32
32
120
120
40
40
56
56
Injection
Injection
Molding
Molding
19
1
19
1
1
1
1
1
42
42
6
6
1
1
95
95
5
5
4
4
8
8
88
88
54
54
10
10
Roller Bearing
Roller Bearing
141
141
4
4
2
2
16
16
26
26
13
13
7
7
493
14
493
14
8
8
59
59
208
208
104
104
56
56
DIESEL ENGINE LIMITS BY MFR
DIESEL ENGINE LIMITS BY MFR
MFR
MFR
Iron
Iron
Chrome
Chrome Nickel
Nickel
Aluminum
Aluminum
Coppe
Coppe
rr
Lead Tin
Lead Tin
Cummins
Cummins
60
60
7
7
4
4
14
14
21
21
47
47
5
5
390
390
46
46
20
20
98
98
147
147
353
353
40
40
CAT
CAT
66
66
6
6
3
3
9
9
37
37
24
24
5
5
429
429
39
39
15
15
63
63
259
259
180
180
40
40
Navistar
Navistar
77
77
7
7
3
3
6
6
17
17
20
20
5
5
501
501
46
46
15
15
42
42
1
119
19
150
150
40
40
Volvo
Volvo
74
74
6
6
5
5
13
13
44
44
16
16
5
5
481
481
39
39
25
25
91
91
308
308
120
120
40
40
DIESEL ENGINE LIMITS BY MODEL
DIESEL ENGINE LIMITS BY MODEL
CA
CAT
T
Iron
Iron
Chrome
Chrome Nickel
Nickel
Aluminum
Aluminum
Coppe
Coppe
rr
Lead Tin
Lead Tin
3406E
3406E
43
43
3
3
3
3
5
5
54
54
5
5
4
4
280
20
280
20
15
15
35
35
378
378
38
38
32
32
3304
3304
49
49
6
6
3
3
9
9
38
38
7
7
5
5
319
39
319
39
15
15
63
63
266
266
53
53
40
40
3512B
3512B
19
19
3
3
3
3
6
6
43
43
7
7
3
3
124
20
124
20
15
15
42
42
301
301
53
53
24
24
3516
3516
13
13
3
3
3
3
4
4
48
48
5
5
3
3
85
85
20
20
15
15
28
28
336
336
38
38
24
24
TREND ANALYSIS
TREND ANALYSIS
•• Oil Analysis works best when at least three samples
Oil Analysis works best when at least three samples
have been taken over a short period of time so that
have been taken over a short period of time so that
trends can be
trends can be identified
identified
•• Result trends over a sufficient period of time
Result trends over a sufficient period of time are more
are more
useful than absolute numbers when trying to determine
useful than absolute numbers when trying to determine
what is occurring in a
what is occurring in a sampled machine.
sampled machine.
•• Trending and graphing offer an easy to read
Trending and graphing offer an easy to read
instantaneous analysis of the condition of the equipment,
instantaneous analysis of the condition of the equipment,
condition of the lubricant, and level of contamination.
condition of the lubricant, and level of contamination.
•• Never base a decision to tear down a machine on the
Never base a decision to tear down a machine on the
results of only one (1) oil analysis report
results of only one (1) oil analysis report
TREND ANALYSIS
TREND ANALYSIS
•• Physical property trends help determine if the
Physical property trends help determine if the
best lubricant is being used
best lubricant is being used
•• Trend analysis helps in
Trend analysis helps in scheduling regular
scheduling regular
maintenance such as oil and/or filter changes
maintenance such as oil and/or filter changes
•• Tr
Tren
end an
d anal
alys
ysis h
is hel
elps e
ps est
stab
ablilish “
sh “be
best
st
practices” maintenance procedures
practices” maintenance procedures
TREND ANALYSIS
TREND ANALYSIS
•• “T
“Top
oppi
ping o
ng off
ff” wi
” will s
ll ske
kew th
w the tr
e tren
end an
d and
d
should be noted when the sample is
should be noted when the sample is
submitted to the laboratory for processing
submitted to the laboratory for processing
•• Note sump or
Note sump or reservoir capacity
reservoir capacity
•• Note if multiple components are lubricated
Note if multiple components are lubricated
from
from same
same sump,
sump, i.e.
i.e. motor
motor or
or turbine,
turbine,
gearbox, compressor
WHAT IS CONSIDERED
WHAT IS CONSIDERED
SIGNIFICANT CHANGE?
SIGNIFICANT CHANGE?
•• Wear Metals
Wear Metals
–
– an increase of 5 to 20 ppm - depending on the
an increase of 5 to 20 ppm - depending on the
metal and the unit type - or an increase of
metal and the unit type - or an increase of
100%, whichever is larger
100%, whichever is larger
•• Contaminant Metals
Contaminant Metals
–
– an increase of 5 to 10 ppm or an increase of
an increase of 5 to 10 ppm or an increase of
100%, whichever is larger
WHAT IS CONSIDERED
WHAT IS CONSIDERED
SIGNIFICANT CHANGE?
SIGNIFICANT CHANGE?
•• Water
Water
–
– an increase of 100%, or
an increase of 100%, or any increase that
any increase that
approaches the advisory levels of that
approaches the advisory levels of that sample
sample
point
point
•• Total Acid Number
Total Acid Number
–
– an increase of 0.1 for R&O oils
an increase of 0.1 for R&O oils
–
– an increase of 0.2 for AW oils
an increase of 0.2 for AW oils
–
WHAT IS CONSIDERED
WHAT IS CONSIDERED
SIGNIFICANT CHANGE?
SIGNIFICANT CHANGE?
•• Viscosity
Viscosity
–
– an increase or decrease of 5%
an increase or decrease of 5%
•• increases usually indicate lubricant degradation
increases usually indicate lubricant degradation
•• decreases indicate product
decreases indicate product contamination
contamination
•• Direct Read
Direct Read Ferrography
Ferrography
–
– a 50% increase of either DRS or DRL
a 50% increase of either DRS or DRL
•• ISO Particle Count
ISO Particle Count
–
– an increase of 2 classes in
an increase of 2 classes in any of the
any of the
reporting ranges (2/5/15 or 4/6/14)
HOW TO READ
HOW TO READ
OIL ANALYSIS REPORTS
OIL ANALYSIS REPORTS
••
Does the report suggest maintenance action?
Does the report suggest maintenance action?
–
– Yes
Yes
•• Consider all other available diagnostic information (vibration,
Consider all other available diagnostic information (vibration,
thermography, in-line sensors)
thermography, in-line sensors)
•• Act on the
Act on the recommen
recommendation or or
dation or order more
der more testing.
testing.
•• If lube change recommendation is due to contamination,
If lube change recommendation is due to contamination, ACT ON
ACT ON
RECOMMENDATION
RECOMMENDATION
to ensure fluid integrity
to ensure fluid integrity
–
– No
No
•• Is re-sampling recommended?
Is re-sampling recommended?
–
– Yes
Yes
»
» Send se
Send second sa
cond sample im
mple immedi
mediately or at ha
ately or at half norm
lf normal sampl
al sample inter
e interval to
val to
verify results
verify results
1. Review highest severity
1. Review highest severity
reports first
2. Review cautionary reports
2. Review cautionary reports
•• Pay particular attention to cautionary data as it becomes
Pay particular attention to cautionary data as it becomes
more useful as more data
more useful as more data is acquired
is acquired –
– trends will
trends will
become easier to identify and appropriate actions to take
become easier to identify and appropriate actions to take
will appear clearer.
will appear clearer.
•• Sa
Samp
mple r
le res
esul
ults
ts ar
are “b
e “bor
orde
derl
rlin
ine”
e” - some wear and
- some wear and
contaminatio
contamination results may be
n results may be flagged but don’t
flagged but don’t
necessarily indicate failure mode or results are not
necessarily indicate failure mode or results are not
significan
significant enough to
t enough to warrant action.
warrant action.
HOW TO READ
HOW TO READ
OIL
3. Review normal reports
3. Review normal reports
•• As time permi
As time permits, review norm
ts, review normal reports to learn w
al reports to learn what
hat
“normal” results are for each
“normal” results are for each unit sampled. Trends are
unit sampled. Trends are
then more easily recognized.
then more easily recognized.
HOW TO READ
HOW TO READ
OIL
SAMPLE INFORMATION
SAMPLE INFORMATION
Unit Type and ID
Unit Type and ID should give as much detail asshould give as much detail as possible.
possible. What kind ofWhat kind of compressor, gearbox,compressor, gearbox, engine, etc. influences flagging parameters and engine, etc. influences flagging parameters and depth of analysis. Different
depth of analysis. Different applicationsapplications and and metallurgies require different lubrication and have metallurgies require different lubrication and have great impact on how results are interpreted. great impact on how results are interpreted.
Manufacturer and Manufacturer and Model
Model can also can also identify metallurgies identify metallurgies involved as well as involved as well as the OEM’s standard the OEM’s standard maintenance maintenance guidelines and guidelines and possible wear possible wear patterns to expect. patterns to expect.
Lube Manufacturer, Type and Lube Manufacturer, Type and Grade
Grade identifies a lube’sidentifies a lube’s
properties and its viscosity and is properties and its viscosity and is critical in determining if the right critical in determining if the right lube is being used.
lube is being used.
Severity Status Levels: Severity Status Levels: 00——NormalNormal
11——Some items have violated initial flagging points yet are stillSome items have violated initial flagging points yet are still considered minor.
considered minor.
22—— A trend is developing. A trend is developing.
33——Simple maintenance and/or diagnostics are recommended.Simple maintenance and/or diagnostics are recommended. 44——Failure is eminent if maintenance not performed.Failure is eminent if maintenance not performed.
A
A Lab #Lab # is assigned to theis assigned to the sample upon entry for sample upon entry for processing and serves as a processing and serves as a reference number when reference number when communicating questions or communicating questions or Filter Types
Filter Types and theirand their Micron Ratings Micron Ratings areare important in analyzing important in analyzing particle count
particle count——thethe higher the micron higher the micron
Sump Capacity Sump Capacity identifies the total identifies the total volume of oil (in gallons) volume of oil (in gallons) in
in which wear which wear metalsmetals are suspended and is are suspended and is
Lube Time
Lube Time is how long theis how long the oil has been used.
oil has been used. UnitUnit Time
Time is the age of theis the age of the equipment and equipment and LubeLube Added
Added is how much oil hasis how much oil has
Make note of the difference Make note of the difference between the
between the Date SampledDate Sampled andand the
the Date ReceivedDate Received by the lab. by the lab. Turnaround issues may point to Turnaround issues may point to storing samples too long before storing samples too long before mailing or mail service problems. mailing or mail service problems.
UNDERSTANDING RESULTS
UNDERSTANDING RESULTS
ELEMENTAL ANALYSIS
ELEMENTAL ANALYSIS
Combinations of these
Combinations of these Wear MetalsWear Metals cancan identify components within the machine that identify components within the machine that are wearing. Knowing what metals a unit is are wearing. Knowing what metals a unit is made of can greatly influence an analyst’s made of can greatly influence an analyst’s recommendations and determine the value recommendations and determine the value of elemental analysis.
of elemental analysis.
Knowledge of the environmental conditions under Knowledge of the environmental conditions under
Additive
Additive and and Multi-Source MetalsMulti-Source Metals may turn up in test results for a variety of may turn up in test results for a variety of reasons. Molybdenum, antimony and boron are additives in some oils. reasons. Molybdenum, antimony and boron are additives in some oils.
Magnesium, calcium and barium are often used in detergent/dispersant additives. Magnesium, calcium and barium are often used in detergent/dispersant additives. Phosphorous is used as an extreme pressure additive in gear oils. Phosphorous, Phosphorous is used as an extreme pressure additive in gear oils. Phosphorous, along with zinc, are used in anti-wear additives (ZDP).
TEST DATA
TEST DATA
Depending on lube grade, Depending on lube grade, Viscosity
Viscosity is tested at 40° is tested at 40° and/or 100° C and reported in and/or 100° C and reported in centiStokes.
centiStokes.
Too much disparity between oxidation and nitration Too much disparity between oxidation and nitration can indicate air to fuel ratio problems. As
can indicate air to fuel ratio problems. As Oxidation/Nitration
Oxidation/Nitration increases, increases, TATANN will also will also increase and
increase and TBNTBN will begin to decrease. will begin to decrease. High
High Fuel DilutionFuel Dilution decreases unit decreases unit load capacity. Excessive
load capacity. Excessive SootSoot is a is a sign of reduced combustion sign of reduced combustion efficiency.
efficiency.
T
Totalotal AAcidcid NNumbers higher than that of new lubeumbers higher than that of new lube indicate oxidation or some type of contamination. indicate oxidation or some type of contamination.
The
The ISO CodeISO Code is an index number that represents a range of particles within a specificis an index number that represents a range of particles within a specific micron range, i.e. 4, 6, 14. Each class designates a range of measured particles per micron range, i.e. 4, 6, 14. Each class designates a range of measured particles per
UNDERSTANDING RESULTS
UNDERSTANDING RESULTS
FLAGGING AND COMMENTING
FLAGGING AND COMMENTING
125
125
^^^^^
^^^^^
Numbers with
Numbers with
“carrots”“carrots”printed below them denote
printed below them denote
test results the analyst has
test results the analyst has
flagged
flagged because they
because they
exceed pre-set warning
exceed pre-set warning
parameters and warrant
parameters and warrant
closer examination or
closer examination or
require action.
Test Reports
Test Reports
••
Report 24 metals (wear,
Report 24 metals (wear,
contaminant, multi-source
contaminant, multi-source
& additive
& additive
••
10 graphs on every report
10 graphs on every report
••
5 severity status levels
5 severity status levels
••
Flags clearly identifiable on
Flags clearly identifiable on
all reports
all reports
••
New lube reference
New lube reference
availability
availability
••
Reports accessible by
Reports accessible by
internet, fax and paper
internet, fax and paper
••
Report Particle Sizes and
Report Particle Sizes and
ISO Code
ISO Code
About POLARIS
About POLARIS
Oil Analysis
Oil Analysis
Wear Debris Analysis
Wear Debris Analysis
Data Interpretation/Alarm Limits
Data Interpretation/Alarm Limits
Sampling Methods
Sampling Methods
Information Technology
Information Technology
SAMPLING
SAMPLING
•• Objectives
Objectives
–
– Maximize data density
Maximize data density
–
– Minimize data disturbance
Minimize data disturbance
–
– Determine proper frequency
Determine proper frequency
•• Sampling Considerations
Sampling Considerations
–
– Sampling location
Sampling location
–
– Sampling hardware
Sampling hardware
–
– Sample bottle
Sample bottle
–
ACTIVE
ACTIVE ZONE SAM
ZONE SAMPLING
PLING
•• Sample from live fluid zones
Sample from live fluid zones
•• Sample from turbulent zones such as
Sample from turbulent zones such as
elbows
elbows
•• Sample downstream of bearings, gears,
Sample downstream of bearings, gears,
pumps, cylinders and actuators
pumps, cylinders and actuators
•• Sample machine during typical working
Sample machine during typical working
conditions and at normal operating
conditions and at normal operating
temperature
ACTIVE Z
ACTIVE ZONE SAM
ONE SAMPLING
PLING
•• Do
Don’
n’t sa
t samp
mple
le fr
from
om de
dead p
ad pip
ipe l
e leg
egs or
s or
hoses
hoses
•• Do
Don’
n’t s
t sam
ampl
ple
e fr
from
om la
lami
mina
nar z
r zon
ones
es
•• Don
Don’t
’t sam
sample
ple aft
after
er fil
filte
ters o
rs or f
r from
rom sum
sumps
ps
•• Do
Don’
n’t sa
t samp
mple
le wh
when m
en mac
achi
hine i
ne is co
s cold o
ld orr
not operating
not operating
ACTIVE Z
SAMPLING PROCEDURES
SAMPLING PROCEDURES
•• Sampling Valve - Best
Sampling Valve - Best
•• Suction Pump - Second Best
Suction Pump - Second Best
•• Drain Plug - Least Best
Drain Plug - Least Best
SAMPLING DEVICES
SAMPLING DEVICES
Quick Draw
Quick Draw
•• Used on systems with 4-100
Used on systems with 4-100
lbs. psi with a permanently
lbs. psi with a permanently
installed valve and a
installed valve and a
disposable cap/needle/tube
disposable cap/needle/tube
assembly
SAMPLING DEVICES
SAMPLING DEVICES
Push Button Valve
Push Button Valve
•• Used on systems with 4-100 lbs. psi
Used on systems with 4-100 lbs. psi
and does not require tubing
and does not require tubing
Vacuum Pump
Vacuum Pump
•• Used on non-pressurized systems
Used on non-pressurized systems –
–
pump is attached to sample jar,
pump is attached to sample jar,
tubing is inserted into pump and
tubing is inserted into pump and
then dipstick or reservoir halfway
then dipstick or reservoir halfway –
–
pump activated until jar ¾ full
BEST PRACTICES SUMMARY
BEST PRACTICES SUMMARY
•• Samples are taken at normal operating temperature
Samples are taken at normal operating temperature
from an active zone upstream of filters and
from an active zone upstream of filters and
downstream of machine components
downstream of machine components
•• Sampling valves and devices are flushed and clean
Sampling valves and devices are flushed and clean
sample bottles are used at each sampling interval
sample bottles are used at each sampling interval
•• Samples are taken at the proper frequency
Samples are taken at the proper frequency
•• Lube type, equipment ID and hours on the oil and the
Lube type, equipment ID and hours on the oil and the
machine are accurately recorded
machine are accurately recorded
•• Samples are forwarded immediately to the laboratory
Samples are forwarded immediately to the laboratory
via a trackable shipping service
THE IMPORTANCE OF TIME
THE IMPORTANCE OF TIME
•• Trend analysis is most effective when
Trend analysis is most effective when
sampling intervals are consistent.
sampling intervals are consistent.
•• Samples should be taken according to
Samples should be taken according to
schedule and shipped to the laboratory
schedule and shipped to the laboratory
immediately.
immediately.
••
Turnaround issues can often be
Turnaround issues can often be
attributed to the amount of
attributed to the amount of time that
time that
elapses from when the sample is taken
elapses from when the sample is taken
to the time it ships.
Why was Aluminum Flagged?
Why was Aluminum Flagged?
High
High
Viscosity
Viscosity
V
VAALLUUEES S EEXXPPRREESSSSEED D IIN N PPAARRTTS S PPEER R MMIILLLLIIOON N ((PPPPMM) ) BBY Y WWEEIIGGHHT T LLUUBBE E FFLLUUIID D DDAATTAA W
WEEAAR R MMEETTAALLS S CCOONNTTAAMMIINNAANNT T AADDDDIITTIIVVE E MMEETTAALLSS
LLUU BB EE IIRR OO NN CC HH RR OO MM IIUU MM MM OO LLYY BB DD EE NN UU MM AA LLUU MM IINN IIUU MM CC OO PP PP EE RR LLEE AA DD TTIINN NN IICC KK EE LL SS IILL IICC OO NN SS OO DD IIUU MM PP OO TTAA SS SS IIUU MM BB OO RR OO NN MM AA GG NN EE SS IIUU MM CC AA LLCC IIUU MM PP HH OO SS PP HH OO RR UU SS ZZIINNCC VV IISS @@ 1100 00 CC TTAANN 1 12 2 1 1 0 0 3 3 3 3 1 1 1 1 0 0 0 0 2 2 7 7 9 9 0 0 11441 1 77774 4 22221 1 1133..9 9 00..8866 750 750 1 14 4 2 2 0 0 4 4 5 5 1 1 0 0 0 0 3 3 2 2 2 2 3 3 0 0 22008 8 66335 5 22336 6 1144..1 1 22..66 790 790 1 15 5 2 2 0 0 3 3 6 6 2 2 2 2 0 0 5 5 2 2 3 3 3 3 0 0 22008 8 66335 5 22336 6 1166..2 2 22..66 720 720 1 15 5 2 2 1 1 3 3 6 6 3 3 2 2 0 0 5 5 3 3 4 4 4 4 0 0 22775 5 66115 5 22335 5 1166..8 8 33..22 750 750 CHG.
CHG. II--R R II--R R II--R R II--R R II--RR WAT
WATEER R HCHCARARB OXID B OXID NITNITR R GLGLYYCC
Y Y 11 777711 1188 2200 00 Y Y 11 772222 2222 2211 00 N N 11 778844 2222 2211 00 Y Y 11 775522 2222 2211 00
V
VAALLUUEES S EEXXPPRREESSSSEED D IIN N PPAARRTTS S PPEER R MMIILLLLIIOON N ((PPPPMM) ) BBY Y WWEEIIGGHHT T LLUUBBE E FFLLUUIID D DDAATTAA W
WEEAAR R MMEETTAALLS S CCOONNTTAAMMIINNAANNT T AADDDDIITTIIVVE E MMEETTAALLSS
LLUU BB EE IIRR OO NN CC HH RR OO MM IIUU MM MM OO LLYY BB DD EE NN UU MM AA LLUU MM IINN IIUU MM CC OO PP PP EE RR LLEEAADD TTIINN NN IICC KK EE LL SS IILL IICC OO NN SS OO DD IIUU MM PP OO TTAA SS SS IIUU MM BB OO RR OO NN MM AA GG NN EE SS IIUU MM CC AA LLCC IIUU MM PP HH OO SS PP HH OO RR UU SS ZZIINNCC VV IISS @@ 1100 00 CC TTAANN 1 12 2 1 1 0 0 3 3 3 3 1 1 1 1 0 0 0 0 2 2 7 7 9 9 0 0 14141 1 77774 4 22221 1 1133..9 9 00..8866 750 750 1 14 4 2 2 0 0 4 4 5 5 1 1 0 0 0 0 3 3 2 2 2 2 3 3 0 0 20208 8 66335 5 22336 6 1144..1 1 22..66 790 790 1 15 5 2 2 0 0 3 3 6 6 2 2 2 2 0 0 5 5 2 2 3 3 3 3 0 0 20208 8 66335 5 22336 6 1144..2 2 22..66 720 720 1 15 5 2 2 0 0 3 3 6 6 3 3 2 2 0 0 770 0 3 3 4 4 4 4 0 0 22775 5 66115 5 22335 5 1144..8 8 22..66 750 750 CHG.
CHG. II--R R II--R R II--R R II--R R II--RR WAT
WATEER R HCHCARARB OXID B OXID NITNITR R GLGLYYCC
Y Y 11 777711 1188 2200 00 Y Y 11 772222 2222 2211 00 N N 11 778844 2222 2211 00
High Silicon
High Silicon
Iron Wear but why?
Iron Wear but why?
VALUES EXPRESSED IN PARTS PER MILLION (PPM) BY WEIGHT VALUES EXPRESSED IN PARTS PER MILLION (PPM) BY WEIGHT W
WEEAAR R MMEETTAALLS S CCOONNTTAAMMIINNAANNT T AADDDDIITTIIVVE E MMEETTAALLSS
LLUU BB EE IIRR OO NN CC HH RR OO MM IIUU MM MM OO LLYY BB DD EE NN UU MM AA LLUU MM IINN IIUU MM CC OO PP PP EE RR LLEE AA DD TTIINN NN IICC KK EE LL SS IILL IICC OO NN SS OO DD IIUU MM PP OO TTAA SS SS IIUU MM BB OO RR OO NN MM AA GG NN EE SS IIUU MM CC AA LLCC IIUU MM PP HH OO SS PP HH OO RR UU SS 1 155 11 00 33 33 11 11 00 1010 22 77 22 00 114411 777744 750 750 2 211 88 00 44 55 11 00 00 1818 55 77 22 00 220088 663355 790 790 9 977 2211 00 33 66 22 22 00 3535 66 77 44 00 220088 663355 720 720 2 21111 3300 00 33 66 22 22 00 7788 55 88 33 00 227755 661155 750 750 CHG.
CHG. II--R R II--R R II--R R II--R R II--RR W WAATTEER HR HCCAARRB B OOXXIID D NNIITTR R GGLLYYCC Y Y 11 777711 1188 2200 00 Y Y 11 772222 2222 2211 00 N N 11 778844 2222 2233 00 Y Y 11 775522 2222 2222 00