2-(3-carboxypropyl)-4
![2 [1 (4 Bromophenyl) 3 hydroxy 3 (4 methoxyphenyl)propyl]cyclohexanol](data:image/gif;base64,R0lGODlhAQABAIAAAP///wAAACH5BAEAAAAALAAAAAABAAEAAAICRAEAOw==)
2 [1 (4 Bromophenyl) 3 hydroxy 3 (4 methoxyphenyl)propyl]cyclohexanol
... C13 0.045 (2) 0.075 (3) 0.046 (2) −0.0012 (19) 0.0297 (19) 0.0007 (19) C14 0.053 (2) 0.058 (2) 0.048 (2) 0.0022 (19) 0.033 (2) 0.0056 (18) C15 0.053 (2) 0.062 ...
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2 (4 Methylphenyl) 2 oxoethyl 3 bromobenzoate
... C1 0.0446 (15) 0.0450 (15) 0.0505 (16) −0.0089 (12) −0.0063 (12) −0.0156 (12) C2 0.0567 (17) 0.0521 (17) 0.0504 (16) −0.0082 (13) −0.0129 (13) −0.0148 (13) C3 0.0624 (19) 0.0616 (19) 0.0565 (18) 0.0044 (15) −0.0214 (14) ...
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(E) 4 (4 Hydroxy 3 methoxyphenyl)but 3 en 2 one
... 4-Hydroxy-3-methoxybenzaldehyde (3.04 g, 20 mmol) was dissolved in 25 ml of acetone and 12 ml of dilute aqueous NaOH solution (10%) was added to the acetone solution with stirring. The mixture was allowed ...
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3 Ethoxy 4 [3 (2 ethoxy 4 formylphenoxy)propoxy]benzaldehyde
... C7 0.0726 (16) 0.0452 (11) 0.0458 (13) −0.0058 (12) 0.0028 (13) 0.0001 (11) C8 0.0694 (17) 0.0777 (18) 0.102 (3) −0.0085 (15) −0.027 (2) −0.0103 (19) C9 0.086 (2) 0.141 (3) 0.211 (5) 0.023 ...
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(Z) 3 Hydroxy 4 (4 methoxyphenyl)but 3 en 2 one
... the 3-hydroxybut-3-en-2-one, benzene and methoxyl fragments are almost ...The 3-hydroxybut- 3-en-2-one fragment is almost planar with an ...The 4-methoxy group also lies ...
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Methyl 3 (4 bromophenyl) 2 (1H indol 3 ylmethyl) 5 [1 (4 methoxyphenyl) 4 oxo 2 phenylazetidin 2 yl] 4 nitropyrrolidine 2 carboxylate
... The methoxy group is coplanar with the C17/C18/C19/C20/C21/C22 benzene ring: dihedral angle C21–C20–O6–C23 = 161.0 (4)°. The methoxyphenyl and the phenyl rings bridged by the β–lactam ring are oriented at an angle ...
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4′ (4 Methoxyphenyl) 1 methylchroman 3 spiro 3′ pyrrolidine 2′ spiro 2′′ indan 4,1′′,3′′ trione
... O24 0.0374 (5) 0.0522 (6) 0.0430 (5) −0.0111 (4) −0.0071 (4) −0.0030 (4) C25 0.0423 (7) 0.0495 (8) 0.0346 (6) −0.0153 (6) −0.0051 (5) −0.0070 (5) O26 0.0396 (5) 0.0462 (6) 0.0596 (6) −0.0043 ...
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4 (3 Allyloxy 2 bromophenoxy)but 2 enenitrile
... Crotonitrile (2.00 g, 0.03 mol), N-bromosuccinamide (6.3 g, 0.04 mol) and azoisobutyronitrile (0.49 g, 0.003 mol) were added to dry acetone (100 ml). The mixture was stirred at re¯ux under a nitrogen atmos- phere for ...
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2 (2 Fluoro 4 nitrophenoxy) 3 nitropyridine
... of 2-chloro-3-nitropyridine (1.0 g, 6.3 mmol) and 2-fluoro-4-nitrophenol ...MgSO 4 , and concentrated in vacuo to yield the crude product as a ...
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3 (2 Aminoethyl) 2 (4 fluoroanilino)quinazolin 4(3H) one
... of 2-ethoxycarbonyliminophosphorane (1.27 g, 3 mmol) in 10 ml anhydrous THF, 4-chlorophenyliso- cyanate ...g, 3 mmol) was added dropwise at room ...g, 3 mmol) in 5 ml anhydrous ...CH ...
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2 (3 Chlorophenyl) 4 (2 hydroxyethyl) 3 methylmorpholin 2 ol monohydrate
... Cl1 0.0319 (8) 0.0587 (12) 0.0534 (10) −0.0054 (8) 0.0299 (7) 0.0025 (9) C1 0.009 (2) 0.018 (3) 0.028 (3) −0.001 (2) 0.0048 (19) −0.001 (2) C2 0.011 (2) 0.023 (3) 0.025 ...
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3 Ethoxy 4 [2 (2 ethoxy 4 formylphenoxy)ethoxy]benzaldehyde
... A view of the molecule is shown in Fig. 1. A crystallographic center of symmetry is located at the mid-point of the C7—C7 i bond [symmetry code: (i) x + 2, y + 1, z + 1]. Each ethylvanillin unit (C1–C10/O1/O3) is ...
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2 (4 Fluoroanilino) 3 (2 hydroxyethyl)quinazolin 4(3H) one
... of 2–ethoxycarbonyliminophosphorane ...THF, 4–fluorophenyl iso- cyanate ...g, 3 mmol) in 5 ml anhydrous ...C 2 H 4 Cl 2 /CH 3 OH (1:1/v:v) to give colourless crystals of ...
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4 [4 (4 Formyl 2 methoxyphenoxy)butoxy] 3 methoxybenzaldehyde
... To a solution of 4-hydroxy-3-methoxybenzaldehyde (15.2 g, 10 mmol) and potassium carbonate (13.8 g, 10 mmol) in acetonitrile (500 ml), 1,4-dibromobutane (10.8 g, 5 mmol) was added over a period of 30 min ...
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SYNTHESIS, SPECTRAL AND THEORETICAL CHARACTERIZATION OF 5,6-DICHLORO/DIMETHYL-2-(2´,3´/2´,4´/2´,5´/3´,4´/3´,5´-DIMETHOXYPHENYL)-1H-BENZIMIDAZOLES
... compounds 2, 3 and 5 show triple fl uorescence whereas the other compounds present dual fl ...forms. 3´,4´-Dimethoxy derivatives (4 and 9) have higher melting points in comparison with ...
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Crystal structure of 2 (4 chlorophenyl) 3 (4 methoxyphenyl) 3 (methylsulfanyl)acrylonitrile
... To a stirred suspension of NaH (0.45 g, 11.0 mmol, 60% suspension in oil) in dry THF (25 ml), a solution of (4-chloro- phenyl)-acetonitrile (0.75 g, 5.0 mmol) and 4-methoxy-dithiobenzoic acid methyl ester ...
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4 [2 (4 Formyl 2 methoxyphenoxy)ethoxy] 3 methoxybenzaldehyde
... To a solution of 4-hydroxy-3-methoxybenzaldehyde (15.2 g, 10 mmol) and potassium carbonate (13.8 g, 10 mmol) in acetonitrile (500 ml), 1,2-dibromoethane (9.4 g, 5 mmol) was added over a period of 30 minutes ...
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4 [3 Benzoyl 4 (4 chlorophenyl) 1 methylpyrrolidin 2 yl] 1 (4 methoxyphenyl) 3 phenylazetidin 2 one
... C8 0.0725 (15) 0.130 (3) 0.0869 (18) −0.0119 (16) 0.0327 (13) 0.0131 (18) C9 0.0622 (12) 0.0796 (16) 0.0643 (13) −0.0096 (11) 0.0163 (10) 0.0088 (11) C10 0.0466 (9) 0.0493 (11) 0.0507 (10) −0.0076 (8) 0.0062 (7) ...
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3 Mesityl 2 oxo 1 oxaspiro[4 4]non 3 en 4 yl 2 (4 chlorophenyl) 3 methylbutyrate
... mmol), 4-dimethylaminopyridine ...min 2-(4-chlorophenyl)-3-methylbutanoyl chloride ...for 3 h and then 1% aqueous HCl was ...Na 2 SO 4 ...
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4 {2 [2 (4 Formyl 2 methoxyphenoxy)ethoxy]ethoxy} 3 methoxybenzaldehyde
... The synthesis of new and designed crystal structures continues to be an important area of research for chemists (Tynan et al., 2005; Parashar et al., 1988). One of the aims of crystal engi- neering is to establish ...
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