3-TRIAZOL-1-YL
Ethyl 6 (4 cyclopropyl 1H 1,2,3 triazol 1 yl)pyridine 3 carboxylate
... Data collection: APEX2 (Bruker, 2007); cell refinement: SAINT (Bruker, 2007); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 ...
7
Synthesis, characterization and biological activities of transition metal chelates of 2-aminothiazole-derived Mannich bases
... M = Cu(II), Co(II), Ni(II) and Zn(II)] L = N-((1H-benzo[d][1,2,3]triazol-1-yl)methyl)thiazol-2-amine] have been synthesized. The structural features have been arrived from their elemental analysis, ...
10
Crystal structure of 3 O benzyl 4(R) C (1 benzyl 1H 1,2,3 triazol 4 yl) 1,2 O isopropylidene α D erythrofuranose
... A search of the Cambridge Structural Database (Version 5.36; Groom & Allen, 2014) for substituted 3a,5,6,6a-tetrahydro- furo[2,3-d][1,3]dioxoles gave 485 hits (excluding organomet- allics). Three of them are ...
9
1 (2,5 Dimethoxyphenyl) 3 ferrocenyl 2 (1H 1,2,4 triazol 1 yl)prop 2 en 1 one
... The molecular structure of (I) is shown in Fig. 1. The Fe—C bond lengths range from 2.021 (3) to 2.042 (3) Å. The Fe1···Cg1 and Fe1···Cg2 distances are 1.634 (2) and 1.647 (2) Å, respectively (where ...
12
[Bis(triazol 1 yl)acetato]nickel(II) monohydrate
... Ni1 0.0364 (4) 0.0301 (4) 0.0241 (4) 0.0151 (2) −0.00220 (16) −0.0044 (3) O1 0.071 (3) 0.048 (2) 0.040 (2) 0.0235 (19) 0.0151 (18) −0.0096 (16) O2 0.038 (2) 0.061 (2) 0.066 (3) 0.0190 (19) 0.0044 ...
7
1 (4 Fluorophenyl) 2 (3 phenylthiazolidin 2 ylidene) 2 (1H 1,2,4 triazol 1 yl)ethanone
... C4 0.070 (3) 0.074 (3) 0.040 (2) 0.030 (2) 0.0050 (19) 0.0168 (19) C5 0.046 (2) 0.051 (2) 0.047 (2) 0.0128 (17) 0.0030 (16) 0.0170 (17) C6 0.0336 (18) 0.0427 (18) 0.0394 (17) 0.0150 (15) 0.0063 (14) 0.0175 ...
7
4 Amino 3 (1,2,4 triazol 1 yl) 1H 1,2,4 triazole 5(4H) thione
... 2-(1H-1,2,4-Triazol-1-yl)acetohydrazide (0.02 mol) and potassium hydroxide (0.02 mol) were dissolved in anhydrous ethanol (80 ml). Carbon disulfide (0.02 mol) was added dropwise to the solution. The ...
6
3 Pyridin 2 yl 1H 1,2,4 triazol 5 amine
... 1,2,4-Triazol-5-amines have been recognized as valuable synthons for the construction of fused heterocyclic systems, e.g. 1,2,4-triazolo[1,5-a]pyrimidines (Fischer, 2007) and 1,2,4-triazolo[1,5-a][1,3,5]triazines ...
6
1 Phenyl 2 (1H 1,2,4 triazol 1 yl)ethanol
... Data collection: COLLECT (Hooft, 1998); cell refinement: DENZO (Otwinowski & Minor, 1997) and COLLECT; data reduc- tion: DENZO and COLLECT; program(s) used to solve structure: SHELXL97 (Sheldrick, 2008); program(s) ...
6
Crystal structure and Hirshfeld surface analysis of ethyl 2 {[4 ethyl 5 (quinolin 8 yloxymethyl) 4H 1,2,4 triazol 3 yl]sulfanyl}acetate
... The synthesis of the title compound was performed according to the scheme in Fig. 5. Ethyl(quinoline-8-yloxy)acetate (2) was synthesized by condensation of 8-hydroxyquinoline (0.01 mol) (1) with ethyl bromoacetate ...
9
Investigation of Spectroscopic, Electronic and Geometric Properties of 2 (3 Methyl 4,5 Dihydro 1h 1,2,4 Triazol 5 On 4 Yl) Azomethine) Benzoic Acid using B3lyp and Hf Basis Sets
... Density Functional Theory (DFT) and Hartree-Fock (HF) methods with the 631G (d) basis sets of the program package Gaussian G09W. Obtained spectroscopic parameters are compared with experimental data. Otherwise, ...
7
2 (2,3 Dimethylphenoxy) 1 (pyridin 2 yl) 2 (1H 1,2,4 triazol 1 yl)ethanone
... on an ice-bath. The reaction mixture was stirred at room temperature for 2.5 h (monitored by TLC). The solution was filtered, and the filtrate was evaporated under reduced pressure. The residue was dissolved in 25 ml ...
9
1 (4 Fluorophenyl) 2 {4 phenyl 5 [(1H 1,2,4 triazol 1 yl)methyl] 4H 1,2,4 triazol 3 ylsulfanyl}ethanone
... S1 0.0507 (4) 0.0683 (5) 0.0467 (4) −0.0130 (3) 0.0092 (3) −0.0168 (3) F1 0.1028 (14) 0.1220 (15) 0.0460 (10) −0.0113 (11) 0.0134 (9) −0.0215 (9) O1 0.0465 (11) 0.0953 (15) 0.0594 (12) −0.0145 (10) ...
7
1 (Benzoylmethyl) 4 (3,5 dimethyl 4H 1,2,4 triazol 4 yl) 3 (2 thienylmethyl) 1H 1,2,4 triazol 5(4H) one
... 4-(3,5-Dimethyl-4H-1,2,4-triazol-4-yl)-3-(2-thienylmethyl)-1H-1,2,4- triazol-5(4H)-one ...(cm 1 ): 1658 (C O benzophenone), 1746 (C O triazole), 1597 (C N), 711(thiophene), 758 ...
9
(2E) 1 [5 Methyl 1 (4 methylphenyl) 1H 1,2,3 triazol 4 yl] 3 [4 (piperidin 1 yl)phenyl]prop 2 en 1 one1
... C42 0.072 (2) 0.106 (2) 0.0505 (16) −0.0104 (17) −0.0015 (15) −0.0159 (15) C43 0.084 (2) 0.095 (2) 0.0521 (16) −0.0065 (17) −0.0126 (15) −0.0154 (14) C44 0.083 (3) 0.134 (3) 0.080 (2) −0.023 (2) −0.0102 ...
15
Diaquabis{3 [4 (1H imidazol 1 yl)phenyl] 5 (pyridin 2 yl κN) 1H 1,2,4 triazol 1 ido κN1}zinc
... C4 0.052 (2) 0.037 (2) 0.043 (3) 0.0054 (18) −0.0035 (19) −0.008 (2) C5 0.0328 (19) 0.034 (2) 0.033 (2) 0.0002 (15) 0.0020 (16) 0.0004 (19) C6 0.038 (2) 0.033 (2) 0.032 (2) −0.0027 (16) 0.0065 (16) −0.0031 (18) C7 ...
8
3 Anilino 1 (2 fluoro 5 methylphenyl) 3 (methylsulfanyl) 2 (1H 1,2,4 triazol 1 yl)prop 2 en 1 one
... S1 0.0366 (3) 0.0796 (4) 0.0369 (3) 0.0015 (3) 0.0039 (2) −0.0162 (3) F1 0.0651 (9) 0.0683 (9) 0.0906 (11) −0.0167 (7) 0.0258 (8) −0.0295 (8) O1 0.0330 (7) 0.0847 (11) 0.0390 (7) 0.0091 (7) ...
7
4,5 Diamino 3 [(E,E) 4 (4,5 diamino 4H 1,2,4 triazol 3 yl)buta 1,3 dienyl] 4H 1,2,4 triazol 1 ium chloride
... Data collection: COLLECT (Nonius, 1999); cell refinement: DIRAX/LSQ (Duisenberg et al., 2000); data reduction: EVALCCD (Duisenberg et al., 2003); program(s) used to solve structure: SIR97 (Altomare et al., 1999); ...
7
2 (1H Benzotriazol 1 yl) 1 (2,5 dichlorophenyl) 2 (1H 1,2,4 triazol 1 yl)ethanone
... Cl2 0.0925 (7) 0.0709 (7) 0.0389 (5) 0.0121 (6) 0.0224 (5) 0.0051 (5) Cl1 0.0698 (7) 0.0610 (7) 0.0887 (8) −0.0232 (5) 0.0098 (6) −0.0261 (6) O1 0.0306 (12) 0.0428 (14) 0.0588 (15) 0.0027 (11) 0.0032 (11) 0.0040 (11) N1 ...
8
2 (1H Benzotriazol 1 yl) 1 (2,4 dichlorophenyl) 2 (1H 1,2,4 triazol 1 yl)ethanone
... The bond lengths and angles in (I) are within normal ranges (Allen et al., 1987) and comparable to those reported in the related compound 2-(1H-1,2,3-benzotriazol-1-yl)-1-(4-methylphenyl)-2- ...
8