SYNCHROTRON DATA
Crystal structure of ammonium bis(pyridine 2,6 dicarboxylato κ3O,N,O′)chromate(III) from synchrotron data
... complex was prepared as the Na + salt according to the literature (Hoggard & Schmidtke, 1973) and its crystal struc- ture determined using synchrotron data. Structural analysis showed the compound to be ...
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Crystal structure of ammonium/potassium trans bis(N methyliminodiacetato κ3O,N,O′)chromate(III) from synchrotron data
... methyliminodiacetate; mida), has been determined from synchrotron data. The Cr III atom is located on a centre of symmetry and is coordinated by two N atoms and four O atoms of two facially arranged ...
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Crystal structure of tris(trans 1,2 cyclohexanediamine κ2N,N′)chromium(III) tetrachloridozincate chloride trihydrate from synchrotron data
... synchrotron data to determine the exact composition and coordination geometry of the Cr III ion. The complex crystal- lizes in the space group I42d with eight formula units in a cell of dimensions a = ...
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Crystal structure of cis aquachloridobis(1,10 phenanthroline κ2N,N′)chromium(III) tetrachloridozincate monohydrate from synchrotron data
... been determined from synchrotron data. The Cr III ion is bonded to four N atoms from two 1,10-phenanthroline (phen) ligands, one water molecule and a Cl atom in a cis arrangement, displaying an overall ...
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Rietveld refinement of Ba5(AsO4)3Cl from high resolution synchrotron data
... high-resolution synchrotron X-ray powder diffraction data collection using station ...Daresbury Synchrotron Radiation ...these data were summed and normalized to account for decay of the ...
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Rietveld refinement of Ba5(AsO4)3Cl from high resolution synchrotron data
... 2003); data reduction: local software; method used to solve structure: coordinates taken from a related compound; program(s) used to refine structure: TOPAS (Coelho, 2000); molecular graphics: Balls and Sticks ...
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Rietveld refinement of Sr5(AsO4)3Cl from high resolution synchrotron data
... For crystal chemistry of apatites, see: Mercier et al. (2005); White & ZhiLi (2003); Wu et al. (2003). For powder diffraction data on Sr As-apatite, see: Kreidler & Hummel (1970). Atomic coordinates as ...
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catena Poly[[copper(I) μ 2,6 bis[4 (pyridin 2 yl)thiazol 2 yl]pyridine] hexafluoridophosphate acetonitrile monosolvate] from single crystal synchrotron data
... 1993); data reduction: XDS; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: Mercury (Macrae et ...
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Crystal structure of 1,4,8,11 tetraazoniacyclotetradecane bis(dichromate) monohydrate from synchrotron data
... 1997); data reduction: HKL3000sm (Otwinowski & Minor, 1997); program(s) used to solve structure: SHELXT2015 (Sheldrick, 2015a); program(s) used to refine structure: SHELXL2015 (Sheldrick, 2015b); molecular ...
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Crystal structure of trans bis(ethane 1,2 diamine κ2N,N′)bis(thiocyanato κN)chromium(III) perchlorate from synchrotron data
... Crystal data, data collection and structure refinement details are summarized in Table 2. In the title compound, the ethane- 1,2-diamine group is disordered with atoms N2A/N2B, C2A/ C2B, C3A/C3B and N3A/N3B ...
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Crystal structure of bis[trans (ethane 1,2 diamine κ2N,N′)bis(thiocyanato κN)chromium(III)] tetrachloridozincate from synchrotron data
... Crystal data, data collection and structure refinement details are summarized in Table 2. Hydrogen atoms bound to carbon or nitrogen were placed in calculated positions (C—H = 0.95, N—H = 0.91 A ˚ ), and ...
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Crystal structure of bis[trans dichloridobis(propane 1,3 diamine κ2N,N′)chromium(III)] dichromate from synchrotron data
... 1997); data reduction: HKL3000sm (Otwinowski & Minor, 1997); program(s) used to solve structure: SHELXT2014 (Sheldrick, 2015a); program(s) used to refine structure: SHELXL2014 (Sheldrick, 2015b); molecular ...
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Rietveld refinement of a natural cobaltian mansfieldite from synchrotron data
... 2001); data reduction: FIT2D (Hammersley, 1997); program(s) used to solve structure: atomic coordinates from Harrison (2000); program(s) used to refine structure: GSAS and EXPGUI; molecular graphics: VICS (Izumi ...
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Crystal structure of trans dichlorido(1,4,8,11 tetraazaundecane κ4N)chromium(III) perchlorate determined from synchrotron data
... 1997); data reduction: HKL3000sm (Otwinowski & Minor, 1997); program(s) used to solve structure: SHELXT (Sheldrick, 2015a); program(s) used to refine structure: SHELXL2014/7 (Sheldrick, 2015b); molecular ...
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Crystal structure of trans difluoridotetrakis(pyridine κN)chromium(III) trichlorido(pyridine κN)zincate monohydrate from synchrotron data
... 1997); data reduction: HKL3000sm (Otwinowski & Minor, 1997); program(s) used to solve structure: SHELXS2014 (Sheldrick, 2008); program(s) used to refine structure: SHELXL2014 (Sheldrick, 2008); molecular ...
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Crystal structure of cis aquachlorido(rac 5,5,7,12,12,14 hexamethyl 1,4,8,11 tetraazacyclotetradecane κ4N)chromium(III) tetrachloridozincate trihydrate from synchrotron data
... Crystal data, data collection and structure refinement details are summarized in Table 2. H atoms were placed in geome- trically idealized positions and constrained to ride on their parent atoms, with C—H = ...
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Orthorhombic Yb5Si4 from synchrotron powder data
... ture type) intensities. This compound was reported by Palenzona et al. (2002) as novel in the Yb±Si system. However, no re®ned atomic parameters were given. Our Rietveld re®nement using synchrotron data ...
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Sr–fresnoite determined from synchrotron X ray powder diffraction data
... For the crystal chemistry of fresnoites, see: Barbar & Roy (2012); Ho¨che et al. (2002); ICDD (1989). For properties of Sr–fresnoites, see: Park & Navrotsky (2010). Atomic coordi- nates as starting parameters for ...
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X ray laser diffraction for structure determination of the rhodopsin arrestin complex
... the synchrotron data, helped with the SFX data collection, processed the data, solved the structures, and wrote the paper; ...for synchrotron data collection, prepared all ...
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Sr–fresnoite determined from synchrotron X ray powder diffraction data
... For the crystal chemistry of fresnoites, see: Barbar & Roy (2012); Ho¨che et al. (2002); ICDD (1989). For properties of Sr–fresnoites, see: Park & Navrotsky (2010). Atomic coordi- nates as starting parameters for ...
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