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[PDF] Top 20 3 (1,3 Dioxolan 2 yl) 2 hydrazino 7 methyl­quinoline

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3 (1,3 Dioxolan 2 yl) 2 hydrazino 7 methyl­quinoline

3 (1,3 Dioxolan 2 yl) 2 hydrazino 7 methyl­quinoline

... The title compound (I), belongs to the quinoline class. Quinolines and quinolinones are an integral part of many naturally occurring fused heterocycles and find application in synthetic and pharmaceutical ... See full document

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Methyl 2 benz­yl­oxy 6 (2 methyl 1,3 dioxolan 2 yl)benzoate monohydrate

Methyl 2 benz­yl­oxy 6 (2 methyl 1,3 dioxolan 2 yl)benzoate monohydrate

... C3 0.0379 (9) 0.0354 (8) 0.0582 (10) −0.0099 (7) 0.0129 (8) −0.0018 (7) C4 0.0409 (9) 0.0350 (8) 0.0440 (9) −0.0027 (6) 0.0109 (7) −0.0063 (7) C5 0.0309 (8) 0.0301 (7) 0.0343 (7) ... See full document

6

Crystal structure of 2 (4 methyl­piperazin 1 yl)quinoline 3 carbaldehyde

Crystal structure of 2 (4 methyl­piperazin 1 yl)quinoline 3 carbaldehyde

... N1 0.0470 (7) 0.0482 (8) 0.0386 (7) −0.0039 (6) 0.0102 (6) 0.0002 (5) N2 0.0423 (7) 0.0538 (9) 0.0381 (7) −0.0054 (6) 0.0119 (5) −0.0038 (6) N3 0.0541 (8) 0.0505 (9) 0.0400 (7) −0.0114 ... See full document

7

(2E) 3 (2 Chloro 8 methyl­quinolin 3 yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one

(2E) 3 (2 Chloro 8 methyl­quinolin 3 yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one

... In the crystal packing, π—π interactions between centrosymmetrically related N2-pyridyl rings [centroid···centroid distance = 3.4947 (7) Å and symmetry operation: -x, 1 - y, 1 - z] combine with ... See full document

10

(2 Methyl 1 phenyl­sulfonyl 1H indol 3 yl)methanol

(2 Methyl 1 phenyl­sulfonyl 1H indol 3 yl)methanol

... Benzenesulfonyl chloride (7.75 ml, 43.9 mmol), 60% NaOH solution (60 g in 100 ml), along with tetrabutylammonium hydrogensulfate (1.5 g) were added to the solution of 2-methylindole-3-carboxaldehyde (8.0 g, ... See full document

7

Methyl 3 (2 oxobenzo­thia­zolin 3 yl)­propanoate

Methyl 3 (2 oxobenzo­thia­zolin 3 yl)­propanoate

... for 3-methyl-2(3H)-benzo- thiazolone (Rudd & Barany, 1984), ...for 3-methyl-2(3H)-benzothiazolone (Rudd & Barany, 1984), ... See full document

7

3 (2 Methyl 1,3 benzo­thia­zol 3 ium 3 yl)propane 1 sulfonate monohydrate

3 (2 Methyl 1,3 benzo­thia­zol 3 ium 3 yl)propane 1 sulfonate monohydrate

... C1 0.0260 (8) 0.0278 (8) 0.0252 (8) 0.0026 (7) 0.0053 (6) −0.0020 (6) C2 0.0262 (8) 0.0304 (8) 0.0289 (8) 0.0044 (7) 0.0058 (7) −0.0041 (7) C3 0.0282 (8) 0.0283 (8) 0.0295 (8) 0.0087 ... See full document

8

1 (3 Methyl 3 phenyl­cyclo­butyl) 2 (piperidin 1 yl)ethanone oxime

1 (3 Methyl 3 phenyl­cyclo­butyl) 2 (piperidin 1 yl)ethanone oxime

... Although close to being planar, the cyclobutane ring in (I) is more puckered than in (II) and (III), because of the steric hindrance of the substituents. The C4/C1/C2 plane forms a dihedral angle of 25.0 (4)° [25.7 (4)°] ... See full document

14

(2E) 3 (6 Chloro 2 meth­­oxy­quinolin 3 yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one acetone monosolvate

(2E) 3 (6 Chloro 2 meth­­oxy­quinolin 3 yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one acetone monosolvate

... C26 0.0219 (9) 0.0199 (10) 0.0268 (10) −0.0022 (7) 0.0039 (7) −0.0002 (8) C27 0.0169 (9) 0.0179 (9) 0.0261 (9) −0.0012 (7) 0.0028 (7) −0.0021 (7) C28 0.0175 (9) 0.0208 (9) 0.0255 (9) ... See full document

10

(2E) 3 (2 Chloro­benzo[h]quinolin 3 yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one

(2E) 3 (2 Chloro­benzo[h]quinolin 3 yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one

... C10 0.0349 (8) 0.0256 (7) 0.0288 (7) −0.0013 (6) −0.0074 (6) 0.0041 (5) C11 0.0222 (6) 0.0186 (6) 0.0209 (6) −0.0011 (5) −0.0019 (5) −0.0019 (5) C12 0.0224 (6) 0.0242 (6) 0.0237 (6) −0.0028 (5) −0.0021 (5) ... See full document

10

Methyl (2Z) 2 [(2 formyl 3 methyl 1H indol 1 yl)meth­yl] 3 (4 meth­­oxy­phen­yl)prop 2 enoate

Methyl (2Z) 2 [(2 formyl 3 methyl 1H indol 1 yl)meth­yl] 3 (4 meth­­oxy­phen­yl)prop 2 enoate

... The indole ring system is planar with a maximum deviation of 0.019 (1) Å for atom C3. The carbaldehyde group atoms (C22 and O1) and methyl atom (C9) deviate 0.111 (1), 0.088 (2) and 0.065 ... See full document

12

3 (4 Chloro­phen­yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one

3 (4 Chloro­phen­yl) 1 (2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one

... Quinoline derivatives are very important compounds because of their wide occurrence in natural products and biologically active compounds (Markees et al. , 1970; Campbell et al. , 1998). Additionally, chalcone ... See full document

8

Iso­propyl 2 (5 methyl 3 methyl­sulfinyl 1 benzo­furan 2 yl)acetate

Iso­propyl 2 (5 methyl 3 methyl­sulfinyl 1 benzo­furan 2 yl)acetate

... 77% 3-chloroperoxybenzoic acid (471 mg, ...isopropyl 2-(5- methyl-3-methylsulfanyl-1-benzofuran-2-yl)acetate (556 mg, ...for 3 h at room temperature, the mixture ... See full document

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3 (2 Methyl 3 methyl­sulfanyl 1 benzo­furan 5 yl)propanoic acid

3 (2 Methyl 3 methyl­sulfanyl 1 benzo­furan 5 yl)propanoic acid

... C2 0.0202 (9) 0.0255 (9) 0.0253 (9) 0.0076 (7) 0.0058 (7) 0.0130 (7) C3 0.0210 (9) 0.0223 (9) 0.0262 (9) 0.0062 (7) 0.0037 (7) 0.0107 (7) C4 0.0196 (9) 0.0276 (9) 0.0239 (9) ... See full document

6

Methyl 2 (5 chloro 3 methyl­sulfinyl 1 benzo­furan 2 yl)acetate

Methyl 2 (5 chloro 3 methyl­sulfinyl 1 benzo­furan 2 yl)acetate

... Cl 0.0594 (4) 0.0550 (3) 0.1360 (6) −0.0274 (3) −0.0214 (4) −0.0029 (4) S 0.0541 (3) 0.0652 (3) 0.0390 (3) −0.0251 (2) −0.0121 (2) −0.0044 (2) O1 0.0496 (7) ... See full document

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(2E) 3 (2 Chloro 7 methyl­quinolin 3 yl) 1 (6 chloro 2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one ethanol monosolvate

(2E) 3 (2 Chloro 7 methyl­quinolin 3 yl) 1 (6 chloro 2 methyl 4 phenyl­quinolin 3 yl)prop 2 en 1 one ethanol monosolvate

... The terminal quinolinyl residues in (I), Fig. 1, are inclined to each other forming a dihedral angle of 46.41 (4)°. The bridge between these, i.e. the prop-2-en-1-one residue, is planar as seen in ... See full document

12

(2E) 1 (2 Methyl 4 phenyl­quinolin 3 yl) 3 (3 methyl­thio­phen 2 yl)prop 2 en 1 one

(2E) 1 (2 Methyl 4 phenyl­quinolin 3 yl) 3 (3 methyl­thio­phen 2 yl)prop 2 en 1 one

... In addition to their being valuable intermediates in organic synthesis (Prasath & Bhavana, 2012; Joshi et al., 2011), quinoline and heterocyclic analogues, such as chalcones, exhibit a variety of biological ... See full document

11

3 Ethyl­sulfinyl 2 (3 fluoro­phen­yl) 5 iodo 7 methyl 1 benzo­furan

3 Ethyl­sulfinyl 2 (3 fluoro­phen­yl) 5 iodo 7 methyl 1 benzo­furan

... the 3-fluorophenyl ring is disordered over two positions with site occupancy factors, from refinement of ...B). ... See full document

7

(E) Methyl 3 (2 methyl 1 phenyl­sulfonyl 1H indol 3 yl)but 2 enoate

(E) Methyl 3 (2 methyl 1 phenyl­sulfonyl 1H indol 3 yl)but 2 enoate

... (Beddoes et al., 1986). The sulfonyl bound phenyl ring is oriented almost perpendicular to the indole ring system as can be seen from the dihedral angle of 86.75 (7)°. The ester group attached to the indole ring ... See full document

9

2 Amino 7 meth­oxy 3 (1 methyl 1H benzimidazol 2 yl)­chromenium perchlorate

2 Amino 7 meth­oxy 3 (1 methyl 1H benzimidazol 2 yl)­chromenium perchlorate

... The ionic crystals of (I) are composed of chromenium cations and perchlorate anions (Fig. 1). In the cation, two planar fragments (r.m.s. deviations of 0.016 and 0.007 AÊ for the coumarin and benzimidazole ... See full document

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