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[PDF] Top 20 4 Meth­­oxy N (pyridin 4 ylmeth­yl) 3 (tri­fluoro­meth­yl)benzamide monohydrate

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4 Meth­­oxy N (pyridin 4 ylmeth­yl) 3 (tri­fluoro­meth­yl)benzamide monohydrate

4 Meth­­oxy N (pyridin 4 ylmeth­yl) 3 (tri­fluoro­meth­yl)benzamide monohydrate

... the N—H bond in the chain is anti with respect to the C=O ...The benzamide molecules are also linked to one another forming C(6) chains (Bernstein et ... See full document

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{rac 5 [Meth oxy(phen yl)meth yl] 10,20 diphenyl porphyrinato}nickel(II)

{rac 5 [Meth oxy(phen yl)meth yl] 10,20 diphenyl porphyrinato}nickel(II)

... Grignard reaction of the respective formylporphyrin to yield {5-[hydroxy(phenyl)methyl]-10,20-diphenylporphyrinato}- nickel(II), followed by crystallization from methylene chloride/methanol. The molecule exhibits a ... See full document

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Crystal structure of N [(morpholin 4 yl)(thio­phen 2 yl)meth­yl]benzamide

Crystal structure of N [(morpholin 4 yl)(thio­phen 2 yl)meth­yl]benzamide

... (Muruganandam et al., 2009; Khan et al., 2012). The morpholine ring adopts a chair conformation. The thiophene ring makes a dihedral angle of 63.54 (14) ° with the mean plane of the four C atoms (maximum deviation 0.010 ... See full document

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N [(1 Benzoyl­piperidin 4 yl)meth­yl]benzamide

N [(1 Benzoyl­piperidin 4 yl)meth­yl]benzamide

... The procedure (Prathebha et al., 2013, Venkatraj et al., 2008) adopted in the synthesis of the typical diamide is as follows: In a 250 mL round-bottomed flask 4-methyl piperidine (0.01 mol) was taken in, to which ... See full document

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Crystal structure of 4 methyl N [2 (piperidin 1 yl)eth­yl]benzamide monohydrate

Crystal structure of 4 methyl N [2 (piperidin 1 yl)eth­yl]benzamide monohydrate

... between the planes of the piperidine and benzene rings is 31.63 (1) . The piperidine ring adopts a chair conformation. The water solvent molecule is involved in interspecies O— H O, O—H N, N—H O and weak ... See full document

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Crystal structure of 4 chloro N [2 (piperidin 1 yl)eth­yl]benzamide monohydrate

Crystal structure of 4 chloro N [2 (piperidin 1 yl)eth­yl]benzamide monohydrate

... Data collection: APEX2 (Bruker, 2004); cell refinement: SAINT (Bruker, 2004); data reduction: XPREP in SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 ... See full document

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2,2 Di­methyl N [3 (3,4,5 tri­meth­oxy­benzo­yl)­pyridin 4 yl]propanamide

2,2 Di­methyl N [3 (3,4,5 tri­meth­oxy­benzo­yl)­pyridin 4 yl]propanamide

... of 3.477 (2) A ˚ . The virtual structure of (III) was first built with the modelling program SYBYL (Tripos, 2006) without any pre-optimization and subsequently minimized by the use of force field MMFF94s (Halgren, 1999) ... See full document

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[4 (4 Meth­­oxy­phen­yl) 2 (pyridin 3 yl) 1,3 thia­zol 5 yl][4 (tri­fluoro­meth­yl)phen­yl]methanone

[4 (4 Meth­­oxy­phen­yl) 2 (pyridin 3 yl) 1,3 thia­zol 5 yl][4 (tri­fluoro­meth­yl)phen­yl]methanone

... In the title molecule, Fig. 1, the thiazole ring makes dihedral angles of 12.98 (13)°, 49.30 (11) ° and 49.83 (12) ° with pyridine ring, the methoxy phenyl ring and the trifluoromethyl phenyl ring, respectively. The ... See full document

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4 [3 (4 Methyl­piperidin 1 yl)propan­amido]­benzene­sulfonamide monohydrate

4 [3 (4 Methyl­piperidin 1 yl)propan­amido]­benzene­sulfonamide monohydrate

... C7—C8—C9 and C7—C8—C9—N3 torsion angles are -0.0 (6), 2.5 (5), -178.2 (3) and 174.1 (3)°, respectively. The bond lengths and bond angles are within the normal range and are comparable to those previously ... See full document

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Crystal structure of 4 methyl N [(4 methyl­pyridin 2 yl)carbamo­thioyl]­benzamide

Crystal structure of 4 methyl N [(4 methyl­pyridin 2 yl)carbamo­thioyl]­benzamide

... The title compound was prepared according to a slight modification of the method described by Hassan et al. (2008b). p-Benzoyl chloride (13 mmol) was added dropwise to a stirred acetone solution (30 ml) of ammonium ... See full document

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Synthesis and Characterization of N-(3-(8-Bromoimidazo[1, 2-a] pyridin-2- yl)-4-Fluorophenyl)Benzamide Derivatives

Synthesis and Characterization of N-(3-(8-Bromoimidazo[1, 2-a] pyridin-2- yl)-4-Fluorophenyl)Benzamide Derivatives

... 126.8, 119.4, 116.4 , 114.7, 113.2, 112.7, 109.8, 105.8; LC-MS: [m+1] 553.0 . (Fig-17 to 20) 2-bromo-N-(3-(8-bromoimidazo[1,2-a]pyridin-2-yl)-4-fluorophenyl)-3-methylbenzamide ... See full document

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Crystal structure of 4 chloro N {[1 (4 chloro­benzo­yl)piperidin 4 yl]meth­yl}benzamide monohydrate

Crystal structure of 4 chloro N {[1 (4 chloro­benzo­yl)piperidin 4 yl]meth­yl}benzamide monohydrate

... Piperidine and its derivatives have a high impact factor on the medical field due to their wide range of pharmacological activities. The piperidone molecule is also an important pharmacophore due to its broad-spectrum of ... See full document

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Mol­ecular structure, DFT studies and UV–Vis absorption of two new linear fused ring chalcones: (E) 1 (anthracen 9 yl) 3 (2 meth­­oxy­phen­yl)prop 2 en 1 one and (E) 1 (anthracen 9 yl) 3 (3 fluoro 4 meth­­oxy­phen­yl)prop 2 en 1 one

Mol­ecular structure, DFT studies and UV–Vis absorption of two new linear fused ring chalcones: (E) 1 (anthracen 9 yl) 3 (2 meth­­oxy­phen­yl)prop 2 en 1 one and (E) 1 (anthracen 9 yl) 3 (3 fluoro 4 meth­­oxy­phen­yl)prop 2 en 1 one

... Experimental electronic absorption spectra of (I) and (II) have been measured and compared to the ground state (HOMO) and excited state (LUMO) molecular orbital ener- gies, calculated using time-dependent DFT B3LYP/6- ... See full document

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N (1,10 Phenanthrolin 5 yl) 4 (2 pyridyl)­benzamide monohydrate

N (1,10 Phenanthrolin 5 yl) 4 (2 pyridyl)­benzamide monohydrate

... The molecular structure of (I) is shown in Fig. 1. The water is hydrogen bonded to one of the nitrogen atoms of the phen moiety (Table 1). The phen moiety is slightly deformed from an ideal planar geometry, presumably ... See full document

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(E) 4 Meth­­oxy N′ [(pyridin 4 yl)methyl­­idene]benzohydrazide monohydrate

(E) 4 Meth­­oxy N′ [(pyridin 4 yl)methyl­­idene]benzohydrazide monohydrate

... A mixture of 2 mmol of 4-methoxybenzohydrazide (0.332 g), 2 mmol isonicotinaldehyde (0.214 g) and catalytical amount of acetic acid was refluxed in methanol (20 ml) for 3 h. The progress of reaction was ... See full document

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4 Methyl N [2 (pyridin 2 yl)ethyl­carbamo­thio­yl]benzamide

4 Methyl N [2 (pyridin 2 yl)ethyl­carbamo­thio­yl]benzamide

... pyridine N-atom (Table 1): a hydrogen bond with O2 (N2—H···O2) and an interaction with N3 (N2—H···N3), giving cyclic motifs [graph sets S6 (Bernstein et ... See full document

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Crystal structures of N [(4 phenyl­thia­zol 2 yl)carbamo­thio­yl]benzamide and N {[4 (4 bromo­phen­yl)thia­zol 2 yl]carbamo­thio­yl}benzamide from synchrotron X ray diffraction

Crystal structures of N [(4 phenyl­thia­zol 2 yl)carbamo­thio­yl]benzamide and N {[4 (4 bromo­phen­yl)thia­zol 2 yl]carbamo­thio­yl}benzamide from synchrotron X ray diffraction

... Unlike (I), compound (II) comprises three almost planar fragments. The first is the central N-(thiazol-2-ylcarbamothioyl)amide (r.m.s. deviation = 0.084 A ˚ ), and the two others comprise the bromophenyl and ... See full document

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Crystal structure of bis­­[2 tert but­­oxy 6 fluoro 3 (pyridin 2 yl κN)pyridin 4 yl κC4](pentane 2,4 dionato κ2O,O′)iridium(III)

Crystal structure of bis­­[2 tert but­­oxy 6 fluoro 3 (pyridin 2 yl κN)pyridin 4 yl κC4](pentane 2,4 dionato κ2O,O′)iridium(III)

... View of the molecular structure of the title compound, with the atom- numbering scheme. Displacement ellipsoids are drawn at the 50% probability level; dashed lines represent intramolecular C—H O and C—H N ... See full document

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Crystal structure of [2,6 di­fluoro 3 (pyridin 2 yl κN)pyridin 4 yl κC4](pentane 2,4 dionato κ2O,O′)platinum(II)

Crystal structure of [2,6 di­fluoro 3 (pyridin 2 yl κN)pyridin 4 yl κC4](pentane 2,4 dionato κ2O,O′)platinum(II)

... 1.951 (4) A ˚ is shorter than the Pt—N bond length of 1.995 (4) A ˚ due to the more electronegative fluorine substit- uent on the C-bound pyridine ring. The Pt—C, Pt—N and Pt— O bond lengths ... See full document

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3 [2 (N,N Di­ethyl­amino)­glyoxyloyl] 1H indol 4 yl acetate monohydrate

3 [2 (N,N Di­ethyl­amino)­glyoxyloyl] 1H indol 4 yl acetate monohydrate

... of 3-[2-(diethylamino)ethyl]-4- indolol (4-HO-DET), a compound belonging to the 3-(2- aminoethyl)indole structural class of psychoactive drugs (Shulgin & Shulgin, ...1997). 4-HO-DET ... See full document

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