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ISSN 2229 – 5046

CONSTRUCTION OF SECOND ORDER ROTATABLE DESIGNS

USING BALANCED TERNARY DESIGNS

KANNA E

1

, AMEEN SAHEB SK

*2

AND BHATRA CHARYULU N. CH.

1

1

Department of Statistics,

University College of Science, Osmania University, Hyderbad-7. India.

2

School of Mathematics and Statistics,

University of Hyderabad, Hyderabad-500046, India.

(Received On: 11-04-18; Revised & Accepted On: 18-05-18)

ABSTRACT

T

he variance of estimated response of Second Order Response Surface Design Model satisfying the property that, at any given point in a design, it is a function of the distance from that point to the origin, specifically; it is a spherical or nearly spherical variance function, are called rotatable designs. This paper provides new series for the construction of Second Order Rotatable Design using Balanced Ternary Design.

Keywords: Balanced Incomplete Block Design, Balanced Ternary Design, Second Order Rotatable Designs,

1. INTRODUCTION

Let X1, X2, … , Xv are ‘v’ factors, each has ‘s’ levels for experimentation. Let D denote the design matrix of combination of the factor levels, given by

D = ( ( xu1, xu2, … , xuv) ) (1.1) where xui be the level of the ith factor in the uth factors combination (i=1, 2, ... v; u =1, 2 … N). Let Yu denote the response at the uth combination. The factor-response relationship is given by

E(Yu) = f (xu1, xu2, … , xuv) (1.2) is called the ‘Response Surface’. The design ‘D’ used for fitting the response surface models are termed as ‘Response Surface Design’. The functional form of the response surface to be fitted to the design is polynomial of degree k, may be linear, second order, third order etc. The second order response surface design model at the uth design point is

Yu = β0 +

=

v

1 i

βi xui +

=

v

1 i

βii xui2 +

<

v

j i

βij xuixuj + ε u = 1, 2, … N (1.3)

where, Yu is the response at the uth design point,

β= (β0, β1, β2, … βv, β11, β22, … β vv, βl2, … βv-1v)' be the vector of parameters

xu = (1, xu1, xu2, … xuv, x2u1, x2u2, … x2uv, xulxu2, … xuv-1xuv) be the uth row of the design matrix X, εu is the random error corresponding to Yu. Assume the random errors are independent follows N(0, σ

2 ).

The model (1.3) can be expressed in the matrix form as

Y = X β + ε (1.4) where, YNx1= [Y1 Y2 … YN] ' is the vector of responses, βk×1 is the vector of parameters and εN×1= [ ε1, ε2,... , εN ] ′ is the vector of random errors. XN×k is the design matrix,

X =

Nv 1 -Nv N3

N1 N2 N1 2 Nv 2

N2 2 N1 Nv N2

N1

2v 1 -2v 23

21 22 21 2 2v 2

22 2 21 2v 22

21

1v 1 -1v 13

11 12 11 2 1v 2

12 2 11 1v 12

11

x

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...

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1

Corresponding Author: Ameen Saheb Sk

*2

(2)

The least square estimate of the parameters and responses are

β

ˆ

= (X′X)-1X′Y and

Υ

ˆ

=

(X′X)-1X′Y and the variance of

estimated response is V (

Υ

ˆ

) = (X′X)-1σ2, where the moment matrix (X′X) is

=

= − = − = − = − = − = − = = − = = = = = = = − = = = = = = = − = = = = = = = − = = = = = = = − = = = = = = = = = = = = N 1 i 2 iv 2 1 iv N 1 i iv 1 iv i2 i1 N 1 i 3 iv 1 iv N 1 i iv 1 iv 2 i1 N 1 i 2 iv 1 iv N 1 i iv 1 iv i1 N 1 i iv 1 -iv N 1 i iv 1 iv i2 i1 N 1 i 2 i2 2 i1 N 1 i 2 iv i2 i1 N 1 i i2 3 i1 N 1 i iv i2 i1 N 1 i i2 2 i1 N 1 i i2 i1 N 1 i 3 iv 1 iv N 1 i 2 iv i2 i1 N 1 i 4 iv N 1 i 2 iv 2 i1 N 1 i 3 iv N 1 i 2 iv i1 N 1 i 2 iv N 1 i iv 1 iv 2 i1 N 1 i i2 3 i1 N 1 i 2 iv 2 i1 N 1 i 4 i1 N 1 i iv 2 i1 N 1 i 3 i1 N 1 i 2 i1 N 1 i 2 iv 1 iv N 1 i iv i2 i1 N 1 i 3 iv N 1 i iv 2 i1 N 1 i 2 iv N 1 i iv i1 N 1 i iv N 1 i iv 1 iv i1 N 1 i i2 2 i1 N 1 i 2 iv i1 N 1 i 3 i1 N 1 i iv i1 N 1 i 2 i1 N 1 i il N 1 i iv 1 -iv N 1 i i2 i1 N 1 i 2 iv N 1 i 2 i1 N 1 i iv N 1 i il

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N

X

X'

The V(Ŷu) is not in a simplified form as the elements in moment matrix are in higher order, hence imposing the restrictions on the moment matrix that all odd power summations are zero, towards reaching to near orthogonality, i.e.

δ4 ul δ3 uk δ2 uj δ1

ui

x

x

x

x

= 0, where all the summations are over the design points u= 1, 2, …N and for distinct i, j, k, l = 1, 2, v. Let Σ x2ui= N λ2 ; Σ x

4

ui= CN λ4 ; Σx 2

ui x 2

uj= Nλ4 then the moment matrix will be in the form

N-1X′X =

[

]

+

I

λ

0

0

0

0

λ

J

1)I

(c

0

J

λ

0

0

J

λ

0

0

J

λ

0

1

4 4 2 2 2

and N(X′X)-1 =

              − − − + + + − − − − − 1 2 VxV 1 2 1 2 1 1 4 λ 0 0 0 0 Z 0 JΔ 2λ 0 0 I λ 0 0 1)JΔ 1)(c v (c 0 1)Δ v (c λ

where, ∆ = [ λ4 (c+v–1) – vλ22] > 0; Zv×v = k,k 2 2 4 2 2 2 4 v v, v

J

k

λ

1)

v

(c

λ

1)

1)(c

v

(c

λ

1)

v

1)(c

(c

λ

J

1)I

v

(c

+

+

+

+

+

Let

= v

i1

xui2 = ρ2 ; then

= v

i 1

xui4 = ρ4 – 2

< v j i 2 uj 2 ui

x

x

. The variance of estimated response at the uth design point is

V (Ŷu) = V (

β

ˆ

0) +ρ

2 V(

i

β

ˆ

) + [ρ4–2

< v j i 2 uj 2 ui

x

x

] V(

β

ˆ

ii) +

< v j i 2 uj 2 ui

x

x

V(

β

ˆ

ij) + 2 Cov(

β

ˆ

0,

β

ˆ

ii)ρ2

+ 2 Cov(

β

ˆ

ii,

β

ˆ

jj)

< v j i 2 uj 2 ui

x

x

(1.5)

where,

V (

β

ˆ

0) = [ λ4 (c+k–1)/ N∆] σ 2

]

V (

β

ˆ

i) = (1/ Nλ2) σ2

V (

β

ˆ

ij) = (1/ Nλ4) σ 2

Cov (

β

ˆ

0,

β

ˆ

ii) = [-λ2 / N∆] σ 2

V (

β

ˆ

ii) = [{λ4(c+k–2)–(k–1)λ22}/{Nλ4 (c–1) ∆}] σ2

(3)

V(Ŷu)=V(

β

ˆ

0) + [V(

β

ˆ

i) + 2Cov(

β

ˆ

0,

β

ˆ

ii)]ρ

2

+ V(

β

ˆ

ii)ρ4 + [V(

β

ˆ

ij)–2V(

β

ˆ

ii) + 2Cov(

β

ˆ

ii,

β

ˆ

jj)]

< v

j i

2 uj 2 ui

x

x

⇒V(Ŷu) =

{

}

<

+

+

 −

+

v

j i

2 uj 2 ui 2

4 2

2 2

2 2 2 4

4 2 2 2

x

x

σ

1)N

λ

(c

3)

(c

v

λ

Δ

ρ

λ

2

λ

Δ

ρ

1)

(c

λ

λ

Δ

N

Δ

σ

(1.6)

The condition [λ4(v+2) – vλ22] > 0 is a non-singularity condition necessary for the v+2Cv coefficients in the response function to be estimated. The condition can always be satisfied by mere addition of central points. The variance of the estimated response at any design point in the design is a function of ρ2, i.e. the distance from design point to the origin. Such a design is called as Second Order Rotatable Design. From (1.6), when c = 3, the variance of estimated response

can be expressed in the form of a function of ρ2 as V(Ŷu) = Aρ

4+ Bρ2

+ C (1.7)

where, A =

  

 

− −

1) (c

λ λ Δ

σ

4 2 2 2

; B =

  

  −

2 2 2 2

λ 2λ Δ NΔ

σ ; C =

[

2

]

2 2

Δ

σ + .

This paper provides new series for the construction of Second Order Rotatable Designs using Balanced Ternary Designs.

2. CONSTRUCTION OF NEW CLASS OF SORD

This section provides a new series for the construction Second Order Rotatable Design using Balanced Ternary Designs. The constructions are illustrated with suitable examples and presented.

Series 2.1: Second Order Rotatable Designs can be constructed using Balanced Ternary Designs provided by Tyagi and Rizwi (1979) are presented below

Step-1: Let N1 be the incidence matrix of a Balanced Incomplete Block Design with parameters v, b, r, k, λ (assume 9λ2≥ 4rλ(v-1) ) and let N2 = Iv, where Iv is the identity matrix of order ‘v’ and ‘p’ is a positive integer. The Balanced Ternary Designs are derived by adding the elements of jth row of N2 to those rows of N1, which contain unity in the jth column, constitute a Balanced Ternary Design with parameters V = v, B = vr, R = (k+1)r, K = k+1 and π = λ(k+2).

Step-2: Replace the elements 2 with α and 1 with β, then associate each block with an appropriate fraction of factorials

(say

2

k1) with levels ±1 such that no lower order interaction effects are confounded.

Step-3: Add n0 (n0 > 0) central design points (0, 0, … 0) to the resulting design, then total number design points in the

design are: N =

2

k1vr + n

0.

Step-4: The levels ‘α’ and ‘β’ can be obtained such that t = α2 / β2. Real roots for t can be obtained as t =

r

1) -(v 4r 9 3λ± λ2 λ

. Choose the value for β then obtain the value of α as α2 = tβ2. The resulting design

provides a v-dimensional Second Order Rotatable Design with five levels ( ±α, ±β, 0).

Theorem 2.1: A Second Order Rotatable Design exists with five levels (±α, ±β, 0) using a Balanced Ternary Design with parameters V = v, B = vr , R = (k+1)r, K = k+1 and π = λ(k+2) satisfying the condition 9λ2≥ 4rλ(v-1).

Proof: Let NBXV be the incidence matrix of a balanced Ternary Design with parameters V = v, B = vr, R = (k+1)r,

K = k+1 and π = λ(k+2). Each column of NBxV contains ‘r’ times 2, λ(v-1) times 1 and (r-λ)(v-1) times 0. Every pair of

columns contains the pairs (1, 2) or (2, 1)’s 2λ times and (2, 2) and (1, 1) pairs zero times. Replace the elements 1 with

β and 2 with α. Associate each block with an appropriate fraction of factorials (say

2

k1) for v factors, with levels ±1.

After augmenting n0 central points, the resulting design has N =

2

1 k

v(b-r) + n0 design points. Then from the rotatable

condition

=

N

1 u

4 ui

x

= 3.

=

N

1 u

2 uj 2 ui

x

x

, we can obtain

2

k1 ( rα4 + λ(v-1)β4 ) = 3.

2

k1(2λα2 β2 ) (2.1)

⇒ rα4 + λ(v-1) β4 - 6 λα2 β2 = 0 (2.2)

Let t = α2/β2, then (2.2) can be expressed in the quadratic form as

(4)

Example 2.1: Let N1 be the incidence matrix of a Balanced Incomplete Block Design with parameters v = 4, b = 6,

r = 3, k = 2 and λ = 1, and N2 = Iv. The resulting Balanced Ternary Design is with parameters V = 4, B = 12, R = 9, K = 3 and π = 4. The Second Order Rotatable Design with four factors is presented in Table 2.1.

Table-2.1: Construction of Second Order Rotatable Design (SORD)

N1 N2 N SORD

       

 

       

 

1 1 0 0

1 0 1 0

0 1 1 0

1 0 0 1

0 1 0 1

0 0 1 1

1

0

0

0

0

1

0

0

0

0

1

0

0

0

0

1

2

1

0

0

2

0

1

0

2

0

0

1

1

2

0

0

0

2

1

0

0

2

0

1

1

0

2

0

0

1

2

0

0

0

2

1

1

0

0

2

0

1

0

2

0

0

1

2

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

α

β

α

β

α

β

β

α

α

β

α

β

β

α

β

α

α

β

β

α

β

α

β

α

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

The real solution for‘t’ is 1. Select value for β arbitrarily and accordingly α can be evaluated.

Series 2.2: A series of Second Order Rotatable Designs can be constructed using Balanced Ternary Designs of Tyagi and Rizwi (1979) is like as follows.

Step-1: Let N1 be the incidence matrix of a Balanced Incomplete Block Design with parameters v, b, r, k, λ and let N2 = 2Iv, where Iv is the identity matrix of order ‘v’. The Balanced Ternary Designs are derived by adding the elements of jth row of N2 those rows of N1 which contain zero in the jth column, then v(b-r) blocks so formed constitute a Balanced Ternary Design with parameters V = v, B = v(b-r), R = (k+2) (b-r), K = k+2 and

π = (r-λ)(4+k-1).

Step-2: Replace the elements 2 with α and 1 with β, then associate each block with an appropriate fraction of factorials (say

2

k1) with levels ±1 such that no lower order interaction effects are confounded.

Step-3: Add n0 (n0 > 0) central design points (0, 0, … 0) to the resulting design, then total number design points in the design is n =

2

k1v(b-r) + n

0.

Step-4: The levels ‘α’ and ‘β’ can be obtained such that t = α2 / β2. Real roots for t can be obtained as t =

r) -2(b

] k) -(v -) -1)(r -r)[(v 4(b ) 2 -9(b ) 2

-3(b λ ± λ2− − λ λ . Choose the value for β then obtain the value of α as α2 = tβ2. The

resulting design provides a v-dimensional Second Order Rotatable Design with five levels (±α, ±β, 0 ).

Theorem 2.2: A Second Order Rotatable Design exists with five levels (±α, ±β, 0) using a Balanced Ternary Design with parameters V = v, B = v(b-r), R = (k+2) (b-r), K = k+2 and π = (r-λ)(4+k-1).

Proof: Let NBXV be the incidence matrix of a balanced Ternary Design with parameters V = v, B = v(b-r), R = (k+2) (b-r), K = k+2 and π = (r-λ)(4+k-1). Each column of NBxV contains 2’s and 1’s ‘b-r-λ’ and ‘r-λ+λ(v-k)’ times. Every

pair of columns contains the pairs (1,2) and (2,1) occurs ‘r-λ’ and ‘b-r-λ’ times. Replace the elements 1 with β and 2 with α. Associate each block with an appropriate fraction of factorials ( say

2

k1) for v factors, with levels ±1. After

augmenting n0 central points, the resulting design has N=

2

1 k

v(b-r)+n0 design points. Then from the rotatable condition

=

N

1 u

4 ui

x

= 3.

=

N

1 u

2 uj 2 ui

x

x

, we can obtain

1

2

k {(b-r) α4 + (r-λ)(v-1) β4 } = 3.

2

k1{λ(v-k) β4 + (b-2λ)α2 β2} (2.4)

From the rotatable condition, we obtain

(5)

Let t = α2/β2, then (2.5) can be expressed in the quadratic form as

(b-r) t2 – 3 (b-2λ) t + [(v-1) (r-λ) - λ(v-k)] = 0 (2.6)

The roots of the quadratic equation are t =

r) -2(b

k)] -(v -) -1)(r -r).[(v 4(b ) 2 -9(b ) 2

-3(b λ ± λ 2− − λ λ .

The roots are real if the discriminant in nonnegative. Choose any real value for ‘β’ then the real value for ‘α’ can be obtained as α2 = tβ2. The resulting design ‘D’ provides a v-dimensional Second Order Rotatable Design in five levels.

Example 2.2: Let N1 be the incidence matrix of a Balanced Incomplete Block Design with parameters v = 4, b = 6, r = 3, k = 2 and λ = 1, and N2 = 2Iv. The resulting Balanced Ternary Design is with parameters V = 4, B = 12, R = 12, K = 4 and

π

= 10. The Second Order Rotatable Design with four factors is presented in. Table 2.2

Table-2.2: Construction of Second Order Rotatable Design (SORD)

N1 N2 N SORD

1

1

0

0

1

0

1

0

0

1

1

0

1

0

0

1

0

1

0

1

0

0

1

1

2

0

0

0

0

2

0

0

0

0

2

0

0

0

0

2

2

1

1

0

2

1

0

1

2

0

1

1

1

2

1

0

1

2

0

1

0

2

1

1

1

1

2

0

1

0

2

1

0

1

2

1

1

1

0

2

1

0

1

2

0

1

1

2

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

±

α

β

β

α

β

β

α

β

β

β

α

β

β

α

β

α

β

β

β

β

α

β

α

β

β

α

β

β

β

α

β

β

α

β

β

α

0

0

0

0

0

0

0

0

0

0

0

0

The real solution for ‘t’ is 3.63. Select value for β arbitrarily and accordingly α can be evaluated.

ACKNOWLEDGEMENT

The authors are thankful to the referees for improving the version of manuscript. The first author is also thankful to the UGC for providing financial assistance in the form of Fellowship under BSR-RFSMS.

REFERENCES

1. Bhatra Charyulu, N. Ch. (2006): “A method for the construction of SORD”, Bulletin of Pure and Applied Science, Math & Stat, Vol.25E (1), pp 205-208.

2. Box, G. E. P., and Draper, N. R. (1959): “A basis for the selection of a response surface design”, Journal of American Statistical Association, 54, pp 622-1439.

3. Das, M. N., and Narasimham, V. L. (1962): “Construction of rotatable designs through balanced incomplete block designs”, Annals of Mathematical Statistics, 33(4), pp 1421-1439.

4. Tyagi, B.N. and Rizwi S. K.H. (1979): “A note on construction of balanced ernary designs”, Journal of Indian Society for Agricultural Statistics, Vol. 31, pp 121-125.

Source of support: UGC, India., Conflict of interest: None Declared.

References

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