1.3 to 2.5 V
5 Isopropyl 2 methyl 3 phenylsulfonyl 1 benzofuran
... of 5-isopropyl-2- methyl-3-phenylsulfanyl-1-benzofuran (282 mg, ...acetate, 2:1 v/v) to afford the title compound as a colorless solid [yield 81%, ...acetate, ...
8
5 Cyclohexyl 3 (3 fluorophenylsulfonyl) 2 methyl 1 benzofuran
... 77% 3-chloroperoxybenzoic acid (515 mg, ...of 5-cyclo- hexyl-3-(3-fluorophenylsulfanyl)-2-methyl-1-benzofuran (374 mg, ...4:1 v/v) to afford the title ...
9
5 Fluoro 2 methyl 3 (3 methylphenylsulfonyl) 1 benzofuran
... of 5-fluoro-2- methyl-3-(3-methylphenylsulfanyl)-1-benzofuran (245 mg, ...4:1 v/v) to afford the title compound as a colorless solid [yield 71%, ...acetate, ...
8
5 Chloro 3 ethylsulfinyl 2 (3 fluorophenyl) 1 benzofuran
... of 5-chloro-3- ethylsulfanyl-2-(3-fluorophenyl)-1-benzofuran (337 mg, ...acetate, 2:1 v/v) to afford the title compound as a colorless solid [yield 67%, ...
10
5 Ethyl 3 (3 fluorophenylsulfonyl) 2 methyl 1 benzofuran
... 77% 3-Chloroperoxybenzoic acid (560 mg, ...of 5-ethyl-3-(3- fluorophenylsulfanyl)-2-methyl-1-benzofuran (320 mg, ...4:1 v/v) to afford the title compound as ...
9
5 Cyclohexyl 2 (2 fluorophenyl) 3 methylsulfinyl 1 benzofuran
... of 5-cyclo- hexyl-2-(2-fluorophenyl)-3-methylsulfanyl-1-benzofuran (271 mg, ...for 5 h, the mixture was washed with saturated sodium bicarbonate solution and the organic layer ...
8
5 Cyclohexyl 2 methyl 3 (3 methylphenylsulfonyl) 1 benzofuran
... of 5-cyclo- hexyl-2-methyl-3-(3-methylphenylsulfanyl)-1-benzofuran (302 mg, ...4:1 v/v) to afford the title compound as a colorless solid [yield 73%, ...
9
2 Methyl 3 phenylsulfonyl 5 propyl 1 benzofuran
... 77% 3-Chloroperoxybenzoic acid (471 mg, ...of 2-methyl-3- phenylsulfanyl-5-propyl-1-benzofuran (282 mg, ...acetate, 2:1 v/v) to afford the title compound as ...
8
5 Cyclohexyl 2 methyl 3 (3 methylphenylsulfinyl) 1 benzofuran
... of 5-cyclo- hexyl-2-methyl-3-(3-methylphenylsulfanyl)-1-benzofuran (302 mg, ...acetate, 2:1 v/v) to afford the title compound as a colorless solid [yield ...
9
5 Bromo 2 methyl 3 (3 methylphenylsulfinyl) 1 benzofuran
... of 5-bromo-2- methyl-3-(3-methylphenylsulfanyl)-1-benzofuran (300 mg, ...acetate, 2:1 v/v) to afford the title compound as a colorless solid [Yield 78%, ...
8
5 (p Tolylsulfonyl) 3 oxa 5 azatricyclo[5 2 1 04,8]decane
... crude product was purified by flash column chromatography (silica gel; hexane–EtOAc 1:5 v/v) to give 55.6 mg (58%) of the title compound, which was recrystallized from EtOH for X-ray analysis. ...
7
3 Ethylsulfinyl 2 (3 fluorophenyl) 5 phenyl 1 benzofuran
... of 3-ethyl- sulfanyl-2-(3-fluorophenyl)-5-phenyl-1-benzofuran (278 mg, ...acetate, 2:1 v/v) to afford the title compound as a colorless solid [yield 62%, ...
9
5 Chloro 2 methyl 3 phenylsulfonyl 1 benzofuran
... 77% 3-chloroperoxybenzoic acid (471 mg, ...of 5-chloro-2- methyl-3-phenylsulfanyl-1-benzofuran (275 mg, ...(hexane–ethylacetate, 2:1 v/v) to afford the I as ...
10
5 Cyclohexyl 3 ethylsulfinyl 2 (3 fluorophenyl) 1 benzofuran
... of 5-cyclo- hexyl-3-ethylsulfanyl-2-(3-fluorophenyl)-1-benzofuran (283 mg, ...acetate, 2:1 v/v) to afford the title compound as a colourless solid [yield ...
8
1 [2 Oxo 1′ phenyl 2′,3′,5′,6′,7′,7a' hexahydroindoline 3 spiro 3′ 1′H pyrrolizin 2′ yl] 3 phenylprop 2 en 1 one
... A solution of (1E,6E)-4-benzylidene-1,7-diphenylhepta-1,6-diene-3,5-dione (1 mmol), isatin (1 mmol) and L-proline (1 mmol) in aqueous methanol (20 ml) was refluxed until the disappearance of starting ...
11
tert Butyl 3 oxo 2 oxa 5 azabicyclo[2 2 1]heptane 5 carboxylate
... O2 0.0234 (14) 0.0253 (16) 0.0352 (16) 0.0018 (13) 0.0050 (12) −0.0054 (13) O3 0.0253 (15) 0.0189 (14) 0.0349 (16) −0.0018 (13) 0.0067 (12) 0.0007 (13) O4 0.0344 (17) 0.0263 (16) 0.0359 (16) −0.0089 (14) 0.0091 (13) ...
6
Ethyl 2 [5 (4 fluorophenyl)pyridin 3 yl] 1 [3 (2 oxopyrrolidin 1 yl)propyl] 1H benzimidazole 5 carboxylate
... In the title compound (Fig. 1), the benzimidazole ring (N1/N2/C1–C7) is planar with a maximum deviation of 0.028 (1) Å for atom N1. It makes dihedral angles of 47.69 (5) and 60.31 (5)°, ...
12
3 (5 Methyl 2 furyl) 1 (p tolyl) 2 propen 1 one
... Data collection: SMART Bruker, 1997; cell refinement: SAINT Bruker, 1997; data reduction: SAINT; programs used to solve structure: SHELXS97 Sheldrick, 2008; programs used to refine struc[r] ...
5
3 (2 Bromophenylsulfonyl) 5 cyclohexyl 2 methyl 1 benzofuran
... 3-Chloroperoxybenzoic acid (77%, 426 mg, 1.9 mmol) was added in small portions to a stirred solution of 3-(2-bromo- phenylsulfanyl)-5-cyclohexyl-2-methyl-1-benzofuran (361 mg, ...
9
5 Cyclohexyl 3 (2 fluorophenylsulfonyl) 2 methyl 1 benzofuran
... C17 0.0289 (7) 0.0324 (7) 0.0306 (7) 0.0136 (6) −0.0001 (6) 0.0043 (6) C18 0.0265 (7) 0.0330 (8) 0.0466 (9) 0.0093 (6) 0.0032 (7) 0.0055 (7) C19 0.0366 (8) 0.0283 (7) 0.0439 (9) 0.0107 (6) 0.0135 (7) 0.0076 (7) C20 ...
9