methyl 3
3 Methyl 3 pyrazolin 5 one
... In the course of our research on nitrogen heterocycles, we recently needed to prepare several pyrazolin-5-one compounds. Synthetic considerations made 3-methyl-3-pyra- zolin-5-one, (I), and ...
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Methyl 3 ferrocenylpropanoate1
... of methyl 3-ferrocenylpropanoate, (I), forms part of wider research on differently substituted ferrocene compounds, their synthesis, stereochemistry and structural analysis (Zoric et ...
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Methyl 3 (2 oxobenzothiazolin 3 yl)propanoate
... An ORTEPIII (Farrugia, 1997) view of (I) and a packing diagram are shown in Figs. 1 and 2, respectively. The bicylic benzothiazole system of (I) is planar within 0.025 AÊ; the displacements of the carbonyl oxygen and the ...
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(Z) Methyl 3 (2,4 dichlorophenyl) 3 hydroxyacrylate
... C3 0.0384 (10) 0.0573 (13) 0.0350 (12) −0.0029 (10) 0.0103 (10) −0.0052 (10) C4 0.0450 (12) 0.0598 (15) 0.0441 (12) 0.0013 (11) 0.0218 (10) 0.0021 (11) C5 0.0355 (11) 0.0657 (15) 0.0541 (14) −0.0083 (10) 0.0130 (11) ...
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(E) Methyl 3 (2 methyl 1 phenylsulfonyl 1H indol 3 yl)but 2 enoate
... Data collection: APEX2 (Bruker, 2004); cell refinement: SAINT (Bruker, 2004); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 ...
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Methyl 3 [(E) furfurylidene]dithiocarbazate
... of methyl dithiocarbazate and furfural in an ethanol solution under reflux, adopts an E configuration; the dithiocarbazate and furan units are located on opposite sides of the C N double ...
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4 Methyl 3 nitrobenzonitrile
... Data collection: CrystalClear Rigaku, 2005; cell refinement: CrystalClear; data reduction: CrystalClear; programs used to solve structure: SHELXS97 Sheldrick, 2008; programs used to refi[r] ...
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1 Benzoyl 3 methyl 3 pentylthiourea
... Two independent molecules, Figs 1 and 2, comprise the asymmetric unit of (I). While similar, the molecules differ in the relative orientations of the pentyl groups, Fig. 3, as quantified in the values of the ...
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1 Furoyl 3 methyl 3 phenylthiourea
... C1 0.068 (2) 0.0363 (18) 0.054 (2) −0.0138 (14) −0.0010 (16) −0.0080 (15) C14 0.077 (2) 0.052 (2) 0.039 (2) 0.0213 (16) 0.0060 (16) 0.0122 (16) C2 0.0294 (13) 0.0317 (16) 0.044 (2) 0.0030 (11) 0.0016 (12) 0.0027 (14) C15 ...
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Methyl 3 (4 {6 methyl 4 [3 (trifluoromethyl)phenyl]pyridazin 3 yloxy}phenyl)propanoate
... Data collection: CrystalClear Rigaku/MSC, 2005; cell refinement: CrystalClear; data reduction: CrystalClear; programs used to solve structure: SHELXS97 Sheldrick, 2008; programs used to [r] ...
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Methyl 3 (4 methylbenzylidene)dithiocarbazate
... Methyl dithiocarbazate was synthesized in the manner reported previously by Hu et al. (2001). Methyl dithiocarbazate (1.24 g, 10 mmol) and 4-methylbenzaldehyde (1.20 g, 10 mmol) were dissolved in ethanol ...
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Methyl 3 phenylisoxazole 5 carboxylate
... 3-Phenylisoxazole-5-carboxylic acid (10 mmol, 1.95 g; Wang et al., 2013) was dissolved in 100 ml dichloromethane, then thionyl chloride (12 mmol, 1.43 g) was added drop wise while the solution was stirred for 20 ...
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1 Methyl 3 phenylthiourea
... Data collection: SMART Bruker 1997; cell refinement: SAINT Bruker 1997; data reduction: SAINT; programs used to solve structure: SHELXS2013 Sheldrick, 2008; programs used to refine struc[r] ...
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Methyl 3 benzoyl 3 (6 methyl 2 pyridyl) 2 phenylacrylate
... Photo-induced oxygenation reactions of indolizine derivatives have been intensively investigated (Tian et al., 2001). In a continuation of this work, we report here the crystal structure of the title compound, (I), which ...
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1 (3 Chlorobenzoyl) 3 methyl 3 phenylthiourea
... Freshly prepared 3-chlorobenzoyl isothiocyanate (1.84 g, 10 mmol) was added to acetone (30 ml) and the mixture was stirred for 15 min. Neat N-methylaniline (1.07 g, 10 mmol) was then added and the resulting ...
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Methyl 4′ (3 bromophenyl) 3′ (2,5 dimethylbenzyl) 1′ methyl 2 oxospiro[indoline 3,2′ pyrrolidine] 3′ carboxylate
... (E)-methyl 3-(3-bromophenyl)-2-(2,5-dimethylbenzyl)acrylate (2 mmol), isatin (2 mmol) and sarcosine (2 mmol) in acetonitrile (8 ml) was refluxed for 12 ...
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Methyl 4 amino 3 methylbenzoate
... Methyl 3-methyl-4-aminobenzoate is important as an intermedicine to prepare telmisartan, an angiotensin II receptor blocker, on the development of obesity and related metabolic disorders in ...
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Novel particulate vaccine candidates recombinantly produced by pathogenic and nonpathogenic bacterial hosts : a thesis presented in partial fulfillment of the requirements for the degree of Doctor of Philosophy in Microbiology at Massey University, Manawatu, New Zealand
... methyl 3-hydroxybutanoate methyl 3-hydroxydecanoate methyl 3-hydroxydodecanoate methyl 3-hydroxyhexanoate methyl 3-hydroxyhexadecanote methyl 3-hydroxynonanoate methyl 3-hydroxyoctanoate[r] ...
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PRENYLATED BENZOIC ACID DERIVATIVES FROM PIPER SPECIES AS SOURCE OF ANTI INFECTIVE AGENTS
... acid methyl ester [methyl ester of 4, 5- dihydroxy-3-(3-methyl-2- butenoyl)benzoic acid] 12, 4, 5- dihydroxy-3-(3-methyl- 2-butenoyl)benzoic acid 13, methyl ...
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Methyl (E) 3 acetamido 4 methyl 2 pentenoate
... Data collection: SMART Siemens, 1995; cell re®nement: SMART; data reduction: SAINT Siemens, 1995 and SHELXTL Siemens, 1995; programs used to solve structure: SHELXS97 Sheldrick, 1997; pr[r] ...
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