Single Crystal Data for CC19
Sr3Al10SiO20 from single crystal data
... Experimental Single crystals were synthesized from well ground analytical SrCO 3 , Al(OH) 3 (both Merck) and SiO 2 (Fluka) by adding 10% by weight of H 3 BO 3 ...and crystal growth, samples were crushed, ...
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2,4,6 Triisopropylbenzenesulfonamide from single crystal data
... from single-crystal and powder data differ by small displacements of ...the single-crystal results of only 6 (1) , for the angle about C2Ð ...powder data yield longer SÐN and SÐC ...
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Reinvestigation of Na3P based on single crystal data
... the crystal structure and lattice parameters were reported with only limited precision, relying on powder-diffraction data obtained by film methods (Brauer & Zintl, ...the single-crystal ...
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Reinvestigation of Hg2GeSe4 based on single crystal data
... and crystal structure of Hg 2 GeSe 4 have been reported, but with limited precision (Parasyuk et ...2003). Single crystals of reasonable quality and size suitable for X-ray diffraction studies have not been ...
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α Lead tellurite from single crystal data
... The crystal structure of the title compound, -PbTeO 3 (PTO), has been reported previously by Mariolacos ...powder data. The current determination at room temperature from data obtained from ...
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Redetermination of Sr2PdO3 from single crystal X ray data
... Geometry . All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, ...
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Redetermination of Ba2CdTe3 from single crystal X ray data
... S2. Experimental The title compound was synthesized through a high temperature metal flux reaction. All starting elements were handled inside an Argon-filled glove box with controlled oxygen and moisture levels below 0.1 ...
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Redetermination of Dy3Ni from single crystal X ray data
... S1. Comment Lattice parameters for RE 3 Ni compounds with RE = Y, La, Pr, Nd, Sm, Gd–Tm, have been determined and their crystal structures reported to be isotypic with the Fe 3 C (or Al 3 Ni) type structure which ...
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Synthesis and structural characterization of a single crystal to single crystal transformable coordination polymer
... 85 open air for 24 hours to give the rehydrated sample. All the powder diffraction data of hydrated, dehydrated and rehydrated samples were collected in a STOE diffractometer under CuKα radiation in Debye-Scherrer ...
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Redetermination of the crystal structure of β zinc molybdate from single crystal X ray diffraction data
... S1. Synthesis and crystallization Reagents were used as commercial sources with no further purification. An aqueous solution was prepared by a mixture of 0.047 g 2,2′-bipyridine, 0.015 g of molybdenum trioxide and 0.043 ...
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Redetermination of the crystal structure of tetralithium octafluoridozirconate(IV), Li4ZrF8, from single crystal X ray data
... Alexander T. Chemey and Thomas E. Albrecht-Schmitt* Department of Chemistry and Biochemistry, Florida State University, 95 Chieftan Way, Tallahassee, FL 32306, USA. *Correspondence e-mail: [email protected] ...
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Redetermination of the crystal structure of NaTcO4 at 100 and 296 K based on single crystal X ray data
... anion) for which the validity of the proposed equations and approximations for the case of d- electrons are verified. It was believed that, owing to the d 0 electronic state, they define the least complex class of ...
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Reinvestigation of the Pb2[B5O9]Br structure based on single crystal data
... 4734 single-crystal re¯ections deviate signi®cantly from the reported powder data, the a parameter being ...the single-crystal data, errors are induced by the observed ...between ...
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Redetermination of dysprosium trinickel from single crystal X ray data
... full single-crystal X-ray determination of DyNi 3 , including refinement of the atomic coordinates and the temperature factors for all ...the crystal structure of DyNi 3 is shown in ...the ...
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Redetermination of tricalcium trilanthanum pentakis(orthoborate) from single crystal data
... Experimental Single crystals of compound (I) were grown using a LiBO 2 -containing ...for crystal growth was 1:1:4:3 of CaCO 3 (Sinopharm Regent, AR), La 2 O 3 (Materials, ...
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Redetermination of LaZn5 based on single crystal X ray diffraction data
... In contrast to previous determinations based on X-ray powder data [Nowotny (1942). Z. Metallkd. 34, 247–253; de Negri et al. (2008). Intermetallics, 16, 168–178], where unit-cell parameters and assignment of the ...
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Redetermination of the crystal structure of R5Si4 (R = Pr, Nd) from single crystal X ray diffraction data
... Condens. Matter, 14, 7191–7200] and X-ray [Smith et al. (1967). Acta Cryst. 22 940–943; Yang et al. (2002b). J. Alloys Compd. 339, 189–194; Yang et al., (2003). J. Alloys Compd. 263, 146–153] and ...
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Reinvestigation of NH4[Co(H2O)6]PO4 based on single crystal data
... supporting information sup-2 Acta Cryst. (2005). E61, i52–i54 Refinement . Refinement of F 2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F 2 , conventional R-factors R are based ...
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Crystal structures of cristobalite type and coesite type PON redetermined on the basis of single crystal X ray diffraction data
... 4. Refinement Crystal data, data collection and structure refinement details are summarized in Table 1. Structure refinements of both coe- PON and cri-PON were performed using occupancies of oxygen ...
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Magnetic properties of single-crystal DyAl2
... experimental data obtained for polycrystalline DyAl 2 ...experimental data. It is seen that the experimental data show that MCE is about zero for ⌬H=10 kOe and becomes more positive with increasing ...
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