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X-ray diffraction powder method

Synthesis, Spectral, Powder X-ray Diffraction and Bio-potential Activities of Hg(II) Complex of Benzimidazole and Benzoate Ion

Synthesis, Spectral, Powder X-ray Diffraction and Bio-potential Activities of Hg(II) Complex of Benzimidazole and Benzoate Ion

... The X-ray diffraction (powder method) study of the complexes was carried out using D8 Focus, Bruker ...diffusion method using Amikacin and ketoconazole as a standard for ...

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Synthesis and Characterization of Antimicrobial Activities of some Transition Metal Complexes of Asymmetrical Tetradentate Ligands Borde V. L 1, Naglolkar B. B2 , Shankarwar S. G 2and Shankarwar A.G1

Synthesis and Characterization of Antimicrobial Activities of some Transition Metal Complexes of Asymmetrical Tetradentate Ligands Borde V. L 1, Naglolkar B. B2 , Shankarwar S. G 2and Shankarwar A.G1

... X-ray powder diffraction: The x-ray diffractogram of metal complexes Cr(III), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II) of L was scanned in the range 20-80° at wavelength ...The ...

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Molecular Dynamics and X-ray Powder Diffraction Simulations: Investigation of nano-polycrystalline microstructure at the atomic scale coupling local structure configurations and X-ray powder Diffraction techniques

Molecular Dynamics and X-ray Powder Diffraction Simulations: Investigation of nano-polycrystalline microstructure at the atomic scale coupling local structure configurations and X-ray powder Diffraction techniques

... the powder diffraction pattern from an atomistic simulation of single crystals as well as of nano-polycrystalline ...(WA) method ( (Warren, et ...

156

Quantifying Isotibolone in Raw Materials of Tibolone

Quantifying Isotibolone in Raw Materials of Tibolone

... Isotibolone can be adequately identified and quantified using the Rietveld method and synchrotron X-ray powder diffraction data. In the case of pharmaceutical com- pounds, high ...

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Photodecolorization of methylene blue using CuO/γ Al2O3 prepared by low temperature combustion method

Photodecolorization of methylene blue using CuO/γ Al2O3 prepared by low temperature combustion method

... In this work, the CuO/γ-Al2O3 catalyst is prepared by low-temperature combustion method and characterized by X-ray powder diffraction XRD, the photo-activity has investigated on light so[r] ...

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Investigation of the structure of the perovskite system (1 x)BiFeO3 (x) (K0 5Bi0 5)TiO3

Investigation of the structure of the perovskite system (1 x)BiFeO3 (x) (K0 5Bi0 5)TiO3

... the method of powder synthesis was a solid state reaction method, which has been investigated by other groups ...by x-ray powder diffraction on these samples, it becomes ...

213

SYNTHESIS OF NOVEL ZIRCONIA-BASED SOLID SUPERACIDS, THEIR CHARACTERIZATION AND APPLICATION IN ORGANIC SYNTHESIS AND TRANSFORMATION REACTIONS

SYNTHESIS OF NOVEL ZIRCONIA-BASED SOLID SUPERACIDS, THEIR CHARACTERIZATION AND APPLICATION IN ORGANIC SYNTHESIS AND TRANSFORMATION REACTIONS

... BET method, application of X-ray powder diffraction studies for crystalline phase and size determination, temperature programmed desorption of ammonia analysis for acid strength ...

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Localization of ferrocene in NaY zeolite by powder x-ray and neutron diffraction

Localization of ferrocene in NaY zeolite by powder x-ray and neutron diffraction

... Zeolites are crystalline aluminosilicates with a three- dimensional open framework structure of channels and cavi- ties of molecular dimensions. Zeolites can thus act as mo- lecular sieves, making catalytic centers in ...

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Studies on the Synthesis, Growth and Characterization of ([Paranitrophenyl]Imino)Benzene NLO Crystal by Sankaranarayanan Ramasamy Method

Studies on the Synthesis, Growth and Characterization of ([Paranitrophenyl]Imino)Benzene NLO Crystal by Sankaranarayanan Ramasamy Method

... SR method using a seed as the ...crystal X-ray diffraction (XRD), X-ray powder diffraction (XRPD), Fourier Transform In- frared (FTIR), Ultraviolet-Visible-Near ...

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Effect of Synthesis Routes on Microstructure of Nanocrystalline Cerium Oxide Powder

Effect of Synthesis Routes on Microstructure of Nanocrystalline Cerium Oxide Powder

... ceria powder has been ...of X-ray diffraction (XRD), particle size analysis, scanning electron microscopy (SEM), and transmission electron microscopy ...ceria powder is much wider than ...

5

Redetermination of the crystal structure of NaTcO4 at 100 and 296 K based on single crystal X ray data

Redetermination of the crystal structure of NaTcO4 at 100 and 296 K based on single crystal X ray data

... on X-ray powder diffraction film data [Schwochau ...neutron powder diffraction data using the Rietveld method [Weaver et ...neutron diffraction structure ...

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Synthesis and Characterization of Barium-Vanadium Oxide Nanocomposite Using a Facile thermolysis Approach

Synthesis and Characterization of Barium-Vanadium Oxide Nanocomposite Using a Facile thermolysis Approach

... Analyzer. X-ray powder diffraction (XRD) measurements were performed using an X’pert diffractometer of Philips Company with graphite monochromatic Cu K á radiation at room temperature in the ...

5

X ray powder diffraction study of LiCrP2O7

X ray powder diffraction study of LiCrP2O7

... = Mn, Fe, V, Mo, Sc and In), was refined from laboratory X-ray powder diffraction data using the Rietveld method. The Cr 3+ cation is bonded to six O atoms from five diphosphate anions ...

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Sol Gel Combustion Synthesis, Structural and Optical Band Gap Energy Study of Zn0 85Ni0 1Mg0 05Fe2O4 Nanoparticles

Sol Gel Combustion Synthesis, Structural and Optical Band Gap Energy Study of Zn0 85Ni0 1Mg0 05Fe2O4 Nanoparticles

... powder diffraction (XRD), Furrier transform infrared (FTIR) spectroscopy and ultraviolent-visible (UV-vis) spectroscopy. Using these techniques, the structure as well as the optical property of the ...

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Effect of Lithium Doping on the Properties L Citrulline Oxalate Monohydrate Nonlinear Optical Crystals

Effect of Lithium Doping on the Properties L Citrulline Oxalate Monohydrate Nonlinear Optical Crystals

... citrulline oxalate (LCO) were grown successfully by slow evaporation technique. The effect of doping with lithium in L-citrulline oxalate crystals is examined in this paper. The powder XRD studies confirm the ...

5

X- RAY DIFFRACTION

X- RAY DIFFRACTION

... Fresh Australia abalones (approximately size of 50mm in length, 30mm in width and shell thickness about 600μm) were purchased from market and the fresh shucked shells were stored in tap water at room temperature. Flat ...

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Laumann, Andreas
  

(2011):


	Novel routes to Li4Ti5O12 spinel: Characterization and phase relations.


Dissertation, LMU München: Fakultät für Geowissenschaften

Laumann, Andreas (2011): Novel routes to Li4Ti5O12 spinel: Characterization and phase relations. Dissertation, LMU München: Fakultät für Geowissenschaften

... with the experimental value of 640 meV 14 at the same temperature. It should be emphasized that the PDF, as determined by diffraction methods, is a time and space average and is thus comparable to macroscopic ...

164

Formulation Development and Validation of Analytical Technique for Novel Drug.

Formulation Development and Validation of Analytical Technique for Novel Drug.

... This method utilizes the physio chemical property of polymers, the polymers which are insoluble in alkaline pH medium, but precipitates/coacervates when it comes in contact with alkaline ...The method is ...

192

Analysis of Heavy Metals in a Tailing Impoundment of Abandoned Mn Mine
by Using Two Sequential Extractions*

Analysis of Heavy Metals in a Tailing Impoundment of Abandoned Mn Mine by Using Two Sequential Extractions*

... Figure 7 shows the comparison between both sequential ex- traction methods for Mn, Fe, Zn and S. The results indicate that the amount of first fraction, that is, HCl-extractable, is fairly correspondent to sum of ...

6

Revision of the Li13Si4 structure

Revision of the Li13Si4 structure

... 1, the resulting calculated pattern is in very good agreement with the experimental one. Main differences to the previous single-crystal X-ray structure determination by Frank et al. (1975) are i) a ...

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