Solid State NMR Experiments
Membrane binding of an acyl-lactoferricin B antimicrobial peptide from solid-state NMR experiments and molecular dynamics simulations
... with solid-state NMR experiments to charac- terize the associations of the small acylated hexapeptide C6-LfB6 with both a model bacterial membrane (POPE:POPG in 3:1 ratio) and a model ...
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A suite of solid state NMR experiments to utilize orphaned magnetization for assigning proteins using parallel high and low gamma detection
... two-receiver solid-state NMR experiments for backbone and side chain resonance ...The experiments rely on either dipolar coupling or scalar coupling for polarization transfer and are ...
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Enhancing the Sensitivity of Solid-State NMR Experiments with Very Low Gyromagnetic Ratio Nuclei with Fast Magic Angle Spinning and Proton Detection
... for solid-state NMR experiments with very low-γ spin-1/2 nuclei such as 89 Y, 103 Rh, 109 Ag and 183 ...of solid-state NMR experiments with 4 mm and ...HETCOR ...
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87Sr,119Sn,127I single and {1H/19F} double resonance solid state NMR experiments : application to inorganic materials and nanobuilding blocks
... advanced solid state NMR techniques could be valuable tools of investigation for materials involving strontium, iodine and ...involved NMR interactions, here quadrupolar and/or ...
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Characterisation of inorganic materials using solid state NMR spectroscopy
... anisotropy Solid-state NMR experiments are typically performed under MAS conditions, averaging out anisotropic interactions ...assigning solid-state NMR ...
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Dipolar recoupling in solid state NMR by phase alternating pulse sequences
... recoupling experiments are the building blocks of essentially all biological solid-state NMR experiments using “powder” ...recoupling experiments are sensitive to the amplitude ...
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Homonuclear correlation in solid state NMR : developing experiments for half integer quadrupolar nuclei
... 1.2. Thesis Overview and Motivation 7 characterisations that help to cement understanding of borates, as well as the important differences between crystalline and disordered materials. Initial NMR results are also ...
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Solid-State NMR of CO2 Mineralization and NMR Crystallography
... an NMR study of two packed beds of forsterite reacted with 13 CO 2 : one with a water-slurry and one with a ...of experiments with a relatively long recycle delay (390 s) to achieve sufficient ...
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Prediction of NMR parameters in the solid-state
... T B = 1 + R,n e 2h ie r·R×B [ | φ R,n − | ˜ φ R,n ] p ˜ R,n | e − 2h ie r·R×B (26) The resulting approach is known as the gauge including projector augmented wave (GIPAW ) method. Although orig- inally formulated for ...
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Continuous Wave NMR Imaging in the Solid State
... swept experiments, in which the NMR spectrometer frequency was swept such that the sensitive slice moved through the sample, have been carried out on sufficiently thin samples 28 ...These experiments ...
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Molecular architecture of softwood revealed by solid state NMR
... FT-IR experiments indicate that the hemicelluloses, and to some extent the lignin, are aligned in parallel to the cellulose, perhaps within these softwood macrofibrils 7,8 ...These experiments provide ...
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Solution- and solid-state NMR studies of GPCRs and their ligands
... 5.1. Detergent micelles and organic solvents Micellar detergent solutions have been used extensively in NMR experiments on membrane proteins; and are typically the solubilising agent of choice in solNMR. In ...
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Solid-state NMR of Complex Nano- and Microcrystalline Materials
... the solid sample of interest, and is able to form a spin glass at 100 ...the solid particles or occupies inter-particle void ...current state-of-the-art 1 H DNP NMR experiments ...
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Solid-State NMR of Quadrupolar Nuclei for Structural Elucidation
... Al NMR experiments and DFT calculations are invaluable for shedding light on the nature of the Al sites in the cage-like MAO structures, and show great potential for identification of the nature of ...
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Characterization of Inorganic Catalysts and Materials by Solid-State NMR
... NQR experiments are provided in the introduction to Chapter ...field NMR spectrometers throughout the world and the continued development of pulsed NMR techniques, SSNMR spectroscopy of nearly any ...
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Multinuclear solid state NMR for the characterisation of inorganic materials
... before NMR calculations were carried out, which has often been seen to provide improved agreement between calculation and NMR ...whereas NMR data are usually collected at room ...
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Perspective : current advances in solid state NMR spectroscopy
... Secondly, powdered materials are generally not magnetically isotropic; different particle orientations will have different magnetic susceptibilities, and hence different effective local magnetic fields. The resulting ...
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Combining solid state NMR spectroscopy with first principles calculations – a guide to NMR crystallography
... in NMR spectroscopy, and its growing use for determining or refining structural models, have led to the emergence of a new field, termed ‘‘NMR ...of NMR spectroscopy (often in combination with ...
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Diffraction and Solid State NMR Studies of Inorganic Framework Materials.
... O NMR probes into the local oxygen environment and provides localised information about the oxygen ...sites. NMR can be used to investigate dynamic processes although prior to 2002 it had not been commonly ...
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A solid state NMR method for solution of zeolite crystal structures
... pulse and 60 s recycle delay. The spectrum was fit with four Lorentzian peaks of equal area as shown in Figure 3a and summarized in Table S1. The 29 Si T 1 relaxation times were measured with a saturation recovery ...
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