Solid State NMR method
A solid state NMR method for solution of zeolite crystal structures
... MAS NMR spectrum, and that the connectivities between the sites were in agreement with the intersite connec- tivities derived from the 2D 29 Si DQ correlation ...
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A solid state NMR method for solution of zeolite crystal structures
... Figure S5. Two-dimensional 29 Si SR26 4 11 double-quantum correlation spectra of zeolite test sample 1 obtained at the indicated recoupling times. 4.4 Structure solution by solid-state NMR The ...
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Prediction of NMR parameters in the solid-state
... T B = 1 + R,n e 2h ie r·R×B [ | φ R,n − | ˜ φ R,n ] p ˜ R,n | e − 2h ie r·R×B (26) The resulting approach is known as the gauge including projector augmented wave (GIPAW ) method. Although orig- inally formulated ...
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Continuous Wave NMR Imaging in the Solid State
... STRAFI method have been reported. Frequency- swept experiments, in which the NMR spectrometer frequency was swept such that the sensitive slice moved through the sample, have been carried out on ...
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Biological Membrane Structure By Solid-State NMR
... particularly solid-state NMR spectroscopy, is a method of choice to study the structure and dynamics of both the lipid and the protein components of model and biological ...C ...
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Solution- and solid-state NMR studies of GPCRs and their ligands
... reliable method for novel drug ...and solid-state NMR approaches have been developed and have provided new insights, particularly focussing on the study of protein-ligand interactions which ...
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Solid-state NMR of Complex Nano- and Microcrystalline Materials
... SSNMR is an excellent complementary technique to those mentioned above, but can also act as a standalone method of characterization when these other methods are inadequate. Among many classes of nanomaterials, ...
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Multinuclear solid state NMR for the characterisation of inorganic materials
... many NMR parameters, ...(PAW) method. 53,54 The PAW method has been modified to allow the calculation of NMR parameters of a nucleus within a magnetic field, gauge-including PAW (GIPAW), 55 ...
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Perspective : current advances in solid state NMR spectroscopy
... with NMR spectroscopy in the solid state will remain the subject of ongoing research effort and technological ...for NMR, and for solid-state NMR in ...conventional ...
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Diffraction and Solid State NMR Studies of Inorganic Framework Materials.
... 26 Chapter 3 Characterisation techniques 3.1 X-Ray Diffraction (XRD) X-Ray diffraction is a very powerful structural characterisation method that can be used to determine the full structure of a material. ...
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Solid state NMR studies of inorganic pigment materials and catalysts
... the method to produce this line is a form of sphere ...the method is not quite as quick as Alderman-Grant interpolation this only results in a factor of 8 slow down for a similar quality spectrum, resulting ...
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Development of solid state NMR techniques for the characterisation of pharmaceutical compounds
... Solid-state NMR techniques applied to solid delivery forms are presented as an alternative to more established structural characterisation ...this method, proton transfer in an ...
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Intermolecular interactions and protein dynamics by solid state NMR spectroscopy
... this method- ology is applicable to a general case of systems with little or no overall symmetry, and samples containing only a few nanomoles of protein can yield spectra with a sensitivity and resolution suitable ...
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The Evaluation of Polyethylene/Clay Composite from Solid State NMR
... [7-16]. Solid-state NMR has become an indispensable ana- lytical tool for the study of crystalline and amorphous materials as silicates; zeolites; concretes and glasses, for instance ...powerful ...
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Algorithms for automated assignment of solution-state and solid-state protein NMR spectra.
... 26 parsing requirements of each peak list format. Additional peak list parsers can be easily defined by subclassing the abstract PeakListParser object. Figure 11 shows the class dependency diagram for the PeakFilter ...
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Structure of (KIAGKIA)3 Aggregates in Phospholipid Bilayers by Solid-State NMR
... Once proximity has been established, a simpler method can be used for quantitation. Because K3 exists exclusively in an all a-helical conformation, the resonance frequency of the labeled carbonyl carbon of Ala 10 ...
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Computing of 93Nb NMR Parameters of Solid-State Niobates. The Geometry Matters
... complex solid-state NMR spectra and it is frequently difficult to extract all the information from these ...a method for calculating electric field gradients (EFG) in solids using the ...
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The development of solid state NMR methodology to study the dynamics of proteins and ice
... In order to access these relatively fast dynamics within the bulk ice of the frozen antifreeze solutions, variable temperature 1 H R 1 measurements were conducted using the saturation recovery method (Figure ...
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Methods for the determination of the structures and dynamics of proteins by solid state NMR spectroscopy
... this method would be equally effective for sedimented or crystallised samples, simple precipitation was found to be a suitable preparation method for this complex, which by extension is likely to be ...
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Techniques of solid-state NMR
... Sanchez 'Surface and bulk characterisation of titanium oxo clusters and nanosized titania particles through 17O solid state NMR.' J. All transitions exhibit second order effects[r] ...
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