Solid state NMR (ssNMR) spectroscopy
Structural Insights into Group 14 Compounds from Solid-State NMR Spectroscopy
... Solid-state NMR spectroscopy is a powerful complement as it makes it possible to circumvent some of the limitations of ...SSNMR spectroscopy. NMR experiments are most commonly ...
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Seminar. Solid-state NMR Spectroscopy
... 3 Solid-state NMR spectroscopy The appearance of NMR spectra is determined by various interactions of nuclear spins with each other, and other quantities like the local and applied ...
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Perspective : current advances in solid state NMR spectroscopy
... of solid-state NMR spectroscopy, it is necessary to address several challenges, not least of which is the need to improve resolution – to remove the effects of anisotropy and to enable ...
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Combining solid state NMR spectroscopy with first principles calculations – a guide to NMR crystallography
... in NMR spectroscopy, and its growing use for determining or refining structural models, have led to the emergence of a new field, termed ‘‘NMR ...of NMR spectroscopy (often in ...
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Investigation of zeolitic imidazolate frameworks using 13C and 15N solid state NMR spectroscopy
... N solid-state NMR spectroscopy to characterise the local structure and disorder in a variety of single- and dual-linker ...solution-state NMR spectroscopy and the use of ...
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Exploring membrane selectivity of the antimicrobial peptide KIGAKI using solid-state NMR spectroscopy
... paper, solid-state NMR spectroscopy was utilized to decipher the interaction mechanism of the KIGAKI peptide with a variety of different ...
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Characterization of Pharmaceutical Cocrystals and Salts by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy
... of solid active pharmaceutical ingredients ...or solid-phase reactions of APIs with suitable cocrystal coformers, which are often weak ...multicomponent solid is whether it should be classified as a ...
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Characterization of Pharmaceutical Cocrystals and Salts by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy
... of solid active pharmaceutical ingredients ...or solid-phase reactions of APIs with suitable cocrystal coformers, which are often weak ...multicomponent solid is whether it should be classified as a ...
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Proton-detected solid-state NMR spectroscopy of a zinc diffusion facilitator protein in native nanodiscs
... outward-facing state [18] (Escherichia coli Yiip, see homology model in Figure 1a), the other in an inward-facing state [19] (Shewanella oneidensis ...high-resolution solid-state NMR ...
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Structure and Alignment of the Membrane-Associated Peptaibols Ampullosporin A and Alamethicin by Oriented 15N and 31P Solid-State NMR Spectroscopy
... P solid-state NMR ...coupling solid-state NMR correlation spectroscopy suggests that in their trans- membrane configuration both peptides adopt mixed a-/3 10 -helical ...
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Intermolecular interactions and protein dynamics by solid state NMR spectroscopy
... NMR spectroscopy offers access to atomic-resolution details of the dynamics over a wide range of time ...solution NMR methods, where slow molecular tumbling leads to enhanced transverse relaxation ...
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Methods for the determination of the structures and dynamics of proteins by solid state NMR spectroscopy
... With rapid development comes potential for applying SSNMR to increasingly complex systems, offering deeper understanding into the workings of biological mechanisms at the molecular level. Large proteins and complexes ...
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Solid-State NMR Spectroscopy of Unreceptive Nuclei in Inorganic and Organic Systems
... 2 1 ω 0 (3 & 4I(I % 1)){ 1 2 V 00 Q % 4V 20 Q % 9V 40 Q } (2.33) larger than the CSA as measured in Hz; in this case, the isotropic peak will be the only observable peak. However, when the spinning speed is less than the ...
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Rapid Characterization of Formulated Pharmaceuticals Using Fast MAS 1H Solid-State NMR Spectroscopy
... SSNMR spectroscopy has not been demonstrated as a method to detect APIs in realistic dosage forms, likely because the limited resolution of 1 H SSNMR spectra causes intense 1 H NMR signals from the abundant ...
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Site specific identification of an Aβ fibril heparin interaction site by using solid state NMR spectroscopy
... MHz solid-state NMR Facility was funded by EPSRC, BBSRC, and the University of Warwick, including funding through Birmingham Science City Advanced Materials Projects 1 and 2 supported by Advantage ...
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Characterisation of inorganic materials using solid state NMR spectroscopy
... the NMR spectrum owing to the incomplete averaging of the dipolar ...MAS NMR spectrum, there is then the potential for the spinning sidebands to overlap, complicating or preventing ...
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Recent developments in solid state NMR spectroscopy of crystalline microporous materials
... predicted NMR parameters and those observed ...and NMR spectroscopy that is often referred to as NMR crystallography, as described previously, in many cases additional insight can be gained by ...
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New methods and applications in solid state NMR spectroscopy of quadrupolar nuclei
... the solid-state chemist is which of these established methods to choose? The literature shows that the most widely applied technique is MQMAS, which has enabled site resolution and extraction of structural ...
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$^{17}$O Solid-State NMR Spectroscopy of Functional Oxides for Energy Conversion
... solution state, rapid molecular tumbling faster than the NMR timescale averages out the anisotropy of many of the spin interactions, resulting in the observation of sharp resonances at the isotropic value ...
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Longer range distances by spinning angle encoding solid state NMR spectroscopy
... 10 acquisition of the free-induction decay, so as to obtain optimum sensitivity. The retention of both ideal resolution and long-range distance sensitivity was achieved by redesigning a 600 MHz HX MAS NMR probe to ...
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