solid state NMR spectroscopy
Seminar. Solid-state NMR Spectroscopy
... 3 Solid-state NMR spectroscopy The appearance of NMR spectra is determined by various interactions of nuclear spins with each other, and other quantities like the local and applied ...
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Perspective : current advances in solid state NMR spectroscopy
... of solid-state NMR spectroscopy, it is necessary to address several challenges, not least of which is the need to improve resolution – to remove the effects of anisotropy and to enable ...
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Combining solid state NMR spectroscopy with first principles calculations – a guide to NMR crystallography
... in NMR spectroscopy, and its growing use for determining or refining structural models, have led to the emergence of a new field, termed ‘‘NMR ...of NMR spectroscopy (often in ...
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Structural Insights into Group 14 Compounds from Solid-State NMR Spectroscopy
... Solid-state NMR spectroscopy is a powerful complement as it makes it possible to circumvent some of the limitations of ...SSNMR spectroscopy. NMR experiments are most commonly ...
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Investigation of zeolitic imidazolate frameworks using 13C and 15N solid state NMR spectroscopy
... N solid-state NMR spectroscopy to characterise the local structure and disorder in a variety of single- and dual-linker ...solution-state NMR spectroscopy and the use of ...
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Exploring membrane selectivity of the antimicrobial peptide KIGAKI using solid-state NMR spectroscopy
... paper, solid-state NMR spectroscopy was utilized to decipher the interaction mechanism of the KIGAKI peptide with a variety of different ...
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Characterization of Pharmaceutical Cocrystals and Salts by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy
... of solid active pharmaceutical ingredients ...or solid-phase reactions of APIs with suitable cocrystal coformers, which are often weak ...multicomponent solid is whether it should be classified as a ...
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Characterization of Pharmaceutical Cocrystals and Salts by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy
... of solid active pharmaceutical ingredients ...or solid-phase reactions of APIs with suitable cocrystal coformers, which are often weak ...multicomponent solid is whether it should be classified as a ...
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Proton-detected solid-state NMR spectroscopy of a zinc diffusion facilitator protein in native nanodiscs
... outward-facing state [18] (Escherichia coli Yiip, see homology model in Figure 1a), the other in an inward-facing state [19] (Shewanella oneidensis ...high-resolution solid-state NMR ...
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Structure and Alignment of the Membrane-Associated Peptaibols Ampullosporin A and Alamethicin by Oriented 15N and 31P Solid-State NMR Spectroscopy
... P solid-state NMR ...coupling solid-state NMR correlation spectroscopy suggests that in their trans- membrane configuration both peptides adopt mixed a-/3 10 -helical ...
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Intermolecular interactions and protein dynamics by solid state NMR spectroscopy
... NMR spectroscopy offers access to atomic-resolution details of the dynamics over a wide range of time ...solution NMR methods, where slow molecular tumbling leads to enhanced transverse relaxation ...
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Characterisation of inorganic materials using solid state NMR spectroscopy
... the NMR spectrum owing to the incomplete averaging of the dipolar ...MAS NMR spectrum, there is then the potential for the spinning sidebands to overlap, complicating or preventing ...
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Methods for the determination of the structures and dynamics of proteins by solid state NMR spectroscopy
... With rapid development comes potential for applying SSNMR to increasingly complex systems, offering deeper understanding into the workings of biological mechanisms at the molecular level. Large proteins and complexes ...
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Recent developments in solid state NMR spectroscopy of crystalline microporous materials
... predicted NMR parameters and those observed ...and NMR spectroscopy that is often referred to as NMR crystallography, as described previously, in many cases additional insight can be gained by ...
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Solid-State NMR Spectroscopy of Unreceptive Nuclei in Inorganic and Organic Systems
... 2 1 ω 0 (3 & 4I(I % 1)){ 1 2 V 00 Q % 4V 20 Q % 9V 40 Q } (2.33) larger than the CSA as measured in Hz; in this case, the isotropic peak will be the only observable peak. However, when the spinning speed is less than the ...
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New methods and applications in solid state NMR spectroscopy of quadrupolar nuclei
... the solid-state chemist is which of these established methods to choose? The literature shows that the most widely applied technique is MQMAS, which has enabled site resolution and extraction of structural ...
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$^{17}$O Solid-State NMR Spectroscopy of Functional Oxides for Energy Conversion
... solution state, rapid molecular tumbling faster than the NMR timescale averages out the anisotropy of many of the spin interactions, resulting in the observation of sharp resonances at the isotropic value ...
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Longer range distances by spinning angle encoding solid state NMR spectroscopy
... 10 acquisition of the free-induction decay, so as to obtain optimum sensitivity. The retention of both ideal resolution and long-range distance sensitivity was achieved by redesigning a 600 MHz HX MAS NMR probe to ...
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An Investigation of the Milled Wood Lignin Isolation Procedure by Solution- and Solid-State NMR Spectroscopy.
... 1 H spectra are most commonly collected using acetylated lignins as information concerning the phenolic and aliphatic hydroxyl groups can be obtained. Acetylated lignins are typically dissolved in CDCl 3 , although other ...
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Retinal dynamics during light activation of rhodopsin revealed by solid-state NMR spectroscopy
... II state is reached [32] , whereas the 2 H NMR relaxation data suggest that the β4 strand displacement happens already in the meta I ...I state (15 kJ/mol versus about 12 kJ/mol in the dark and meta ...
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