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Solid State NMR

Techniques of solid-state NMR

Techniques of solid-state NMR

... Sanchez 'Surface and bulk characterisation of titanium oxo clusters and nanosized titania particles through 17O solid state NMR.' J. All transitions exhibit second order effects[r] ...

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Development of solid state NMR techniques for the characterisation of pharmaceutical compounds

Development of solid state NMR techniques for the characterisation of pharmaceutical compounds

... world. NMR is a site-specific tool which is sensitive to subtle changes in chemical ...the solid state is often more appropriate than liquid state ...the NMR interactions, which ...

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Solid-state NMR applied to photosynthetic light-harvesting complexes

Solid-state NMR applied to photosynthetic light-harvesting complexes

... how solid-state NMR has provided a mechanistic and electronic picture of pigment–protein and pigment–pigment interactions in photosynthetic antenna ...complexes. NMR results on purple ...

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The Evaluation of Polyethylene/Clay Composite from Solid State NMR

The Evaluation of Polyethylene/Clay Composite from Solid State NMR

... by solid-state nuclear magnetic resonance (NMR). The solid-state NMR measurements were used to observe both polymer matrix (through carbon-13 and hydrogen nuclei) and the clay ...

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Characterisation of inorganic materials using solid state NMR spectroscopy

Characterisation of inorganic materials using solid state NMR spectroscopy

... new solid is made, it is usually subjected to single-crystal X-ray diffraction, which still seen as the ‘gold standard’ for structure determination by ...and NMR is a highly complementary technique ...

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Solid state NMR studies of inorganic pigment materials and catalysts

Solid state NMR studies of inorganic pigment materials and catalysts

... Using multiple quantum (MQ)[42] techniques the anisotropic quadrupolar term can be refocused so that only the isotropic term of the quadrupolar inter- action affects the spectra. This is possible due to the isotropic and ...

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Intermolecular interactions and protein dynamics by solid state NMR spectroscopy

Intermolecular interactions and protein dynamics by solid state NMR spectroscopy

... The research leading to these results has received funding from the European Research Council under the European Union’s Seventh Framework Programme (FP/2007-2013)/ ERC Grant Agreement 639907. J.R.L. also acknowledges ...

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The development of solid state NMR methodology to study the dynamics of proteins and ice

The development of solid state NMR methodology to study the dynamics of proteins and ice

... chapter, solid-state NMR relaxation measurements are used to investigate the proton dynamics and exchange within ice in the presence of antifreeze (glyco)proteins and their synthetic ...

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A solid state NMR method for solution of zeolite crystal structures

A solid state NMR method for solution of zeolite crystal structures

... Powder XRD data (7 – 75 o 2θ) were collected in transmission mode on a Stoe STADIP diffractometer equipped with a monochromator (Cu Kα, λ = 1.54056 Å) and a position sensitive detector. The powder diffraction pattern was ...

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A solid state NMR method for solution of zeolite crystal structures

A solid state NMR method for solution of zeolite crystal structures

... Structure completion and refinements of the zeolite crystal structures against the powder XRD data were carried out using the atomic coordinates for the silicon atoms solved by solid-state NMR as the ...

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Multinuclear solid state NMR investigation of Hexaniobate and Hexatantalate compounds

Multinuclear solid state NMR investigation of Hexaniobate and Hexatantalate compounds

... Therefore this site is more prone to accommodate the Nb-Ta substitution. This assumption was clearly corroborated by 1 H MAS NMR data (insert (B) in Figure 7) where the resonance at ~ + 4.9 ppm can be safely ...

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Bio-Solid State NMR

Bio-Solid State NMR

... Magic angle spinning solid state NMR narrows anisotropically broadened spectra.. Small (Mr ~ 3k) peptide in fluid lipid bilayers Static NMR spectrum.[r] ...

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The use of solid state NMR to monitor reactions and doping in inorganic materials

The use of solid state NMR to monitor reactions and doping in inorganic materials

... Solid state NMR studies on of melt-quench glasses and sol-gel nanoparticles has been an active research area for a ...while. Solid state NMR’s strength to investi- gate local structural ...

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Perspective : current advances in solid state NMR spectroscopy

Perspective : current advances in solid state NMR spectroscopy

... predicting solid-state NMR ...quadrupolar NMR parameters is relatively straightforward, as the EFG is a function solely of the total charge density, while the shielding tensor requires the ...

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Theory and applications of supercycled symmetry based recoupling sequences in solid state NMR

Theory and applications of supercycled symmetry based recoupling sequences in solid state NMR

... For most macromolecular applications of solid-state NMR, the employed techniques must be compatible with magic-angle spinning 共MAS兲, which provides good sensitiv- ity and resolution. 1–5 A wide ...

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Symmetry based pulse sequences in solid state NMR and applications to biological systems

Symmetry based pulse sequences in solid state NMR and applications to biological systems

... In solidstate NMR, all the spin interactions survive motional averag- ing, unlike the case of solution–state NMR where all interactions except the isotropic scalar coupling, J, and ...

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Recent technique developments and applications of solid state NMR in characterising inorganic materials

Recent technique developments and applications of solid state NMR in characterising inorganic materials

... ion-exchangers. Solid state niobate chemistry also plays a crucial role in several very important piezoelectric phases, as well as several other technological applications such as optical materials and ...

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Development of solid state NMR on disordered systems, from bioactive glasses to mullites

Development of solid state NMR on disordered systems, from bioactive glasses to mullites

... Early solid state NMR studies on glasses first appeared in the 1950s,[54] al- though due to the broad nature of the NMR resonances arising from the vast array of nuclear sites found within its ...

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New methods and applications in solid state NMR spectroscopy of quadrupolar nuclei

New methods and applications in solid state NMR spectroscopy of quadrupolar nuclei

... of NMR parameters from first ...a solid as a cluster (centred on the atom of interest and with remote bonds terminated, typically by H), had limited the influence of computation in solid-state ...

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Solid state NMR of a protein in a precipitated complex with a full length antibody

Solid state NMR of a protein in a precipitated complex with a full length antibody

... typical solid-state NMR studies of protein complexes in the literature) in ∼10 min with fast recycling enabled by the addition of 50 mM Cu II − ...of solid-state NMR spectroscopy ...

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